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National Food Safety Standard -- Food Additives -- Hesperidin
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Basic data
| Standard ID | GB 1886.260-2016 (GB1886.260-2016) |
| Description (Translated English) | National Food Safety Standard -- Food Additives -- Hesperidin |
| Sector / Industry | National Standard |
| Classification of Chinese Standard | X40 |
| Word Count Estimation | 10,189 |
| Date of Issue | 2016-08-31 |
| Date of Implementation | 2017-01-01 |
| Regulation (derived from) | Announcement of the State Administration of Public Health and Family Planning 2016 No.11 |
| Issuing agency(ies) | National Health and Family Planning Commission of the People's Republic of China, State Food and Drug Administration |
GB 1886.260-2016: National Food Safety Standard -- Food Additives -- Hesperidin
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
(Food safety national standard - Food additive - Hesperetin)
National Standards of People's Republic of China
National Food Safety Standard
Food additives hesperetin
Published 2016-08-31
2017-01-01 implementation
People's Republic of China
National Health and Family Planning Commission issued
National Food Safety Standard
Food additives hesperetin
1 Scope
This standard applies to the hesperidin for raw materials of food additives hesperetin.
2 Chemical name, molecular formula, structural formula and relative molecular mass
2.1 Chemical Name
5,7-dihydroxy-2- (3-hydroxy-4-methoxy - phenyl) - chroman-4-one
Formula 2.2
C16H14O6
2.3 formula
2.4 Molecular Weight
302.28 (according to 2007 international relative atomic mass)
3 Technical requirements
3.1 Sensory requirements
Sensory requirements shall comply with the requirements in Table 1.
Table 1 Sensory requirements
Project requires test methods
Pale yellow or white color
Status powder
The sample was placed on a clean white paper, were visually observed
GB vanilla aroma with a faint aroma oil flavor/T 14454.2
3.2 Physical and Chemical Indicators
Physical and chemical indicators should be consistent with the provisions of Table 2.
Table 2. Physical and chemical indicators
Item Index Test Method
Hesperetin content, w /% ≥ 95 Appendix A
Melting point/℃ 226 ~ 228 GB/T 14457.3
Appendix A
Determination of Content of hesperetin
A.1 Reagents and materials
A.1.1 Acetonitrile. chromatographically pure.
100mL. The resulting solution was filtered with a 0.45μm membrane, the filtrate was set aside.
A.4.3 Determination
In reference A.3 chromatographic conditions, respectively, the reference solution and the sample solution is measured, the peak area recorded.
A.5 calculation results
Hesperetin mass fraction levels w1, calculated according to formula (A.1).
w1 =
A1 × m2 × w2
A2 × m1 ×
100% (A.1)
Where.
Peak area of the main peak in the chromatogram of the sample solution A1 ---;
m2 --- reference mass, in grams (g);
Mass fraction content w2 of hesperetin --- reference in%;
Peak area of the main peak in the chromatogram of the reference solution A2 ---;
M1 --- sample mass, in grams (g).
...
