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Test method of furfural alcohol purity. Gas chromatography
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Basic data
| Standard ID | SN/T 1251-2003 (SN/T1251-2003) |
| Description (Translated English) | Test method of furfural alcohol purity. Gas chromatography |
| Sector / Industry | Commodity Inspection Standard (Recommended) |
| Classification of Chinese Standard | B72 |
| Classification of International Standard | 71.080.60 |
| Word Count Estimation | 7,769 |
| Date of Issue | 2003-05-28 |
| Date of Implementation | 2003-12-01 |
| Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People Republic of China |
| Summary | This standard applies to content greater than 96% alcohol test. |
SN/T 1251-2003: Test method of furfural alcohol purity. Gas chromatography
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Test method of furfural alcohol purity.Gas chromatography
People's Republic of China Entry-Exit Inspection and Quarantine Industry Standard
Method for testing industrial sterol content
Gas chromatography
Released on.2003-05-28
Implementation of.2003-12-01
People's Republic
The General Administration of Quality Supervision, Inspection and Quarantine issued
Foreword
Appendix A and Appendix B of this standard are informative annexes.
This standard is proposed and managed by the National Certification and Accreditation Administration.
This standard was drafted by the Shanxi Entry-Exit Inspection and Quarantine Bureau of the People's Republic of China.
The main drafters of this standard. Song Huan, Chen Yong, Yang Xiaobing, Pan Yali, Qu Jun.
This standard is the industry standard for inspection and quarantine issued for the first time.
Method for testing industrial sterol content
Gas chromatography
1 Scope
This standard specifies the sampling, sample preparation and inspection methods for sterol content.
This standard applies to tests with a content greater than 96% sterol.
2 Normative references
The terms in the following documents become the terms of this standard by reference to this standard. All dated references, followed by all
Modifications (not including errata content) or revisions do not apply to this standard, however, parties to agreements based on this standard are encouraged to study
Is it possible to use the latest version of these files? For undated references, the latest edition applies to this standard.
GB/T 6680-1996 General rules for sampling of liquid chemical products
GB/T 9722-1988 General rules for gas chromatography of chemical reagents
GB/T 14022.1-1992 industrial sterol
3 sampling and sample preparation
3.1 Sampling method
Sampling is carried out in accordance with the provisions of GB/T 6680-1996.
3.2 Sample preparation method
Sample preparation is carried out in accordance with the provisions of GB/T 6680-1996.
3.3 Sample storage
Sample storage is carried out in accordance with the provisions of GB/T 14022.1-1992.
4 Inspection methods
4.1 Moisture determination
See Appendix A for moisture determination.
4.2 Determination of sterol content
4.2.1 Principle of the method
Gas chromatograph, direct injection, separation by capillary column, detection by hydrogen flame ionization detector, normalized by area
Quantity calculation.
4.2.2 Instrumentation
a) Gas chromatograph. equipped with hydrogen flame ionization detector and data processor, sensitivity and stability in line with GB/T 9722-1988
Provisions;
b) Microsampler.
4.2.3 Test procedure
4.2.3.1 Chromatographic conditions
a) Column. TPA modified polyethanol capillary column (25m × 0.33mm × 0.25μm);
b) column temperature. 110 ° C;
c) inlet temperature..200 ° C;
...