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Textiles -- Determination of dyestuffs of disperse yellow 23 and disperse orange 149
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Basic data
| Standard ID | GB/T 23345-2009 (GB/T23345-2009) |
| Description (Translated English) | Textiles -- Determination of dyestuffs of disperse yellow 23 and disperse orange 149 |
| Sector / Industry | National Standard (Recommended) |
| Classification of Chinese Standard | W04 |
| Classification of International Standard | 59.080.01 |
| Word Count Estimation | 9,915 |
| Date of Issue | 2009-03-19 |
| Date of Implementation | 2010-02-01 |
| Quoted Standard | GB/T 6682 |
| Regulation (derived from) | National Standard Approval Announcement 2009 No.3 (Total No.143) |
| Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China |
| Summary | This standard specifies the use of liquid chromatography-Textile products Disperse Yellow 23 and Disperse Orange 149 dye content of tandem mass spectrometry (LC-MS/MS) and high performance liquid chromatography (HPLC) determination. This standard applies to textile products by dyeing process. |
GB/T 23345-2009: Textiles -- Determination of dyestuffs of disperse yellow 23 and disperse orange 149
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Textiles. Determination of dyestuffs of disperse yellow 23 and disperse orange 149
ICS 59.080.01
W04
National Standards of People's Republic of China
textile
Determination of Disperse Yellow 23 and Disperse Orange 149 dye
Posted 2009-03-19
2010-02-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
Appendix A of this standard and Appendix B is an informative annex.
The standard proposed by China Textile Industry Association.
The standard basis by the National Textile Standards Technical Committee of Standardization Technical Committee (SAC/TC209/SC1) centralized.
This standard was drafted. People's Republic of China Jiangsu Entry-Exit Inspection and Quarantine Bureau, Textile Industry Research Institute of Standardization.
The main drafters of this standard. Friends of Ding Chao, Caoxi Zhong, Zhou Jing Chu, Wu Hao, and Cai, Zhou Jia, Tian Shu, Wang Hsiao-ping.
textile
Determination of Disperse Yellow 23 and Disperse Orange 149 dye
Warning. Use of this standard shall have a person experiences regular laboratory work. This standard does not point out all possible security issues.
Users have the responsibility to take appropriate safety and health practices and to ensure compliance with the conditions relevant national regulations.
1 Scope
This standard specifies the use of liquid chromatography - tandem mass spectrometry (LC-MS/MS) and high performance liquid chromatography (HPLC) Determination of textile products
The Disperse Yellow 23 and Disperse Orange 149 dye content method.
This standard applies to processed by dyeing of textile products.
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
Laboratory use specifications and test methods GB/T 6682 Analysis
Principle 3
Reflux extraction with boiling chlorobenzene sample dye concentrate rid extract the solvent, the residue was washed with methanol to volume. With polytetrafluoroethylene
After ene membrane filtration, the sample solution by liquid chromatography - tandem mass spectrometry (LC-MS/MS) measurement and validation, external standard; or high performance liquid chromatography
Spectrometer (HPLC) assay, if necessary, supplemented by thin layer chromatography (TLC) to confirm, external standard.
4 Reagents
Unless otherwise indicated, the reagents used in the analysis were of analytical grade and GB/T 6682 provisions tertiary water.
4.1 chlorobenzene.
4.2 toluene.
4.3 xylene.
4.4 tetrahydrofuran.
4.5 n-hexane.
4.6 chloroform.
4.7 ethyl acetate.
4.8 phosphoric acid.
4.9 Methanol (HPLC grade).
4.10 Acetonitrile (HPLC grade).
4.11 formic acid (HPLC grade).
4.12 standard solution
4.12.1 Disperse Yellow 23 (CAS Number. 6250-23-3) and Disperse Orange 149 (CAS Number. 85136-74-9) one-component stock standard solution
(500mg/L), formulated with the methanol solvent.
NOTE. The standard solution in a refrigerator 2 ℃ ~ 4 ℃ in preservation, valid for 12 months.
4.12.2 HPLC analysis of standard working solution (5.0mg/L). Pipette from each single component standard stock solution into the same flask 1mL
...