SN/T 1924-2011 English PDF

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SN/T 1924-2011: Determination of clenbuterol, ractopamine, salbutemol and terbutalin residues in foodstuffs of animal origin for import and export. HPLC-MS/MS Method
Status: Valid

SN/T 1924: Historical versions

Standard ID	USD	BUY PDF	Lead-Days	Standard Title (Description)	Status
SN/T 1924-2011	369	Add to Cart	3 days	Determination of clenbuterol, ractopamine, salbutemol and terbutalin residues in foodstuffs of animal origin for import and export. HPLC-MS/MS Method	Valid
SN/T 1924-2007	839	Add to Cart	6 days	Determination of clenbuterol, ractopamine, salbutamol and terbutalin residues in foodstuffs of animal origin for import and export. HPLC-MS/MS method	Obsolete

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Basic data

Standard ID: SN/T 1924-2011 (SN/T1924-2011)
Description (Translated English): Determination of clenbuterol, ractopamine, salbutemol and terbutalin residues in foodstuffs of animal origin for import and export. HPLC-MS/MS Method
Sector / Industry: Commodity Inspection Standard (Recommended)
Classification of Chinese Standard: C53
Classification of International Standard: 67.020
Word Count Estimation: 14,194
Date of Issue: 2011-02-25
Date of Implementation: 2011-07-01
Older Standard (superseded by this standard): SN/T 1924-2007
Quoted Standard: GB/T 6682
Regulation (derived from): ?AQSIQ-Inspection [2011] 90
Issuing agency(ies): General Administration of Customs
Summary: This standard specifies the import and export of food of animal origin clenbuterol, ractopamine, salbutamol and terbutaline residual liquid chromatography-mass spectrometry/mass spectrometry (HPLC-MS/MS) Determination and confirmatory methods. This standard applies to the import and export of animal source foods muscle, viscera, fine bone soup and milk, milk Clenbuterol, ractopamine, salbutamol and terbutaline residues measured and confirmed.

SN/T 1924-2011: Determination of clenbuterol, ractopamine, salbutemol and terbutalin residues in foodstuffs of animal origin for import and export. HPLC-MS/MS Method

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of clenbuterol, ractopamine, salbutemol and terbutalin residues in foodstuffs of animal origin for import and export.HPLC-MS/MS Method People's Republic of China Entry-Exit Inspection and Quarantine Standards Instead of the SN/T 1924-2007 Import and export of food of animal origin clenbuterol, Laikeduoba Amines, salbutamol and terbutaline determination of residues Liquid chromatography - mass spectrometry/mass spectrometry Determinationofclenbuterol, ractopamine, salbutemolandterbutalin HPLC-MS/MSMethod Issued on. 2011-02-25 2011-07-01 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released

Foreword

This standard was drafted in accordance with GB/T 1.1-2009 given rules. Instead of the standard SN/T 1924-2007 "Importers clenbuterol in food of animal origin, Lecco dopamine, salbutamol, terbutaline Detection of Residual liquid chromatography - mass spectrometry/mass spectrometry. " This standard compared with SN/T 1924-2007, the main technical changes are as follows. --- Increasing the scope of food of animal origin fine bone soup, milk and milk powder; --- Sample before adding n-hexane degreasing step; --- By a C18 solid phase extraction column and cation exchange column changed to mixed cation exchange column; --- Sample liquid solvent consisting of aqueous acetonitrile (19) is amended as 0.1% formic acid; --- Clenbuterol ion monitoring by the 277.3/203.0,277.3/modify 277.0 259.2/203.0,277.0/132.0, 277.0/168.0; --- The experiments prove that the lower limit of the measurement Clenbuterol 0.5μg/kg revised to 0.05μg/kg. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard was drafted. People's Republic of China Shandong Entry Inspection and Quarantine Bureau, People's Republic of China Shanghai Entry-Exit Inspection and Quarantine Bureau, Chinese Academy of Inspection and Quarantine. The main drafters of this standard. Wang Mei, cattle Zengyuan, Cai hair, Deng Xiaojun, Tangzhi Xu, Zhang Feng, Zhang Gang, Luo Xin, Chen Shan, Zhang Hongwei, Pang Shiping. This standard replaces the standards previously issued as follows. --- SN/T 1924-2007. Import and export of food of animal origin clenbuterol, Laikeduoba Amines, salbutamol and terbutaline determination of residues Liquid chromatography - mass spectrometry/mass spectrometry

1 Scope

This standard specifies the import and export of food of animal origin clenbuterol, ractopamine, salbutamol and terbutaline residual amount of liquid chromatography Spectrum - mass spectrometry/mass spectrometry (HPLC-MS/MS) method for the determination and confirmation. This standard applies to the import and export of food of animal origin muscles, organs, bone soup and fine milk, milk powder clenbuterol, ractopamine, sand Butylamine alcohol terbutaline Residues Determination and confirmation.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document. Laboratory use specifications and test methods GB/T 6682 Analysis

3 Method summary

Sample of clenbuterol, ractopamine, salbutamol and terbutaline residue using β- glucuronidase enzyme glycosides/aryl sulfatase enzyme Solution of ammonium acetate buffer solution extraction, hexane, and the aqueous phase solution was mixed cation exchange solid phase extraction (SPE), HPLC-MS/MS Determination of internal standard.

4 Reagents and materials

Unless otherwise indicated, the reagents used were of analytical grade water as a water line with GB/T 6682 regulations. 4.1 acetonitrile. HPLC grade. 4.2 Methanol. HPLC grade. 4.3 hexane. HPLC grade. Ethyl acetate 4.4. HPLC grade. 4.5 formic acid. HPLC grade. Ammonium acetate 4.6. HPLC grade. Concentrated hydrochloric acid 4.7. content of 36 to 38%. Ammonia 4.8. content of 25% to 28%. 4.9 β- glucuronidase enzyme glycosides/arylsulfatase solution. glycosides containing [beta] glucuronidase enzymes 111000U/mL; arylsulfatase 1079U/mL. 4.10 ammonium acetate buffer solution (2mol/L). Weigh ammonium acetate (4.6) 77.0g, diluted with water and dilute to 500mL, and mix with B Acid adjusted to pH 5.2. 4.11 0.1% formic acid solution. Pipette 1.0mL of formic acid (4.5), diluted with water and dilute to 1000mL, and mix. 4.12 0.1mol/L hydrochloric acid solution. take 9mL concentrated hydrochloric acid (4.7), diluted with water to 1000mL, and mix. ......

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