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GB/T 18116.2-2008: Chemical analysis methods of Yttrium-europium oxides -- Determination of europium oxides
Status: Valid GB/T 18116.2: Evolution and historical versions
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| GB/T 18116.2-2008 | English | 189 |
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Chemical analysis methods of Yttrium-europium oxides -- Determination of europium oxides
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GB/T 18116.2-2008
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| GB/T 18116.2-2000 | English | 199 |
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Yttrium-europium oxide-Determination of europium oxide content-Inductively coupled plasma atomic emission spectrographic method
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GB/T 18116.2-2000
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PDF similar to GB/T 18116.2-2008
Basic data | Standard ID | GB/T 18116.2-2008 (GB/T18116.2-2008) | | Description (Translated English) | Chemical analysis methods of Yttrium-europium oxides -- Determination of europium oxides | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | H14 | | Classification of International Standard | 77.120.99 | | Word Count Estimation | 8,816 | | Date of Issue | 2008-03-31 | | Date of Implementation | 2008-09-01 | | Older Standard (superseded by this standard) | GB/T 18116.2-2000; GB/T 18116.3-2000 | | Regulation (derived from) | National Standard Approval Announcement 2008 No.5 (Total No.118) | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the determination of yttrium oxide and europium europium oxide content. This method is applicable to the determination of the amount of europium oxide of yttrium oxide and europium. Measuring range (mass fraction): 2. 00 %-8. 00%. | GB/T 18116.2-2008: Chemical analysis methods of Yttrium-europium oxides -- Determination of europium oxides
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Chemical analysis methods of Yttrium-europium oxides. Determination of europium oxides
ICS 77.120.99
H14
National Standards of People's Republic of China
Replacing GB/T 18116.2-2000, GB/T 18116.3-2000
Methods for chemical analysis of yttrium oxide
Determination of the amount of europium oxide
Posted 2008-03-31
2008-09-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
This standard is divided into two parts. Part 1 GB/T 18116.1-2000 "yttrium oxide chemical analysis by Inductively Coupled Plasma
Atomic emission spectrometry yttrium oxide lanthanum oxide, cerium oxide, praseodymium oxide, neodymium oxide, samarium oxide, gadolinium oxide, terbium oxide, dysprosium oxide
Holmium oxide, erbium oxide, thulium oxide, ytterbium and lutetium oxide amount "; Part 2 GB/T 18116.2-2008" Methods for chemical analysis of yttrium oxide
Determination of europium oxide content. "
This is Part 2. This part is GB/T 18116.2-2000 "yttrium oxide chemical inductively coupled plasma optical
Yttrium oxide and europium oxide europium "and GB/T 18116.3-2000" spectrophotometric determination of yttria yttrium oxide spectroscopy measurement fluorescence chemical methods
Europium europium oxide, "the integration of amendments to this part of the GB/T 18116.2-2000, the main changes compared to the GB/T 18116.3-2000
as follows.
--- Increasing the precision (repeatability) terms;
--- Expands the measurement range of the method;
--- Standard norms of writing text.
When analyzing the scope of the two methods overlap parts to Tier 1 as a method of arbitration.
This part is proposed by the National Development and Reform Commission, Office of Rare Earth.
This part of the National Standardization Technical Committee under the jurisdiction of rare earths.
This part 1 by the Shanghai Yuelong New Materials Co., Ltd. is responsible for drafting.
Method 1 of this section by the Jiangyin Jiahua Advanced Material Resources Co., Ltd Ganzhou Nonferrous Metallurgy Research Institute participated in the drafting.
The main drafters of this Part 1. Zhang Fei, Zhao Feng, Jin Jie, Shubing Yan.
Method 1 of this section participate drafters. Zhao Ping Hung, Ni Juhua, Wangshou Hong, Liu Hong, Zhong Daoguo.
Method 2 of this section by the Jiangyin Jiahua Advanced Material Resources Co., Ltd. is responsible for drafting.
Method 2 of this section by the Shanghai Yuelong New Materials Co., Ltd., Ganzhou Nonferrous Metallurgy Research Institute participated in the drafting.
The main drafters of this section Method 2. Yaojing Bi, Liu Wenhua.
Method 2 of this section participate drafters. Zhang Fei, Jin Jie, Yang Feng, Pan Jianzhong.
This part of the standard replaces the previous editions are.
--- GB/T 18116.2-2000;
--- GB/T 18116.3-2000.
Methods for chemical analysis of yttrium oxide
Determination of the amount of europium oxide
Inductively coupled plasma spectrometry (method 1)
1 Scope
This method specifies the method for determination of yttrium oxide and europium europium oxide content.
This method is applicable to the determination of the amount of europium oxide, yttrium oxide and europium. Measurement range (mass fraction). 2.00% - 8.00%.
2 principle of the method
Samples with hydrochloric acid dissolved in dilute hydrochloric acid medium, direct excitation of argon plasma light source, subjected to spectral measurement, with the correction matrix matching method
Effect of matrix on the determination.
3 Reagents
3.1 hydrochloric acid (1 + 1), pure class distinctions.
3.2 hydrochloric acid (1 + 19), pure class distinctions.
3.3 Argon ((mass fraction) > 99.99%).
3.4 yttrium oxide stock solution. Weigh 0.1000g 1h at 900 ℃ burning yttrium oxide (REO (mass fraction) > 99.9%, Y2O3/REO
(Mass fraction) > 99.99%), placed in 100mL beaker, add 10mL of hydrochloric acid (1 + 1), low temperature dissolved and transferred to 100mL volumetric flask
Diluted with water to volume, and mix. 1mL solution containing 1mg yttrium oxide.
3.5 europium oxide stock solution. Weigh 0.1000g 1h at 900 ℃ burning of europium oxide (REO (mass fraction) > 99.9%, Eu2O3 /
REO (mass fraction) > 99.99%), placed in 100mL beaker, add 10mL of hydrochloric acid (1 + 1), low temperature dissolved and transferred to 100mL
Volumetric flask, dilute with water to volume, and mix. 1mL solution containing 1mg europium oxide. This solution was then washed with hydrochloric acid (3.2) diluted to
1mL containing 0.1mg standard solution of europium oxide.
4 Instrument
4.1 Inductively coupled plasma spectrometer with a resolution of < 0.006nm (200nm office).
4.2 source. argon plasma light source.
5 Sample
The sample was calcined at 900 ℃ 1h, placed in a desiccator, cooled to room temperature, and immediately weighed.
Step 6 Analysis
6.1 Preparation of test solution analysis
6.1.1 Accurately weigh 0.1000g sample (5) in 50mL beaker, moistened with water, was added 10mL of hydrochloric acid (3.1), and dissolved at a low temperature
Cooled to room temperature and transferred to 100mL volumetric flask, dilute with water to volume, and mix.
6.1.2 Pipette 10.00mL test solution (6.1.1) added 9mL hydrochloric acid (3.1) in 100mL volumetric flask, dilute with water to volume, and mix.
Tested.
6.2 preparation of standard solution
The rare earth oxide stock solution (3.4 to 3.5) in Table 1 were transferred to 100mL volumetric flask (3.2) diluted to the mark with hydrochloric acid
Degree of mixing, to prepare the standard solution.
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