Path:
Home >
MISC >
Page95 > GA/T 2068-2023
Price & Delivery
US$399.00 · In stock · Download in 9 secondsGA/T 2068-2023: Forensic sciences--Screening methods for 16 rodenticides including tetramine in biological samples--LC-MS
Delivery: 9 seconds. True-PDF full-copy in English & invoice will be downloaded + auto-delivered via email. See
step-by-step procedureStatus: Valid
| Std ID | Version | USD | Buy | Deliver [PDF] in | Title (Description) |
| GA/T 2068-2023 | English | 399 |
Add to Cart
|
4 days [Need to translate]
|
Forensic sciences--Screening methods for 16 rodenticides including tetramine in biological samples--LC-MS
|
Click to Preview a similar PDF
Basic data
| Standard ID | GA/T 2068-2023 (GA/T2068-2023) |
| Description (Translated English) | Forensic sciences--Screening methods for 16 rodenticides including tetramine in biological samples--LC-MS |
| Sector / Industry | Public Security (Police) Industry Standard (Recommended) |
| Classification of Chinese Standard | A92 |
| Classification of International Standard | 13.310 |
| Word Count Estimation | 18,135 |
| Date of Issue | 2023-03-01 |
| Date of Implementation | 2023-12-01 |
| Issuing agency(ies) | Ministry of Public Security |
GA/T 2068-2023: Forensic sciences--Screening methods for 16 rodenticides including tetramine in biological samples--LC-MS
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
ICS 13:310
CCSA92
People's Republic of China Public Security Industry Standards
16 kinds of tetramine, etc: in forensic science biological samples
Rodenticide Screening by Liquid Chromatography-Mass Spectrometry
Released on 2023-03-01
2023-12-01 Implementation
Released by the Ministry of Public Security of the People's Republic of China
foreword
This document is in accordance with the provisions of GB/T 1:1-2020 "Guidelines for Standardization Work Part 1: Structure and Drafting Rules for Standardization Documents"
drafting:
Please note that some contents of this document may refer to patents: The issuing agency of this document assumes no responsibility for identifying patents:
This document was proposed by the National Criminal Technology Standardization Technical Committee Toxic Analysis Sub-Technical Committee (SAC/TC179/SC1) and submitted
Focus on:
This document was drafted by: Hangzhou Public Security Bureau, Criminal Investigation Team of Public Security Department of Guangxi Zhuang Autonomous Region, Criminal Investigation Team of Zhejiang Provincial Public Security Bureau
Team, Huzhou Public Security Bureau, Criminal Investigation Corps of Guangdong Provincial Public Security Bureau:
The main drafters of this document: Ying Jianbo, Xu Chen, Tang Lei, Li Xiaofei, Xie Weihong, Huang Kejian, Liu Xiaofeng, Fu Defeng, Xuanyu, Cui Yanhua,
Yang Fan and Zhang Liang:
16 kinds of tetramine, etc: in forensic science biological samples
Rodenticide Screening by Liquid Chromatography-Mass Spectrometry
1 Scope
This document specifies liquid chromatography-triple quadrupole mass spectrometry for 15 rodenticides in biological samples (blood, urine) in the field of forensic science
(LC-TQ/MS) test method and liquid chromatography-high resolution mass spectrometry (LC-HRMS) of 16 rodenticides in biological samples (blood, urine)
Testing method:
This document is applicable to the qualitative analysis of 16 rodenticides in biological samples (blood, urine) in the field of forensic science: Other test materials can refer to
use:
2 Normative references
The contents of the following documents constitute the essential provisions of this document through normative references in the text: Among them, dated references
For documents, only the version corresponding to the date is applicable to this document; for undated reference documents, the latest version (including all amendments) is applicable to
this document:
GB/T 6682 Analytical laboratory water specifications and test methods
GA/T 122 Toxicological Analysis Terminology
3 Terms and Definitions
The terms and definitions defined in GA/T 122 apply to this document:
4 principles
Using the blank sample and the added sample as a control, according to the requirements of parallel operation, the 16 rodenticides in blood and urine (compound basic information
See Appendix A) for extraction, purification and concentration, and detection by liquid chromatography-triple quadrupole mass spectrometry:
and ion-pair abundance ratio as the basis for qualitative judgment; or use liquid chromatography-high resolution mass spectrometry for detection, based on retention time, precursor ion and secondary
The exact mass of the characteristic ions of mass spectrometry was used as the basis for qualitative judgment:
5 Reagents and materials
5:1 Reagents
The experimental water should meet the first-class water specified in GB/T 6682: Unless otherwise stated, all reagents used in the analysis were chromatographically pure:
Reagents include:
a) Acetonitrile;
b) Methanol;
c) 0:1% acetic acid solution (take the preparation of 1000mL as an example): Measure 1:0mL of acetic acid, dilute it with water and set the volume to 1000mL,
mix well;
...
