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National Food Safety Standard -- Food Additives -- Ethyl benzoate
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Basic data
| Standard ID | GB 1886.288-2016 (GB1886.288-2016) |
| Description (Translated English) | National Food Safety Standard -- Food Additives -- Ethyl benzoate |
| Sector / Industry | National Standard |
| Classification of Chinese Standard | X40 |
| Word Count Estimation | 5,527 |
| Date of Issue | 2016-08-31 |
| Date of Implementation | 2017-01-01 |
| Regulation (derived from) | Announcement of the State Administration of Public Health and Family Planning 2016 No.11 |
| Issuing agency(ies) | National Health and Family Planning Commission of the People's Republic of China, State Food and Drug Administration |
GB 1886.288-2016: National Food Safety Standard -- Food Additives -- Ethyl benzoate
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
(Food safety national standard - Food additive - Benzoate)
National Standards of People's Republic of China
National Food Safety Standard
Food additive benzoate
Published 2016-08-31
2017-01-01 implementation
People's Republic of China
National Health and Family Planning Commission issued
National Food Safety Standard
Food additive benzoate
1 Scope
This standard applies to a food additive ethyl alcohol and benzoic acid as raw materials obtained.
2 Chemical name, molecular formula, structural formula and relative molecular mass
2.1 Chemical Name
Benzoate
Formula 2.2
C9H10O2
2.3 formula
2.4 Molecular Weight
150.18 (according to 2007 international relative atomic mass)
3 Technical requirements
3.1 Sensory requirements
Sensory requirements shall comply with the requirements in Table 1.
Table 1 Sensory requirements
Project requires test methods
Color
status
colorless
Oily liquid
The sample was placed in a cuvette, were visually observed
Mild aroma, strong floral, fruity aroma GB/T 14454.2
3.2 Physical and Chemical Indicators
Physical and chemical indicators should be consistent with the provisions of Table 2.
Table 2. Physical and chemical indicators
Item Index Test Method
Benzoate content, w /% ≥ 98.0 Appendix A
Acid number (as KOH)/(mg/g) ≤ 1.0 GB/T 14455.5
Refractive index (20 ℃) 1.502 ~ 1.508 GB/T 14454.4
Relative density (25 ℃/25 ℃) 1.043 ~ 1.050 GB/T 11540
Appendix A
Content Determination benzoate
A.1 instruments and equipment
A.1.1 Chromatography. in GB/T 11538-2006 specified in Chapter 5.
A.1.2 Column. capillary column.
A.1.3 Detector. hydrogen flame ionization detector.
A.2 Determination
Area normalization method. Press the GB/T 11538-2006 Determination 10.4.
A.3 repeatability and results are expressed
11538-2006 carried out in accordance with the provisions of 11.4 GB/T , should meet the requirements.
Food additive gas chromatogram benzoate and operating conditions see Appendix B.
Appendix B
Benzoate gas chromatogram and operating conditions
(Area normalization method)
B.1 food additive gas chromatogram of ethyl
Benzoate food additive gas chromatography is shown in Figure B.1.
Figure B.1 food additive gas chromatogram of ethyl
B.2 operating conditions
B.2.1 Column. capillary column, length 30m, internal diameter 0.53mm.
B.2.2 stationary phase. 100% polydimethyl siloxane.
B.2.3 film thickness. 1.5μm.
B.2.4 chromatographic oven temperature. 100 ℃ thermostat 0.1min, then linear temperature programmed from 100 deg.] C to 180 ℃, a rate of 5 ℃/min, then linear
Temperature programmed from 180 [deg.] C to 260 ℃, a rate of 10 ℃/min, the final temperature at 260 ℃ 10min.
B.2.5 Inlet temperature. 260 ℃.
B.2.6 detector temperature. 260 ℃.
B.2.7 Detector. hydrogen flame ionization detector.
B.2.8 Carrier gas. nitrogen.
B.2.9 before the column pressure. 30kPa.
B.2.10 Injection volume. 0.2μL.
B.2.11 split ratio. 80.1.
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