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Rapid determination of melamine in export liquid state milk. Raman spectrometry method
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Basic data
| Standard ID | SN/T 2805-2011 (SN/T2805-2011) |
| Description (Translated English) | Rapid determination of melamine in export liquid state milk. Raman spectrometry method |
| Sector / Industry | Commodity Inspection Standard (Recommended) |
| Classification of Chinese Standard | X16 |
| Word Count Estimation | 8,852 |
| Date of Issue | 2011-02-25 |
| Date of Implementation | 2011-07-01 |
| Quoted Standard | GB/T 6682; GB/T 22388-2008 |
| Regulation (derived from) | ?AQSIQ-Inspection [2011] 90 |
| Issuing agency(ies) | General Administration of Customs |
| Summary | This standard specifies the rapid detection of melamine in liquid milk, two pull is spectrometric methods. This standard applies to raw milk, ������syntax determination yogurt two melamine content, pure milk. |
SN/T 2805-2011: Rapid determination of melamine in export liquid state milk. Raman spectrometry method
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Rapid determination of melamine in export liquid state milk.Raman spectrometry method
People's Republic of China Entry-Exit Inspection and Quarantine Standards
Exports of liquid milk melamine Rapid Determination
Raman spectroscopy
Issued on. 2011-02-25
2011-07-01 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
This standard was drafted in accordance with the rules of GB/T 1.1-2009 and GB/T 20001.4-2001 given.
This standard is proposed and managed by the National Certification and Accreditation Administration Committee.
This standard was drafted. China Inspection and Quarantine Science Research Institute, Heilongjiang People's Republic of China Exit Inspection and Quarantine.
The main drafters of this standard. Qi flowers, ROCKETS, Liu Feng, Zhang Cheng, Zou Mingjiang, Wang Xi Meng, Wu Miao Miao, Hong celebrate, Li Meng, Yang Fuqiang.
Introduction
When issuing authority of the document drew attention to the statement of compliance with this document may involve 4.5 sensitizing agents related to the use of patents.
The issuing authority for the patent document authenticity, validity and scope without any position.
The patent holder has to ensure that the issuing authority of the document, he was willing to reasonable and non-discriminatory terms and conditions with any applicant,
Patent licensing negotiations. The patent holder's statement has been filed in the release mechanism of the present document. Related information is available through the following
Contact at.
Patent holder. Chinese Academy of Inspection and Quarantine
Contact. Zou Mingjiang
Address. Gaobeidian Road, Chaoyang District, Beijing, No. 3 Chinese Academy of Inspection and Quarantine Zip code. 100123
Please note that in addition to the above patents, some of the contents of this document can still be involved in the patent. The issuing authority of this document does not bear this recognition
These patent liability.
Exports of liquid milk melamine Rapid Determination
Raman spectroscopy
1 Scope
This standard specifies the Raman spectroscopy method for rapid detection of melamine in liquid milk.
This standard applies to raw milk, determination and sour milk melamine content Raman spectroscopy.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
Laboratory use specifications and test methods GB/T 6682 Analysis
GB/T 22388-2008 raw milk and dairy products of melamine detection methods
Principle 3
Different materials have their molecular structure corresponding characteristic Raman (Raman) spectroscopy. Raw milk, milk and yogurt samples were diluted
Release, centrifugation, dried the surface enhancement principle based detection kit enhancement, scanning for Raman scattering. To 928cm-1 ± 2cm-1 as a reference
Test peak, set the corresponding strength of 100 spectra were normalized at 698cm-1 ± 2cm-1 under, according to the melamine content in the sample and return
Houla Man correspondence between a spectrum of relative strength was determined by external standard method.
4 Reagents and materials
Unless otherwise indicated, the reagents used were of analytical grade or above water as a water GB/T 6682 regulations.
4.1 melamine standard. purity ≥99.0%.
4.2 Melamine standard stock solution. 1.00g/L. Accurately weighed 100mg (accurate to 0.1mg) melamine standard (4.1), was added
60mL ~ 80mL of water, ultrasonic solubilization, constant volume to 100mL volumetric flask. Stored in the dark at 0 ℃ ~ 4 ℃ condition.
4.3 negative samples. Determination of melamine by the GB GB/T 22388-2008 Method < 0.1mg/kg actual sample or negative
Dry sample by sample matrix matching ratio was diluted with water before use when the existing service.
4.4 standard solution. When you use the existing service.
4.4.1 standard solution Ⅰ (50.0μg/mL). accurate Pipette 5.0mL melamine stock standard solution (4.2) in 100mL flask
With water to volume, and mix.
4.4.2 standard solution Ⅱ (10.0μg/mL). accurate Pipette 1.0mL melamine stock standard solution (4.2) in 100mL flask
With water to volume, and mix.
4.4.3 Table 1 pipette different volumes of each standard solution Ⅰ or Ⅱ (4.4.1 and 4.4.2) and negative sample volume to 5.0mL,
Mix well.
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