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GB 13458-2013 English PDF

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GB 13458-2013: Discharge standard of water pollutants for ammonia industry
Status: Valid

GB 13458: Evolution and historical versions

Standard ID	Contents [version]	USD	STEP2	[PDF] delivered in	Standard Title (Description)	Status	PDF
GB 13458-2013	English	229	Add to Cart	3 days [Need to translate]	Discharge standard of water pollutants for ammonia industry	Valid	GB 13458-2013
GB 13458-2001	English	199	Add to Cart	2 days [Need to translate]	Discharge standard of water pollutants for ammonia industry	Obsolete	GB 13458-2001
GB 13458-1992	English	439	Add to Cart	4 days [Need to translate]	Discharge standard of water pollutants for ammonia industry	Obsolete	GB 13458-1992

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Basic data

Standard ID	GB 13458-2013 (GB13458-2013)
Description (Translated English)	Discharge standard of water pollutants for ammonia industry
Sector / Industry	National Standard
Classification of Chinese Standard	Z60
Classification of International Standard	13.060.30
Word Count Estimation	10,11
Older Standard (superseded by this standard)	GB 13458-2001
Quoted Standard	GB/T 6920; GB/T 11893; GB/T 11901; GB/T 11914; GB/T 16489; GB/T 17133; HJ 484; HJ 502; HJ 503; HJ 535; HJ 536; HJ 537; HJ 636; HJ 637; HJ/T 60; HJ/T 195; HJ/T 199; HJ/T 200; HJ/T 399; " automatic monitoring pollution management approach" (State Environmen
Regulation (derived from)	Department of Environmental Protection Notice No. 15 of 2013; National Standards Bulletin 2013 No. 5
Issuing agency(ies)	Ministry of Environmental Protection, General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China
Summary	This standard specifies the ammonia industry enterprises or production facilities of water pollutant discharge limits, surveillance and monitoring requirements, and standards for the implementation and supervision of relevant regulations. This standard ap

GB 13458-2013: Discharge standard of water pollutants for ammonia industry

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Discharge standard of water pollutants for ammonia industry National Standards of People's Republic of China Replacing GB 13458-2001 Ammonia industrial water pollutant discharge standards (release draft) Issued on. 2013-03-14 2013-07-01 implementation Ministry of Environmental Protection State Administration of Quality Supervision, Inspection and Quarantine release

Preface .II 1 Scope 1 2 Normative references 1 3 Terms and definitions ..2 4 2 water pollutant emission control requirements 5 water pollutants monitoring requirements ..4 Implementation and monitoring .. 5 6

Foreword

To implement the "People's Republic of China Environmental Protection Law", "People's Republic of China Water Pollution Prevention Law," "People's Republic of China And the National Marine Environmental Protection Law "," State Council on Strengthening Key Environmental Protection Tasks "and other laws and regulations," State Homes for the preparation of the national main functional area planning advice "to protect the environment, prevent pollution and promote industrial ammonia production process And advances in pollution control technology, the development of this standard. This standard specifies the ammonia production process of industrial water pollutant discharge limits, and monitoring requirements. The standard emission concentrations of pollutants are mass concentration. National pollutant discharge ammonia emissions of industrial enterprises air pollutants (including odor pollutants), apply appropriate environmental noise Play standards, resulting in identification of solid waste treatment and disposal applicable national solid waste pollution control limits. This standard was first published in 1992 and revised in 2001 for the first time, this is the second revision. This revision of the main elements. - According to the implementation plan requires environmental management and enforcement of national environmental protection, adjusted for controlling emissions Pollutants projects to improve the pollutant emission control requirements; - Canceled by sewage whereabouts of hierarchical control provisions; - To promote the coordinated development of regional economy and the environment, promote the adjustment and transformation of economic growth mode of economic structure, lead Guide the direction of development of industrial ammonia production process and pollution control technologies, in particular the provisions of the water pollutant discharge limits; - To improve the national system of environmental standards, norms water pollution discharge, meet the national water pollution control work The need to increase the indirect water pollutant discharge limits. The date of implementation of this standard, "ammonia industrial water pollutant discharge standards" (GB 13458-2001) shall be repealed simultaneously. Local people's governments at the provincial level are not specified in this standard pollutants may establish their local emission standards; for This standard has been provided for projects of contaminants, may establish more stringent standards in this local emission standards. This standard is developed by the Ministry of Environmental Protection Science, Technology organization. This standard drafting units. China Environmental Science Research Institute. This standard MEP February 25, 2013 for approval. This standard from July 1, 2013 implementation. The standard explanation by the Ministry of Environmental Protection. Ammonia industrial water pollutant discharge standards

