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GB/T 30773-2014 English PDF

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GB/T 30773-2014: Determination of residual phenol content in phenolic resins by gas chromatography
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PDF similar to GB/T 30773-2014


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Basic data

Standard ID GB/T 30773-2014 (GB/T30773-2014)
Description (Translated English) Determination of residual phenol content in phenolic resins by gas chromatography
Sector / Industry National Standard (Recommended)
Classification of Chinese Standard G31
Classification of International Standard 83.080.01
Word Count Estimation 13,186
Date of Issue 7/8/2014
Date of Implementation 12/1/2014
Quoted Standard ISO 1042-1998; ISO 6353-2-1983; ISO 10082-1999
Adopted Standard ISO 8974-2002, MOD
Regulation (derived from) 2014 National Standards Bulletin No. 18
Issuing agency(ies) General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary This Standard specifies the phenolic resin free phenol content by gas chromatography test two methods. This Standard applies to the determination of free phenol content of phenolic resin.

GB/T 30773-2014: Determination of residual phenol content in phenolic resins by gas chromatography


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Determination of residual phenol content in phenolic resins by gas chromatography ICS 83.080.01 G31 National Standards of People's Republic of China Determination of the content of free phenol in phenolic resin by gas chromatography (ISO 8974.2002, Plastics-Phenolicresins- Determinationofresidualphenolcontentbygaschromatography, MOD) Issued on. 2014-07-08 2014-12-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released

Foreword

This standard was drafted in accordance with GB/T 1.1-2009 given rules. This standard uses redrafted law revision using ISO 8974.2002 Determination of free phenol containing "plastic phenolic resin by gas chromatography the amount". This standard and ISO 8974.2002 technical differences and their reasons are as follows. --- Chapter 1 "Scope" Add "This standard applies to phenolic resin of free phenol content determination" to increase the standard of the applicable limit, Fu Write requirements set standards; --- Increasing the internal standard mass m 'in the formula, the international standard was originally written in the "quality of the internal standard to calculate the concentration of the liquid storage and To "in order to more clearly increases the concentration is calculated from the conversion quality; --- Chapter 9 of the precision in Appendix C, said chapter accordingly explanation for failing to obtain laboratory data, it will be international Standard precision choreography in an appendix. This standard also made the following editorial changes. --- Change the standard name is "the determination of free phenol content of phenolic resin by gas chromatography", in line with existing standards; --- Chapter 2, "Normative references", according to GB/T 1.1-2009 requirements, adjust normative language reference guide. The standard proposed by China Petroleum and Chemical Industry Association. This standard by the National Standardization Technical Committee plastic thermosetting plastics Club (SAC/TC15/SC11) centralized. This standard is drafted by. Shandong Shengquan Chemical Corporation. Participated in the drafting of this standard. Country synthetic resin Quality Supervision and Inspection Center, Shanghai European-Asian Synthetic Material Co., Ltd, Changshu Southeast Plastic Expected Ltd. Shaxian Hongsheng Plastic Co., Ltd., Wuxi Chong Electronics Co., Ltd. The main drafters of this standard. Tang Lulin, Chen Ling, Zhao Ping, Chen Zeling, Zhu Chunyu, Chen Jiwei, Wengen yuan, Li Dong flower, Yin Quan. Determination of the content of free phenol in phenolic resin by gas chromatography

1 Scope

This standard specifies the phenolic resin of free phenol content by gas chromatography two test methods. This standard applies to the determination of free phenol content of phenolic resin.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document. ISO 1042.1998 laboratory glassware with a single scale flask (Laboratorygiassware-One-markvolumetric flasks) ISO 6353-2. 1983 Reagents for chemical analysis - Part 2. Specification of the first series (Reagentsforchemicalanalysis- Part 2. Specifications-Firstseries) ISO 10082.1999 Plastics - Phenolic resins classification and test methods (Plastics-Phenolicresins-Classification andtestmethods) Principle 3 The sample is dissolved in a suitable solvent, with a test of free phenol content by gas chromatography.

4 Terms and Definitions

ISO 10082.1999 as defined in the following terms and definitions apply to this document. 4.1 Internal standard internalstandard In response factor test and phenol test solution was added to a known amount of reference material. 4.2 Mass ratio massratio The ratio of phenol and internal standard quality test solution. 4.3 Peak area ratio peakarearatio Phenol peak areas to an internal standard peak area ratios. Note. The chromatogram peak area refers phenol phenol area between the peaks and the baseline surrounded. It refers to the internal standard peak area between the internal standard peak and surrounded the baseline area. 4.4 Response factor responsefactor The ratio of phenol in response to an internal standard response. K = Mass ratio Peak area ratio

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