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SN/T 4691-2016: Determination of ethylenimine in wood and wood products - Gas chromatography
Status: Valid
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| SN/T 4691-2016 | English | 139 |
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Determination of ethylenimine in wood and wood products - Gas chromatography
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SN/T 4691-2016
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PDF similar to SN/T 4691-2016
Basic data | Standard ID | SN/T 4691-2016 (SN/T4691-2016) | | Description (Translated English) | Determination of ethylenimine in wood and wood products - Gas chromatography | | Sector / Industry | Commodity Inspection Standard (Recommended) | | Classification of Chinese Standard | B69 | | Word Count Estimation | 6,613 | | Date of Issue | 2016-12-12 | | Date of Implementation | 2017-07-01 | | Regulation (derived from) | State-Quality-Inspection-Accredidation (2016) No.590 | | Issuing agency(ies) | General Administration of Customs | SN/T 4691-2016: Determination of ethylenimine in wood and wood products - Gas chromatography---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of ethylenimine in wood and wood products-Gas chromatography
People's Republic of China Exit Inspection and Quarantine standards
Determination of aziridine in wood and its products
Gas chromatography
2016-12-12 released
2017-07-01 implementation
People's Republic of China
General Administration of Quality Supervision, Inspection and Quarantine released
Exit Inspection and Quarantine of People's Republic of China
Industry Standard
Determination of aziridine in wood and its products
Gas chromatography
China Standard Press
First edition of November.2017
Foreword
This standard was drafted in accordance with the rules given in GB/T 1.1-2009.
Please note that some of this document may be patentable. The issuing agencies of this document do not bear the responsibility of identifying these patents.
This standard is proposed and managed by the National Certification and Accreditation Administration Committee.
This standard was drafted by Shenzhen Inspection and Quarantine Academy, Shenzhen Entry-Exit Inspection and Quarantine Bureau, People's Republic of China.
The main drafters of this standard. Gu Hao Fei, Li Yongtao, Zhou Junhui, Yang Zuojun, Liu Yi, Long Bin, Wang Chengyun.
Determination of aziridine in wood and its products
Gas chromatography
Warning --- personnel using this standard should have the formal laboratory work experience. This standard does not indicate all possible safety issues
question. It is the user's responsibility to take appropriate safety and health measures and to ensure compliance with the requirements of the relevant state laws and regulations.
1 Scope
This standard specifies the determination of aziridine content of wood and wood products by gas chromatography - flame ionization detector (GC-FID) determination.
This standard applies to the determination of aziridine content in wood and wood products.
2 principle
The sample was extracted by methanolic solvent and determined by Gas Chromatography (GC-FID) with flame ionization detector and quantified by external standard method.
3 Reagents and materials
3.1 methanol, CH3OH, chromatographic purity.
3.2 aziridine, C2H5N purity of not less than 99.5%.
3.3 aziridine standard stock solution, accurately weighed 100mg aziridine (3.2) in 50mL volumetric flask, dissolved with an appropriate volume of methanol,
The resulting solution concentration of.2000mg/L, placed in a refrigerator under the conditions of less than 4 ℃ sealed, valid for six months.
3.4 Helium, purity not less than 99.999%.
4 instruments and equipment
4.1 Gas Chromatograph with Hydrogen Flame Ionization Detector (FID).
4.2 Analytical balance, flu 0.1mg.
4.3 ultrasonic cleaner. Operating frequency 40kHz.
4.4 cutting mills or similar equipment.
4.5 micropipette, range 10μL ~ 100μL, accuracy of 0.1μL.
4.6 Teflon filter, 0.22μm.
5 Sample Preparation
For surfaces treated with wood (eg lacquered, veneer etc) or contaminated wood and wood products, the surface material should be removed
except. Using drilling, sawing, planing and other methods to prepare samples, samples should be split knot knot, decay and other parts of the wood defects. The preparation of the sample through the cut
Slitter or similar equipment (4.4) crushed, should avoid the high temperature and heat in the crushing process, made of powder diameter not more than 1mm crushed, mixed
Even, spare.
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