1 Scope

This standard specifies the ammonia production facilities of industrial enterprises or water pollutant discharge limits, monitoring and control requirements, as well as standard Registration and other relevant provisions of the implementation and supervision. This standard applies to existing industrial enterprises or ammonia production facilities of water pollutant emissions management. This standard applies to ammonia industry enterprises construction projects environmental impact assessment, environmental protection facilities design completion ring Acceptance of Environmental Protection water pollutant discharge management after putting into operation. This standard does not apply to management of discharge of water pollutants nitrate, fertilizer and associated alkaline soda production. This standard applies to water pollution discharge permitted by law. Sources within the newly established location and special protected areas now There are sources of management, according to "People's Republic of China Water Pollution Prevention Law," "People's Republic of China Marine Environmental Protection Law" Relevant provisions of the "People's Republic of China Environmental Impact Assessment Law" and other laws implemented. Water pollutant emission control requirements of this standard apply to companies directly or indirectly to discharge its statutory outer boundary water pollution Dyeing behavior thereof.

2 Normative references

The standard content of the following documents cited in the articles. For undated references, the effective version applies to this standard. Determination of the glass electrode method GB/T 6920 Water Quality pH value Determination of GB/T 11893 of total phosphorus - Ammonium molybdate spectrophotometric method Determination of GB/T 11901 Quality of suspended solids - Gravimetric method Determination of GB/T 11914 Quality Chemical Oxygen Demand dichromate method By infrared spectrophotometry GB/T 16488 quality oil and animal and vegetable oils GB/T 16489 Water quality Determination of sulfide - Methylene blue spectrophotometric method Determination of GB/T 17133 Quality sulfide direct color spectrophotometry Determination of cyanide HJ 484 Water capacity and spectrophotometric methods HJ 502 Water quality - Determination of volatile phenol bromine method HJ 503 Water quality - Determination of volatile phenol 4-amino-antipyrine spectrophotometric method HJ 535 Water quality - Determination of ammonia Nessler reagent spectrophotometric HJ 536 Water quality - Determination of ammonia acid spectrophotometric method HJ 537 Water quality - Determination of ammonia distilled - and titration HJ 636 Water quality Determination of total nitrogen - Alkaline potassium persulfate digestion - UV spectrophotometric method Determination of HJ/T 60 quality sulfides Iodimetry HJ/T 195 Water quality - Determination of ammonia gas phase molecular absorption spectrometry HJ/T 199 Determination of Water Quality Total Nitrogen gas phase molecular absorption spectrometry Determination of HJ/T 200 Water sulfide gas phase molecular absorption spectrometry Determination of HJ/T 399 Water quality COD rapid digestion spectrophotometry "Pollution automatic monitoring and management approach" (SEPA Order No. 28) "Environmental Monitoring Management Measures" (SEPA Order No. 39)

3 Terms and Definitions

The following terms and definitions apply to this standard. 3.1 Ammonia Industry Ammonia industry, including the production of ammonia and urea to ammonia as raw material, ammonium nitrate, ammonium bicarbonate and ammonia alcohol Heat and power production enterprises or production facilities. 3.2 Existing Enterprise It means before implementation of this standard has been put into operation or environmental impact assessment document has been approved ammonia industrial enterprises Or production facilities. 3.3 new enterprises Refers to the date of implementation of this standard, EIA documents approved new construction, renovation and expansion of industrial ammonia Production facilities construction projects. 3.4 displacement It refers to the amount of business to business or production facilities outside the legal boundaries of wastewater discharge, including direct or indirect relationship with the production Various efflux wastewater (including sewage plant, cooling water, boiler plant and power plant drainage). 3.5 reference displacement per unit of product Refers to wastewater emissions for approved prescribed concentration of water pollutant discharge per ton of ammonia production limits. Note. alcohol ammonia generation companies need to be translated into the production of alcohol after ammonia production unit together with the approved product and the reference displacement. 3.6 Direct Emissions It refers to the emission units discharged directly to the environment of water pollutants behavior. 3.7 Indirect Emissions Sewage discharge unit refers to a public sewage system water pollutants behavior. 3.8 public sewage system Refers to the collection of wastewater pollutant by pipelines, etc., provide drainage and wastewater services can provide more than two sewage units Meet the relevant emission standards required by enterprises or institutions, including all sizes and types of urban sewage treatment plants, regional (including Various industrial parks, development zones and industrial gathering, etc.) waste water treatment plants, waste water treatment level it should reach two or secondary the above.

