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Screening of organotin in electrical and electronic products -- Infrared spectrometry
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Basic data
| Standard ID | GB/T 32888-2016 (GB/T32888-2016) |
| Description (Translated English) | Screening of organotin in electrical and electronic products -- Infrared spectrometry |
| Sector / Industry | National Standard (Recommended) |
| Classification of Chinese Standard | L10 |
| Classification of International Standard | 31.020 |
| Word Count Estimation | 14,141 |
| Date of Issue | 2016-08-29 |
| Date of Implementation | 2017-03-01 |
| Regulation (derived from) | National Standard Announcement 2016 No.14 |
| Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China |
GB/T 32888-2016: Screening of organotin in electrical and electronic products -- Infrared spectrometry
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Screening of organotin in electrical and electronic products - Infrared spectrometry
ICS 31.020
L10
National Standards of People's Republic of China
Screening of organotin in electrical and electronic products
Infrared spectroscopy
2016-08-29 released
2017-03-01 implementation
General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China
China National Standardization Management Committee released
Foreword
This standard is drafted in accordance with the rules given in GB/T 1.1-2009.
This standard is proposed by the National Environmental Electronics Standardization Technical Committee (SAC/TC297).
The drafting unit of this standard. Guangdong Entry-Exit Inspection and Quarantine Bureau, Shenzhen Institute of Measurement and Quality Inspection.
The main drafters of this standard. Xiao Dahui, Yue Dalei, Su Caizhu, Xing Yuanna, Zhou Minghui, Liu Yingfeng, Zheng Jianguo, Zhai Cuiping, Xiao Qian,
Li Han, Zhang Zihao, Peng Ying, Wang Jing.
Screening of organotin in electrical and electronic products
Infrared spectroscopy
1 Scope
This standard specifies the organic tin in the electronic components of electronic products Fourier transform infrared spectroscopy (FT-IR) screening method.
This standard applies to the electrical and electronic products in the plastic parts of not less than 0.05% of the organic tin screening.
2 normative reference documents
The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article
Pieces. For undated references, the latest edition (including all modifications) applies to this document.
Limits for Restricted Substances in Electrical and Electronic Products GB/T 26572-2011
3 principle
Collect the sample of the polymer material for the electrical and electronic products, freeze and crush the organic tin in the sample by adding n-hexane, and then
The extract was concentrated. The concentrated extract was added to the potassium bromide chip to collect the infrared spectrum, and it was observed whether the spectrum had organic tin C-Sn bond
630cm-1 ~ 440cm-1 between the characteristics of absorption, to determine whether the sample contains organic tin.
4 Reagent or material
In addition to the special provisions of this standard are the use of excellent pure reagent.
4.1 potassium bromide (KBr), the spectrum of pure.
4.2-butyltin trichloride, purity greater than or equal to 96.0%.
4.3 Dipropyltin dichloride, purity greater than or equal to 99.5%.
4.4 dibutyltin dichloride, purity greater than or equal to 99.0%.
4.5 Diphenyltin dichloride, purity greater than or equal to 97.0%.
4.6 Trimethyltin chloride, purity greater than or equal to 99.0%.
4.7 tributyltin chloride, purity greater than or equal to 96.5%.
4.8 Triphenyltin chloride, purity greater than or equal to 96.0%.
4.9 tetrabutyltin, purity greater than or equal to 99.0%.
4.10 Tetrapropyltin, purity greater than or equal to 99.0%.
4.11 Tetraphenyltin, purity greater than or equal to 99.0%.
4.12 n-hexane, analytical grade.
5 equipment
5.1 Fourier transform infrared spectrometer, wave range. 4000cm-1 ~ 400cm-1, the minimum resolution. 0.3cm-1.
5.2 electronic balance, accurate to 0.1mg.
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