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GB/T 37196-2018: Plastics -- Polyether polyols/polymeric polyols -- Determination of aldehydes and ketones
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Plastics -- Polyether polyols/polymeric polyols -- Determination of aldehydes and ketones
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GB/T 37196-2018
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Basic data | Standard ID | GB/T 37196-2018 (GB/T37196-2018) | | Description (Translated English) | Plastics -- Polyether polyols/polymeric polyols -- Determination of aldehydes and ketones | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | G31 | | Classification of International Standard | 83.040 | | Word Count Estimation | 10,134 | | Date of Issue | 2018-12-28 | | Date of Implementation | 2019-11-01 | | Issuing agency(ies) | State Administration for Market Regulation, China National Standardization Administration | GB/T 37196-2018: Plastics -- Polyether polyols/polymeric polyols -- Determination of aldehydes and ketones
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Plastics--Polyether polyols/polymeric polyols--Determination of aldehydes and ketones
ICS 83.040
G31
National Standards of People's Republic of China
Plastic polyether polyol/polymer polyol
Determination of aldehyde and ketone content
Published on.2018-12-28
2019-11-01 implementation
State market supervision and administration
China National Standardization Administration issued
Foreword
This standard was drafted in accordance with the rules given in GB/T 1.1-2009.
This standard was proposed by the China Petroleum and Chemical Industry Federation.
This standard is under the jurisdiction of the National Plastics Standardization Technical Committee (SAC/TC15).
This standard is mainly drafted by. Sinopec Shanghai Gaoqiao Petrochemical Co., Ltd., Changhua Chemical Technology Co., Ltd., Shandong Blue
Xingdongda Co., Ltd., Jiangsu Zhongshan Chemical Co., Ltd., Wanhua Chemical Group Co., Ltd., Shandong Yinuowei New Materials Co., Ltd., Li
Ming Chemical Research and Design Institute Co., Ltd.
The main drafters of this standard. Lu Yi, Chen Fengqiu, Kong Wei, Wu Yaqing, Yan Luhai, Xu Yidong, Liu Genlan, Cheng Ying, Zhang Li, Shi Shuhui.
Plastic polyether polyol/polymer polyol
Determination of aldehyde and ketone content
Caution - Personnel using this standard should have practical experience in formal laboratory work. This standard does not address any safety related to use.
Full question. It is the responsibility of the user to take appropriate safety and health measures and to ensure compliance with the conditions set by the relevant national regulations.
1 Scope
This standard specifies the determination of aldehyde and ketone content in polyether polyols or polymer polyols by high performance liquid chromatography.
This standard applies to the determination of formaldehyde, acetaldehyde, acrolein and acetone in polyether polyols or polymer polyols, other carbonyl containing
The content of the compound can be determined by reference to this standard.
2 Normative references
The following documents are indispensable for the application of this document. For dated references, only dated versions apply to this article.
Pieces. For undated references, the latest edition (including all amendments) applies to this document.
GB/T 6682 Analytical laboratory water specifications and test methods
3 Terms and definitions
The following terms and definitions apply to this document.
3.1
Derivative derivatization
The target compound which is difficult to detect in the sample is quantitatively converted into a compound which is easy to detect by a chemical reaction, and the latter can be detected by the latter.
Qualitative and/or quantitative analysis of the target compound.
3.2
Purine derivatives hydrazonederivatives
The carbonyl-containing compound component reacts with 2,4-dinitrophenylhydrazine (hereinafter referred to as DNPH) under the action of a strong acid to form a stable
Compound.
4 Method summary
The carbonyl-containing compound component of the sample reacts with DNPH under strong acid to form a stable colored quinone derivative, which is highly efficient.
Determination of anthraquinone derivatives by liquid chromatography, using retention time characterization and peak area quantification to obtain the aldehyde/ketone substance content in the sample
The chemical reaction equation is as follows.
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