4 water pollutant emission control requirements

4.1 is from July 1, 2014 until December 31, 2015, the implementation of existing enterprises specified in Table 1 water pollutant discharge limits. Table 1 water pollutant discharge of existing business units and product concentration limits reference displacement Unit. mg/L (except pH) Item No. pollutants Limit Emissions monitoring location Direct emissions indirect emissions 1 pH value 6 ~ 96 ~ 9 companies total wastewater outfall 2 suspension 60100 3 Chemical oxygen demand (CODCr) 100 200 Ammonia 40 50 4 5 TN 50 60 TP 6 1.0 1.5 7 0.2 0.2 Cyanide Volatile Phenol 0.1 0.1 8 Sulfide 0.5 0.5 9 10 Petroleum 55 Unit product reference displacement (m3/t ammonia) 101) displacement measuring position and pollutants Same emission monitoring position 302) Note. 1) a single set of equipment with an annual output of synthetic ammonia ≥30 tons; 2) a single set of equipment with an annual output of synthetic ammonia < 30 tons. 4.2 Since January 1, 2016, the implementation of existing enterprises specified in Table 2 of water pollutant discharge limits. 4.3 Since July 1, 2013, implementation of new enterprises specified in Table 2 of water pollutant discharge limits. Table 2 New business concentration limits and water pollutant discharge per unit of product reference displacement Unit. mg/L (except pH) Item No. pollutants Limit Emissions monitoring location Direct emissions indirect emissions 1 pH value of 6 ~ 96 ~ 9 Enterprise total wastewater outfall 2 suspension 50100 3 Chemical oxygen demand (CODCr) 80 200 Ammonia 25 50 4 5 TN 3560 TP 6 0.5 1.5 7 0.2 0.2 Cyanide Volatile Phenol 0.1 0.1 8 Sulfide 0.5 0.5 9 10 Petroleum 33 Unit product reference displacement (m3/t ammonia) 10 Displacement measuring position and pollutants Emissions Monitoring same location 4.4 According to the requirements of environmental protection work in the already high density land development, environmental carrying capacity began to weaken, or the environment Smaller capacity, the ecological environment is fragile, prone to serious environmental pollution problems need to take special measures to protect areas should Strictly control the emissions behavior of enterprises, enterprises in these areas to perform specified in Table 3 of water pollutant discharge limit special value. Implementation of water pollutant discharge limits in particular geographical scope, timing, environmental protection administrative department of the State Council or provincial People's Government. Table 3 water pollutant discharge limits Special Unit. mg/L (except pH) Item No. pollutants Limit Emissions monitoring location Direct emissions indirect emissions 1 pH value of 6 ~ 96 ~ 9 Enterprise total wastewater outfall 2 suspension 3050 3 Chemical oxygen demand (CODCr) 50 80 Ammonia 15 25 4 5 TN 25 35 TP 6 0.5 0.5 7 0.2 0.2 Cyanide Volatile Phenol 0.1 0.1 8 Sulfide 0.5 0.5 9 10 Petroleum 33 Unit product reference displacement (m3/t ammonia) 10 Displacement measuring position and pollutants Emissions Monitoring same location 4.5 water pollutant discharge concentration limits for the unit displacement of not more than the actual product Unit product reference displacement. If the actual displacement per unit of product per unit of product than the reference displacement, shall formula (1) will be measured in terms of the concentration of water pollutants Displacement of water pollutant emissions baseline concentration, and the concentration of water pollutant emissions as a baseline displacement of emissions is determined whether the target of in accordance with. Product yield and displacement statistical period is one day. In the company's production facilities produce two or more products, emission control requirements applicable to different countries or different industries pollution Most cases of sewage pollutants emission standards, and the production facilities to produce hybrid process emissions, emission standards should be implemented as specified in Strict concentration limits, according to the equation (1) the reference in terms of displacement of water pollutants emission concentration. Base = ρρ × • Σ ii Q (1) Where. Yl ρ - water pollutant discharge displacement of the reference concentration, mg/L; Total Q - drainage volume, m3; iY - a product yield, t; Yl iQ - a product of the reference product unit displacement, m3/t; Real ρ - measured water pollutant discharge concentration, mg/L. Q and Σ • If the total group ii QY ratio less than 1, places the water measured concentrations of pollutants as a determination of whether the target emissions in accordance with.

