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Food additive -- Dihydro-ionone standards: food additives specified standards of food additives dihydro-ionone
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Basic data
| Standard ID | GB 29957-2013 (GB29957-2013) |
| Description (Translated English) | Food additive -- Dihydro-ionone standards: food additives specified standards of food additives dihydro-ionone |
| Sector / Industry | National Standard |
| Classification of Chinese Standard | C53 |
| Classification of International Standard | 67.020 |
| Word Count Estimation | 8,811 |
| Regulation (derived from) | China Food & Drug Administration [2013] No. 234, November, 1, 2013 |
| Issuing agency(ies) | National Health and Family Planning Commission of the People's Republic of China |
| Summary | This standard applies to food additives: dihydro ionone. |
GB 29957-2013: Food additive -- Dihydro-ionone standards: food additives specified standards of food additives dihydro-ionone
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Food additive-Dihydro-ionone standards. food additives specified standards of food additives dihydro-ionone
National Standards of People's Republic of China
National Food Safety Standard
Food Additives dihydro ionone -β-
Issued on. 2013-11-29
2014-06-01 implementation
National Food Safety Standard
Food Additives dihydro ionone -β-
1 Scope
This standard applies to the β- ionone materials obtained food additive dihydro -β- ionone.
2 chemical name, molecular formula, molecular mass and structural formula
2.1 Chemical Name
4- (2,6,6-trimethyl-1-cyclohexen-yl) -3-butyl-2-one
Formula 2.2
C13H22O
2.3 formula
2.4 relative molecular mass
194.32 (according to 2007 international relative atomic mass)
3 Technical requirements
3.1 Sensory requirements
Sensory requirements shall comply with the requirements of Table 1.
Table 1 Sensory requirements
Project requires test methods
Colorless to pale yellow color of the sample was placed inside color than the tube, were visually observed
Liquid state
Fruity aroma, with a woody bottom rhyme GB/T 14454.2
3.2 Physical and Chemical Indicators
Physical and chemical indicators should be consistent with the provisions of Table 2.
Table 2. Physical and chemical indicators
Item Index Test Method
Content (dihydro and tetrahydro -β- -β- ionone ionone sum), w /% ≥ 99.0 Appendix A
Refractive index (20 ℃) 1.479 ~ 1.485 GB/T 14454.4
The relative density (25 ℃/25 ℃) 0.920 ~ 0.930 GB/T 11540
Appendix A
Determination dihydro-ionone content -β-
A.1 instruments and equipment
A.1.1 chromatograph. According to GB/T 11538-2006 provisions in Chapter 5.
A.1.2 Column. capillary column.
A.1.3 Detector. Hydrogen flame ionization detector.
A.2 Determination
Area normalization method. According to GB/T 11538-2006 10.4 Determination.
A.3 repeatability and results are shown
According to GB/T 11538-2006 provisions in 11.4, shall comply with the requirements.
Food Additives dihydro -β- ionone gas chromatograph (area normalization method) See Appendix B.
Appendix B
Food additives dihydro ionone gas chromatogram -β-
(Area normalization method)
B.1 food additives dihydro ionone -β- gas chromatogram
Figure B.1.
1-- tetrahydro -β- ionone;
2-- dihydro -β- ionone.
B.1 food additives dihydro ionone -β- gas chromatogram
B.2 operating conditions
B.2.1 Column. capillary column, length 30 m, an inner diameter of 0.25 mm.
B.2.2 stationary phase. modified polyethylene glycol.
B.2.3 film thickness. 0.25 μm.
B.2.4 chromatography oven temperature. 120 ℃ constant temperature 2 min; then linear temperature program from 120 ℃ ~ 200 ℃, the rate of 5 ℃/min; final
At 200 ℃ thermostat 5 min.
B.2.5 Inlet temperature. 250 ℃.
B.2.6 detector temperature. 250 ℃.
B.2.7 Detector. Hydrogen flame ionization detector.
B.2.8 carrier gas. nitrogen.
B.2.9 pre-column pressure. 69 kPa.
B.2.10 Injection volume. 0.2 μL.
B.2.11 split ratio. 100︰1.
...