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                    Test method of physical properties for sulfur exhaust hydrogenation catalyst
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                    GB/T 33068-2016
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  Basic data             |  Standard ID  |          GB/T 33068-2016 (GB/T33068-2016) |               |  Description (Translated English)  |          Test method of physical properties for sulfur exhaust hydrogenation catalyst |               |  Sector / Industry  |          National Standard (Recommended) |               |  Classification of Chinese Standard  |          G74 |               |  Classification of International Standard  |          71.100.99 |               |  Word Count Estimation  |          6,644 |               |  Date of Issue  |          2016-10-13 |               |  Date of Implementation  |          2017-05-01 |               |  Regulation (derived from)  |          National Standard Notice No.1716 of 2016 |               |  Issuing agency(ies)  |          General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China |         
  GB/T 33068-2016: Test method of physical properties for sulfur exhaust hydrogenation catalyst---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.  
Test method of physical properties for sulfur exhaust hydrogenation catalyst
ICS 71.100.99
G74
National Standards of People's Republic of China
Standard Test Method for Physical Properties of Sulfur Tail Gas Hydrogenation Catalysts
2016-10-13 released
2017-05-01 implementation
General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China
China National Standardization Management Committee released
Foreword
This standard is drafted in accordance with the rules given in GB/T 1.1-2009.
This standard is proposed by the China Petroleum and Chemical Industry Association.
This standard is under the jurisdiction of the National Chemical Standardization Technical Committee Chemical Catalyst Subcommittee (SAC/TC63/SC10).
The drafting unit of this standard. Nanhua Group Research Institute, Shandong Qilu Keli Chemical Industry Research Institute Co., Ltd., Shandong Xunda Chemical Group Co., Ltd.
Division, Zibo Luyuan Industrial Catalysts Co., Ltd.
The main drafters of this standard. Qiu Ailing, Cheng Yuchun, Hu Wenbin, Xu Donggang, Chen Yanhao.
Standard Test Method for Physical Properties of Sulfur Tail Gas Hydrogenation Catalysts
1 Scope
This standard specifies the bulk density of the sulfur tail gas hydrogenation catalyst, particle crush resistance, wear rate and specific surface area, pore volume, average
Method for determination of pore diameters.
This standard is suitable for the hydrogen sulfide acid gas as the raw material of the Claus sulfur recovery process, with cobalt oxide, molybdenum oxide as the main active component,
Catalyst for sulfur tail gas hydrogenation with alumina as carrier.
2 normative reference documents
The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article
Pieces. For undated references, the latest edition (including all modifications) applies to this document.
GB/T 6003.1 Test sieve technical requirements and testing - Part 1. Wire mesh test screen
General rules for sampling of chemical products GB/T
Determination of Crushedness of Particles in HG/T 2782 Fertilizer Catalysts
Determination of Wear Rate of Fertilizer Catalyst for HG/T
Determination of Bulk Density of HG/T 4680 Fertilizer Catalyst
Determination of bulk density
According to the provisions of HG/T 4680, where the test sample to be 120 ℃ temperature, drying 2h.
Determination of Radial Anti - crushing Force of 4 Particles
According to the provisions of HG/T 2782, which intelligent particle strength testing machine range of 0N ~ 500N, the number of particles measured 40 samples;
Long strip sample length processing is 2.5mm ~ 3.5mm.
5 Determination of wear rate
According to the provisions of HG/T 2976, which after grinding on the screen material at 120 ℃ under the conditions of drying 2h.
6 specific surface area, pore volume, average pore diameter
6.1 Principles
Particles placed in the gas, the surface (including the outer and internal through-hole surface) at a low temperature physical adsorption occurs. When the adsorption reaches flat
The equilibrium adsorption pressure and the amount of adsorbed gas are measured, and the saturated adsorption of the monomolecular layer is obtained from the adsorption isotherm according to the BET equation.
And the specific surface area of the sample is calculated. The pore diameter of the sample can be calculated from the desorption isotherm according to the Kelvin equation.
6.2 Instruments, equipment and materials
6.2.1 physical adsorption instrument. in the liquid nitrogen temperature, the nitrogen adsorption.
   
   
  
  
    
  
    
   
        
       
          
               
 
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