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National Food Safety Standard -- Food Additives -- Ethyl Isovalerate
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Basic data
| Standard ID | GB 1886.287-2016 (GB1886.287-2016) |
| Description (Translated English) | National Food Safety Standard -- Food Additives -- Ethyl Isovalerate |
| Sector / Industry | National Standard |
| Classification of Chinese Standard | X40 |
| Word Count Estimation | 6,620 |
| Date of Issue | 2016-08-31 |
| Date of Implementation | 2017-01-01 |
| Regulation (derived from) | Announcement of the State Administration of Public Health and Family Planning 2016 No.11 |
| Issuing agency(ies) | National Health and Family Planning Commission of the People's Republic of China, State Food and Drug Administration |
GB 1886.287-2016: National Food Safety Standard -- Food Additives -- Ethyl Isovalerate
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
(Food safety national standard - Food additive - Ethyl isovalerate)
National Standards of People's Republic of China
National Food Safety Standard
Ethyl isovalerate food additives
Published 2016-08-31
2017-01-01 implementation
People's Republic of China
National Health and Family Planning Commission issued
National Food Safety Standard
Ethyl isovalerate food additives
1 Scope
This standard applies to isovalerate ethanol for raw materials and food additive ethyl isovalerate.
2 Chemical name, molecular formula, structural formula and relative molecular mass
2.1 Chemical Name
Ethyl 3-methylbutanoate, ethyl 2-methylbutyrate
Formula 2.2
C7H14O2
2.3 formula
Ethyl 3-methylbutanoate, ethyl 2-methylbutyrate
2.4 Molecular Weight
130.19 (according to 2007 international relative atomic mass)
3 Technical requirements
3.1 Sensory requirements
Sensory requirements shall comply with the requirements in Table 1.
Table 1 Sensory requirements
Project requires test methods
Color
status
colorless
liquid
The sample was placed in a cuvette, visually
Was observed
After dilution with a Qiang Lie aroma of fruit, wine, apple-like aroma GB/T 14454.2
3.2 Physical and Chemical Indicators
Physical and chemical indicators should be consistent with the provisions of Table 2.
Table 2. Physical and chemical indicators
Item Index Test Method
Ethyl isovalerate content, w /% ≥ 98.0 (sum of two isomers) Appendix A
Acid number (as KOH)/(mg/g) ≤ 2.0 GB/T 14455.5
Refractive index (20 ℃) 1.395 ~ 1.399 GB/T 14454.4
Relative density (25 ℃/25 ℃) 0.862 ~ 0.866 GB/T 11540
Appendix A
Determination of the content of ethyl isovalerate
A.1 instruments and equipment
A.1.1 Chromatography. in GB/T 11538-2006 specified in Chapter 5.
A.1.2 Column. capillary column.
A.1.3 Detector. hydrogen flame ionization detector.
A.2 Determination
Area normalization method. Press the GB/T 11538-2006 Determination 10.4.
A.3 repeatability and results are expressed
11538-2006 carried out in accordance with the provisions of 11.4 GB/T , should meet the requirements.
Food additive gas chromatogram of ethyl isovalerate and operating conditions see Appendix B.
Appendix B
Ethyl isovalerate food additive gas chromatography and the operating conditions of FIG.
(Area normalization method)
B.1 ethyl isovalerate food additive gas chromatogram
Ethyl isovalerate food additive gas chromatography is shown in Figure B.1.
Description.
. 1 --- ethyl 2-methylbutyrate;
2 --- 3-methylbutanoate.
Figure B.1 ethyl isovalerate food additive gas chromatogram
B.2 operating conditions
B.2.1 Column. capillary column, length 50m, diameter 0.2mm.
B.2.2 stationary phase. polyethylene glycol 20000.
B.2.3 film thickness. 0.2μm.
B.2.4 chromatographic oven temperature. 80 ℃.
B.2.5 Inlet temperature. 250 ℃.
B.2.6 detector temperature. 250 ℃.
B.2.7 Detector. hydrogen flame ionization detector.
B.2.8 Carrier gas. nitrogen.
B.2.9 before the column pressure. 138kPa.
B.2.10 Injection volume. 0.2μL.
B.2.11 split ratio. 100.1.
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