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JJF 1563-2016: Calibration Specification for Workstation of Chromatographic Data
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Calibration Specification for Workstation of Chromatographic Data
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JJF 1563-2016
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Basic data | Standard ID | JJF 1563-2016 (JJF1563-2016) | | Description (Translated English) | Calibration Specification for Workstation of Chromatographic Data | | Sector / Industry | Metrology & Measurement Industry Standard | | Classification of Chinese Standard | A61 | | Classification of International Standard | 17.020 | | Word Count Estimation | 18,162 | | Date of Issue | 2016-06-27 | | Date of Implementation | 2016-09-27 | | Quoted Standard | GB/T 25478-2010; ASTM E1657-1998 | | Adopted Standard | ASTM E1657-1998(2011), NEQ | | Regulation (derived from) | Notice of the General Administration of Quality Supervision, Inspection and Quarantine of the People Republic of China 2016 No.16 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine | | Summary | This standard applies to liquid chromatography, gas chromatography, ion chromatograph used in the analog interface of the calibration of the chromatographic data workstation. Other types of chromatographic data The calibration of the workstation can be done with reference to this standard. | JJF 1563-2016: Calibration Specification for Workstation of Chromatographic Data---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Calibration Specification for Workstation of Chromatographic Data
National Metrological Technical Code of the People's Republic of China
Standard for Calibration of Chromatographic Data Workstations
2016-06-27 released
2016-09-27 implementation
State Administration of Quality Supervision, Inspection and Quarantine issued
Standard for Calibration of Chromatographic Data Workstations
Responsible unit. National Physical and Chemical Metrology Technical Committee
The main drafting unit. China Institute of Metrology
Institute of Metrology and Measurement, Guangxi Zhuang Autonomous Region
Participated in the drafting unit. Xinjiang Uygur Autonomous Region Measurement and Testing Research Institute
Dalian Yili Te Analysis Instrument Co., Ltd.
This specification entrusts the National Physical Chemistry Metrology Technical Committee to explain
The main drafters of this specification.
Tao Hong (China Institute of Metrology)
Feng Keli (Institute of Metrology and Measurement, Guangxi Zhuang Autonomous Region)
Zhang qinghe (China Institute of Metrology)
Participate in the drafters.
Bai Xu (Xinjiang Uygur Autonomous Region Measurement and Testing Institute)
Yu Dexiu (Dalian Li Lite Analytical Instruments Co., Ltd.)
table of Contents
Introduction (II)
1 Scope (1)
2 References (1)
3 Overview (1)
4 Metering characteristics (1)
5 Calibration conditions (2)
5.1 Environmental conditions (2)
5.2 Measuring equipment (2)
6 Calibration items and calibration methods (2)
6.1 Sampling frequency (2)
6.2 Baseline noise and baseline drift (2)
6.3 Interval error and repeatability (3)
6.4 Voltage indication error and repeatability (3)
6.5 Dynamic Linearity (4)
6.6 Qualitative Repeatability and Quantitative Repeatability (4)
6.7 Quantitative error (4)
7 Calibration results (4)
8 Recurrence time interval (5)
Appendix A Chromatographic Signal Generators (6)
Appendix B Calibration records (for reference) (7)
Appendix C Calibration Certificate Inside Page Format (9)
Appendix D Examples of Measurement Uncertainty Evaluation (11)
Introduction
This specification is based on JJF 1001-2011 "General measurement terms and definitions", JJF 1071-2010 "National measurement
Calibration rules for the preparation of rules ", JJF 1059.1-2012" measurement uncertainty assessment and representation "as the basis and basis,
Reference GB/T 25478-2010 "Chromatographic Data Workstation", ASTME1657-98 (2011) "Liquid Chromatography
Quot; StandardPractice for Test & lt; RTI ID = 0.0 & gt; & lt;/RTI & gt;
PhotometricDetectorsUsedinLiquidChromatography).
This specification is the first release.
Standard for Calibration of Chromatographic Data Workstations
1 Scope
This specification applies to the chromatographic data of the analog interface used in liquid chromatography, gas chromatograph, ion chromatograph
Station calibration. Other types of chromatographic data The calibration of the workstation can be done with reference to this specification.
2 reference file
This specification refers to the following documents.
Chromatographic Data Workstation
Standard Test Method for Variable Wavelength Photometric Detectors for Liquid Chromatography (Standard
PracticeforTestingVariable-WavelengthPhotometricDetectorsUsedinLiquidChroma-
tography
For dated references, only the dated edition applies to this specification; references that are not dated
, The latest version (including all modifications) applies to this specification.
3 Overview
The chromatographic data workstation consists of a computer, one or more data collectors and colors that convert analog signals into digital
Spectrum data processing software, is able to complete the chromatograph signal conversion, data acquisition, analysis, storage and other functions
Complete system.
4 measurement characteristics
Chromatographic data station measurement of the technical indicators in Table 1.
Table 1 Chromatographic data workstation main technical indicators
Terms and Conditions Technical Specifications
4.1 sampling frequency ≥ 20Hz
4.2 Baseline noise ≤ 6μV
4.3 Baseline drift ≤50μV/h
4.4 Maximum permissible error of time interval ± 0.6s
4.5 time interval repeatability ≤ 1s
4.6 Voltage indication maximum allowable error ± 1%
4.7 voltage indication repeatability ≤ 0.01%
4.8 Dynamic linear linear correlation coefficient r≥0.9998
4.9 Qualitative Repetitive RSD Retention Time ≤0.3%
4.10 Quantitative repeatability RSD peak height ≤ 0.3%, RSD peak area ≤ 0.3%
4.11 Quantitative maximum allowable error ± 0.5%
Note. The technical indicators are not used for qualified judgment, for reference only.
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