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SN/T 3545-2013 PDF English

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SN/T 3545-2013: Determination of various preservaives in foods for export
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SN/T 3545-2013English519 Add to Cart 4 days [Need to translate] Determination of various preservaives in foods for export

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Basic data

Standard ID SN/T 3545-2013 (SN/T3545-2013)
Description (Translated English) Determination of various preservaives in foods for export
Sector / Industry Commodity Inspection Standard (Recommended)
Classification of Chinese Standard XO4
Classification of International Standard 67.050
Word Count Estimation 20,240
Regulation (derived from) AQSIQ notification issued in 2013 on the first batch of 179 entry-exit inspection and quarantine of industry standards; industry standard for filing Notice 2013 No. 9 (No. 165 overall)
Issuing agency(ies) General Administration of Customs
Summary This standard specifies the foods propionic acid, sorbic acid, benzoic acid, acetic acid dehydrogenation, the US-hydroxy benzoate, methyl paraben Shen, paraben, ethyl paraben Shen acid isobutylamide acetate, propyl paraben and gas chromatography and sampl

SN/T 3545-2013: Determination of various preservaives in foods for export


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of various preservaives in foods for export People's Republic of China Entry-Exit Inspection and Quarantine Standards Export more preservatives in food measurement method Issued on. 2013-03-01 2013-09-16 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released

Foreword

This standard was drafted in accordance with GB/T 1.1-2009 given rules. Please note that some of the content of this document may involve patents. Distribution of this document Institutions do not assume the responsibility to identify these patents. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard was drafted. People's Republic of China Liaoning Province Exit Inspection and Quarantine. The main drafters of this standard. Dongzhen Lin, Mike Sui, Pang Yanhua, even Xu, Jiang Wei. Export more preservatives in food measurement method

1 Scope

This standard specifies the foods propionic acid, sorbic acid, benzoic acid, dehydroacetic acid, p-hydroxy benzoate, methyl paraben, for Ethyl paraben, isobutyl p-hydroxybenzoate, propyl paraben and butyl paraben more preservatives Gas Chromatography Detection and sample preparation methods. This standard applies to salted pepper, instant noodles, miso, milk, salted mushrooms, orange juice, cakes, soy sauce, wine and salted foods such as bracken more Species Determination of preservatives content.

2 Method summary

Preservative in the sample under acidic conditions (vitriol) with ethyl acetate or acetonitrile (added anhydrous magnesium sulfate and sodium chloride salting) mentioned Take, Pipette part extract was dried over anhydrous magnesium sulfate, determined by gas chromatography (GC), external standard.

3 Reagents and materials

Unless otherwise specified, the reagents used were HPLC grade. 3.1 acetonitrile. 3.2 ethyl acetate. 3.3 n-hexane. 3.4 Concentrated sulfuric acid. AR. 3.5 Sodium carbonate. AR. 3.6 Sodium chloride. AR. 3.7 anhydrous magnesium. AR; 650 ℃ burning 4h, stored in a sealed container in the back. 3.8 aqueous solution of sulfuric acid. 10% (volume fraction). 3.9 aqueous sodium carbonate solution. 0.20g/mL. 3.10 Standard preservative. purity of greater than or equal to 98%. For more information refer to the Material standard tables in Appendix A A.1. 3.11 Standard stock solution. namely, accurately weighed amount of preservative standards (4.10), paired with acetonitrile concentration of 10mg/mL standard Quasi stock solution. Standard stock solution stored at 0 ℃ ~ 4 ℃ condition. Formulated once every 12 months. 3.12 mixed standard stock solution. Pipette appropriate amount of acid, sorbic acid, benzoic acid, dehydroacetic acid, methylparaben, hydroxy Benzoate, propyl paraben, butyl paraben, p-hydroxy benzoate and parabens 10 kinds of isobutyl Standard preservative stock solution with acetonitrile dubbed mixed standard stock solution at a concentration of 500μg/mL. Mixed standard stock solution at 0 ℃ ~ At 4 ℃ storage, preparation once every six months. 3.13 mixed standard working solution. mixed standard stock solution was diluted with acetonitrile to a suitable concentration of standard working solution. At 0 ℃ ~ 4 ℃ Storage conditions. Once every three months preparation.

4 instruments and equipment

4.1 Gas chromatograph. equipped with a flame ionization detector (FID).
...

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