5 water pollutants monitoring requirements

5.1 pairs of enterprises discharge waste water sampling, monitoring should be based on the type of contaminant, pollutant emission monitoring in a predetermined position, Waste water treatment facilities, reprocessing facilities should be monitored. In emissions monitoring location should be set permanently outfall signs. 5.2 New and existing business to install automatic monitoring equipment, emissions requirements according to the relevant laws and "source of pollution from Provisions dynamic monitoring and management approach "implementation. 5.3 pairs Pollutant emissions monitoring frequency, sampling time and other requirements, according to the national pollution monitoring technology Standardized regulations. 5.4 enterprise approved product yield, based on the statutory report. 5.5 Enterprise in accordance with relevant laws and regulations, "environmental monitoring management approach", the sewage to monitor the situation and keep the original Start monitoring records. Determination of 5.6 pairs of enterprises discharge of water pollutants concentrations using standard methods listed in Table 4. Table 4 Water pollutant concentration measurement method standard Item No. Pollutant Method Standard Method Standard No. Title Method 1 pH glass electrode measuring the value of the water quality of pH GB/T 6920 2 Determination of suspended solids by weight aqueous suspension composition method GB/T 11901 3 COD Water quality - Determination of the chemical oxygen demand dichromate method GB/T 11914 Water quality - Determination of the chemical oxygen demand rapid digestion spectrophotometric method HJ/T 399

4 ammonia

Water quality - Determination of ammonia Nessler reagent spectrophotometric method HJ 535 Water quality - Determination of ammonia acid spectrophotometric method HJ 536 Water quality - Determination of ammonia distilled - and titration HJ 537 Water quality - Determination of ammonia gas phase molecular absorption spectrometry HJ/T 195 5 TN Water quality Determination of total nitrogen - Alkaline potassium persulfate digestion - UV spectrophotometric method HJ 636 Determination of Water Quality Total Nitrogen gas phase molecular absorption spectrometry HJ/T 199 TP 6 Determination of total phosphorus - Ammonium molybdate spectrophotometric method GB/T 11893 7 Determination of cyanide cyanide quality volumetric method and spectrophotometry HJ 484

8 volatile phenol

Water quality - Determination of volatile phenol bromine method HJ 502 Water quality - Determination of volatile phenol 4-amino-antipyrine spectrophotometric method HJ 503

9 sulfides

Water quality - Determination of sulfide Methylene blue spectrophotometric method GB/T 16489 Water quality - Determination of sulfide - Direct development of the spectrophotometry GB/T 17133 Water quality - Determination of sulfide Iodimetry HJ/T 60 Water quality-Determination of sulfide gas phase molecular absorption spectrometry HJ/T 200 Grade 10 by infrared petroleum oil, animal and vegetable oils spectrophotometry GB/T 16488

6 Implementation and Supervision

6.1 standard by the people's governments above the county level environmental protection administrative department responsible for overseeing implementation. 6.2 In any case, the enterprise shall comply with the requirements of this standard pollutant emission control requirements, take the necessary measures to ensure that pollution Transfected control facilities running. Environmental protection departments at all levels in the enterprise when the supervisory inspection, sampling or monitoring can spot instantly The result, as the determination of sewage behavior meets the emissions standards and the implementation of environmental management measures related basis. The hair Enterprise is the case or water displacement abnormal changes should be approved enterprise actual product yield and displacement, according to the standard Regulations, terms of reference displacement of water pollutant discharge concentration.

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