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GB 1886.201-2016: National Food Safety Standard -- Food Additives -- Benzyl acetate
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| GB 1886.201-2016 | English | 109 |
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National Food Safety Standard -- Food Additives -- Benzyl acetate
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GB 1886.201-2016
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Basic data | Standard ID | GB 1886.201-2016 (GB1886.201-2016) | | Description (Translated English) | National Food Safety Standard -- Food Additives -- Benzyl acetate | | Sector / Industry | National Standard | | Classification of Chinese Standard | X40 | | Word Count Estimation | 5,580 | | Date of Issue | 2016-08-31 | | Date of Implementation | 2017-01-01 | | Regulation (derived from) | Announcement of the State Administration of Public Health and Family Planning 2016 No.11 | | Issuing agency(ies) | National Health and Family Planning Commission of the People's Republic of China, State Food and Drug Administration | GB 1886.201-2016: National Food Safety Standard -- Food Additives -- Benzyl acetate---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
(Food safety national standard - Food additive - Benzyl acetate)
National Standards of People's Republic of China
National standards for food safety
Food additives benzyl acetate
2016-08-31 released
2017-01-01 Implementation
People's Republic of China
National Health and Family Planning Commission released
National standards for food safety
Food additives benzyl acetate
1 Scope
This standard applies to benzyl alcohol or benzyl chloride as a raw material by chemical reaction of the food additives benzyl acetate.
2 chemical name, molecular formula, structural formula and relative molecular mass
2.1 Chemical name
Benzyl acetate
2.2 Molecular formula
C9H10O2
2.3 Structural formula
2.4 Relative molecular mass
150.18 (according to.2007 international relative atomic mass)
3 technical requirements
3.1 sensory requirements
Sensory requirements shall comply with the requirements of Table 1.
Table 1 sensory requirements
The project requires a test method
Colorless to pale yellow
State liquid
The sample was placed in a colorimetric tube and visually observed
Aroma sweet, fruity, jasmine aroma GB/T 14454.2
3.2 Physical and chemical indicators
Physical and chemical indicators should be consistent with the provisions of Table 2.
Table 2 Physical and chemical indicators
Item Index Test Method
Benzyl acetate content, w /% ≥ 98.0 Appendix A
Acid value (in KOH)/(mg/g) ≤ 1.0 GB/T 14455.5
Refractive index (20 ° C) 1.500 ~ 1.504 GB/T 14454.4
Relative density (25 ℃/25 ℃) 1.049 ~ 1.059 GB/T 11540
Trace chlorine through test GB/T 14454.12
Appendix A
Determination of benzyl acetate content
A.1 Instruments and equipment
A.1.1 chromatograph. according to GB/T 11538-2006 in Chapter 5 of the provisions.
A.1.2 Column. Capillary column.
A.1.3 Detector. Hydrogen flame ionization detector.
A.2 Determination method
Area normalization method. according to GB/T 11538-2006 10.4 determination of content.
A.3 repeatability and result representation
According to GB/T 11538-2006 11.4 provisions, should meet the requirements.
The chromatographic and analytical conditions for the benzyl acetate of the food additive are given in Appendix B.
Appendix B
Food additives - Benzyl acetate - Gas chromatographic and operating conditions
(Area normalization method)
B.1 Food Additive Acetyl acetate Gas Chromatography
Food additive benzyl acetate gas chromatogram shown in Figure B.1.
Figure B.1 Food additives Acetate acetate gas chromatogram
B.2 Operating conditions
B.2.1 Column. capillary column, length 30m, diameter 0.53mm.
B.2.2 Stationary phase. 100% dimethylpolysiloxane.
B.2.3 Film thickness. 1.5 μm.
B.2.4 Chromatographic furnace temperature. linear program temperature from 70 ℃ to 180 ℃, the rate of 5 ℃/min; then linear program temperature from 180 ℃ to
260 ℃, the rate of 10 ℃/min, and finally at 260 ℃ constant temperature 10min.
B.2.5 Inlet temperature. 260 ° C.
B.2.6 Detector temperature. 260 ° C.
B.2.7 Detector. Hydrogen flame ionization detector.
B.2.8 Carrier gas. nitrogen.
B.2.9 Pre-column pressure. 30 kPa.
B.2.10 Injection volume. 0.2 μL.
B.2.11 Split ratio. 80. 1.
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