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GB/T 35410-2017 PDF English

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GB/T 35410-2017: Method of performance testing for liquid chromatography-tandem quadrupole mass spectrometry
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Basic data

Standard ID GB/T 35410-2017 (GB/T35410-2017)
Description (Translated English) Method of performance testing for liquid chromatography-tandem quadrupole mass spectrometry
Sector / Industry National Standard (Recommended)
Classification of Chinese Standard N54
Classification of International Standard 71.040.30
Word Count Estimation 10,130
Date of Issue 2017-12-29
Date of Implementation 2018-04-01
Regulation (derived from) National Standards Bulletin 2017 No. 32
Issuing agency(ies) General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China

GB/T 35410-2017: Method of performance testing for liquid chromatography-tandem quadrupole mass spectrometry




---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Method of performance testing for liquid chromatography-tandem quadrupole mass spectrometry ICS 71.040.30 N54 National Standards of People's Republic of China Liquid chromatography - tandem quadrupole mass spectrometry Determination of performance 2017-12-29 Posted 2018-04-01 implementation General Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China China National Standardization Administration released

Foreword

This standard was drafted in accordance with the rules given in GB/T 1.1-2009. This standard is proposed by the Ministry of Science and Technology of the People's Republic of China. This standard by the National Instrument Analysis and Testing Standardization Technical Committee (SAC/TC481) centralized. This standard drafting unit. China Institute of Metrology. The main drafters of this standard. Dai Xinhua, Shao Mingwu, He Haihong, Jiang You, Wang Weihua, Zhang Wei, Song Dewei, Su Fuhai. Liquid chromatography - tandem quadrupole mass spectrometry Determination of performance

1 Scope

This standard specifies the performance of liquid chromatography - quadrupole mass spectrometry test methods. This standard applies to liquid chromatography - tandem quadrupole mass spectrometer performance measurement.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version applies to this article Pieces. For undated references, the latest edition (including all amendments) applies to this document. GB/T 32264 gas chromatography quadrupole mass spectrometer performance measurement methods GB/T 32267 analytical instruments performance measurement terminology

3 Terms and definitions

GB/T 32264, GB/T 32267 and defined by the following terms and definitions apply to this document. 3.1 Linear correlation coefficient linearcorrelationcoefficient A parameter that characterizes the linear correlation between response area and analyte concentration.

4 Reagents and standards

Unless otherwise specified, all solvents are chromatographic grade. The following reagents should be used, according to the instrument when used to the appropriate dilution concentration. 4.1 reserpine standard solution, 1.0μg/mL. 4.2 polypropylene glycol (PPG) 450 solution, 3.6μg/mL. 4.3 PPG1000 solution, 3.6 μg/mL. 4.4 PPG2000 solution, 3.6 μg/mL. 4.5 Chloramphenicol, 99.7%. 4.6 Methanol, acetonitrile, isopropanol, formic acid. 4.7 water, Milipore ultrapure water. 4.8 solution dilution and preparation methods see A.3.

5 laboratory environmental conditions

5.1 should be clean, dust-free, non-flammable, explosive and highly corrosive gases or reagents, good ventilation. 5.2 indoor temperature .15 ℃ ~ 30 ℃; relative humidity less than 75%. 5.3 instrument table should be smooth, no strong mechanical vibration and electromagnetic interference around. ...

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