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GB/T 20771-2008: Determination of 486 pesticides and related chemicals residues in honey -- LC-MS-MS method
Status: Valid GB/T 20771: Evolution and historical versions
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB/T 20771-2008 | English | 1809 |
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Determination of 486 pesticides and related chemicals residues in honey -- LC-MS-MS method
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GB/T 20771-2008
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| GB/T 20771-2006 | English | RFQ |
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Honey, fruit juice and wine 420 kinds of pesticides and related chemicals residues in liquid chromatography -- Tandem mass spectrometry
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GB/T 20771-2006
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Basic data | Standard ID | GB/T 20771-2008 (GB/T20771-2008) | | Description (Translated English) | Determination of 486 pesticides and related chemicals residues in honey -- LC-MS-MS method | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | X04 | | Classification of International Standard | 67.050 | | Word Count Estimation | 82,850 | | Date of Issue | 2008-12-31 | | Date of Implementation | 2009-05-01 | | Older Standard (superseded by this standard) | GB/T 20771-2006 | | Quoted Standard | GB/T 6379.1; GB/T 6379.2; GB/T 6682 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the acacia honey, Rape honey, linden tree honey, buckwheat honey, Date Honey 486 pesticides and related chemicals residues in liquid chromatography-tandem mass spectrometry. This standard applies to acacia honey, Rape honey, linden tree honey, buckwheat honey, qualitative identification Date Honey 486 pesticides and related chemicals residues, but also for the quantitative determination of 461 kinds of pesticides and related chemicals residues. 461 kinds of pesticides quantitative determination of the criteria and related chemicals detection limit of 0. 01 ��g/kg ~ 3. 34 mg/kg. | GB/T 20771-2008: Determination of 486 pesticides and related chemicals residues in honey -- LC-MS-MS method
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Determination of 486 pesticides and related chemicals residues in honey-LC-MS-MS method
ICS 67.050
X04
National Standards of People's Republic of China
Partially replace GB/T 20771-2006
Honey 486 pesticides and related chemicals
Determination of residues of liquid chromatography - tandem mass spectrometry
Posted 2008-12-31
2009-05-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Table of Contents
Preface Ⅰ
1 Scope 1
2 Normative references 1
3 Principle 1
4 Reagents and materials 1
5 Apparatus 2
6 Sample Preparation and Storage 2
7 measuring step 2
8 result of the calculation 5
9 Precision 6
Appendix A (informative) 486 kinds of pesticides and related chemicals English name, the detection limit, grouping, solvent selection and mixing
Standard concentration Table 7
Annex B (informative) 486 kinds of pesticides and related chemicals monitoring ion pair, air collision energy, and a retention time of voltage to cluster 22
Annex C (informative) 486 kinds of pesticides and related chemicals in multiple reaction monitoring (MRM) chromatogram 38
Annex D (informative) 486 kinds of pesticides and related chemicals precision data table 56
Appendix E (normative) 486 kinds of pesticides and related chemicals English name Chinese control index (in alphabetical order) 71
Foreword
The partial replacement of standard GB/T 20771-2006 "honey, fruit juice and wine in 420 kinds of pesticide residues determination by liquid chromatography -
Tandem mass spectrometry. "
This standard compared with GB/T 20771-2006, the main changes are as follows.
--- The determination of honey is separated from the GB/T 20771-2006 out, revision of this standard, and to redefine the standard
name;
--- Pesticides can be measured by the 420 kinds to 486 kinds, an increase of negative ESI and APCI source of positive and negative test for the presence of pesticide varieties;
--- Optimized pretreatment methods and increasing the negative ESI and APCI source source of positive and negative test conditions.
The Standard Appendix A, Appendix B, Appendix C, Appendix D, Appendix E is an information appendix.
This standard is proposed and managed by the State Administration of Quality Supervision Inspection and Quarantine of People's Republic of China.
This standard was drafted. People's Republic of China Qinhuangdao Exit Inspection and Quarantine, Shandong Agricultural University, Hebei University.
The main drafters of this standard. Pang Guofang, Li Yan, Individual Students Lian Jing, Zhao Shujun, ZHENG Hong, Liu Yongming, Caoyan Zhong, Zhang Jinjie,
Li Xuemin.
This standard was first published in 2006.
Honey 486 pesticides and related chemicals
Determination of residues of liquid chromatography - tandem mass spectrometry
1 Scope
This standard specifies the acacia honey, rape honey, linden tree honey, buckwheat honey, Date Honey 486 pesticides and related chemicals (see Appendix A and
Appendix E) residual amount of liquid chromatography - tandem mass spectrometry.
This standard applies to acacia honey, rape honey, linden tree honey, buckwheat honey, Date Honey 486 pesticides and related chemicals residues qualitative Kam
Do not also suitable for the quantitative determination of 461 kinds of pesticides and related chemicals residues.
461 kinds of pesticides and related chemicals quantitative determination of the standard method detection limit was 0.01μg/kg ~ 3.34mg/kg (see attached
Record A).
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
GB/T 6379.1 measurement methods and results of Accuracy (trueness and precision) - Part 1. General principles and definitions
(GB/T 6379.1-2004, ISO 5725-1.1994, IDT)
GB/T 6379.2 measurement methods and results of Accuracy (trueness and precision) - Part 2. Determine the standard measurement method to repeat
Of the basic methods of reproduction (GB/T 6379.2-2004, ISO 5725-2.1994, IDT)
GB/T 6682 analytical laboratory use specifications and test methods (GB/T 6682-2008, ISO 3696. 1987, MOD)
Principle 3
The sample was extracted with dichloromethane, the solid-phase extraction (SPE) eluting pesticides and related chemicals, liquid chromatography with acetonitrile and toluene (3 + 1) -
Tandem mass spectrometer detection, external standard.
4 Reagents and materials
Water as a water GB/T 6682 regulations.
4.1 acetonitrile. chromatography.
4.2 acetone. chromatography.
4.3 Toluene. pure class distinctions.
4.4 isooctane. chromatography.
4.5 hexane. chromatographically pure.
4.6 Methanol. chromatographically pure.
4.7 dichloromethane. chromatography.
4.8 microfiltration membrane (nylon). 13mm × 0.2μm.
4.9 Sep-Pak Amino-SPE. 1g, 6mL or equivalent person.
4.10 0.05% formic acid solution (volume fraction).
4.11 5mmol/L ammonium acetate solution. Weigh 0.375g ammonium acetate diluted with water to 1000mL.
4.12 acetonitrile and toluene (3 + 1, volume ratio).
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