Path:
Home >
MISC >
Page95 > GA/T 2023-2023
Price & Delivery
US$299.00 · In stock · Download in 9 secondsGA/T 2023-2023: Forensic sciences - Examination methods for 5F-AMB and 5F-APINACA in suspected drugs - LC and LC-MS
Delivery: 9 seconds. True-PDF full-copy in English & invoice will be downloaded + auto-delivered via email. See
step-by-step procedureStatus: Valid
| Std ID | Version | USD | Buy | Deliver [PDF] in | Title (Description) |
| GA/T 2023-2023 | English | 299 |
Add to Cart
|
3 days [Need to translate]
|
Forensic sciences - Examination methods for 5F-AMB and 5F-APINACA in suspected drugs - LC and LC-MS
|
Click to Preview a similar PDF
Basic data
| Standard ID | GA/T 2023-2023 (GA/T2023-2023) |
| Description (Translated English) | Forensic sciences - Examination methods for 5F-AMB and 5F-APINACA in suspected drugs - LC and LC-MS |
| Sector / Industry | Public Security (Police) Industry Standard (Recommended) |
| Classification of Chinese Standard | A92 |
| Classification of International Standard | 13.310 |
| Word Count Estimation | 15,179 |
| Date of Issue | 2023-03-01 |
| Date of Implementation | 2023-12-01 |
| Issuing agency(ies) | Ministry of Public Security |
GA/T 2023-2023: Forensic sciences - Examination methods for 5F-AMB and 5F-APINACA in suspected drugs - LC and LC-MS
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
ICS 13.310
CCSA92
Public safety industry standards of the People's Republic of China
Forensic science suspects 5F-AMB and 5F-AMB in drugs
5F-APINACA inspection
Liquid Chromatography and Liquid Chromatography-Mass Spectrometry
Published on 2023-03-01
Implemented on 2023-12-01
Released by the Ministry of Public Security of the People's Republic of China
Foreword
This document complies with the provisions of GB/T 1.1-2020 "Standardization Work Guidelines Part 1.Structure and Drafting Rules of Standardization Documents"
Drafting.
Please note that some content in this document may be subject to patents. The publisher of this document assumes no responsibility for identifying patents.
This document is proposed and submitted by the Toxic Analysis Sub-Technical Committee of the National Technical Committee for Standardization of Criminal Technology (SAC/TC179/SC1).
Return to home.
This document was drafted by. Beijing Municipal Public Security Forensic Identification Center, Ministry of Public Security Anti-Narcotics Intelligence Technology Center, Jiangsu Provincial Public Security Department Physical Evidence Identification Center
Center, Hunan Provincial Public Security Department Physical Evidence Identification Center.
The main drafters of this document. Xu Zizhen, Liu Hua, Qiao Jing, Yan Jin, Zhang Qianshang, Zhang Xudong, Wu Hai, Qin Shiyang, Liu Yongtao, Yuan Zengping.
Forensic science suspects 5F-AMB and 5F-AMB in drugs
5F-APINACA inspection
Liquid Chromatography and Liquid Chromatography-Mass Spectrometry
1 Scope
This document describes N-(1-methoxycarbonyl-2-methylpropyl)-1-(5-fluoropentyl)indazole-3-formyl in suspected narcotics in the field of forensic science
Liquid Chromatography-Mass Spectrometry (LC-
MS) qualitative testing method and liquid chromatography (LC) quantitative testing method.
This document is applicable to the qualitative and quantitative analysis of 5F-AMB and 5F-APINACA in suspected drugs in the field of forensic science.
2 Normative reference documents
The contents of the following documents constitute essential provisions of this document through normative references in the text. Among them, the dated quotations
For undated referenced documents, only the version corresponding to that date applies to this document; for undated referenced documents, the latest version (including all amendments) applies to
this document.
GB/T 6682 Specifications and test methods for water used in analytical laboratories
GB/T 27418 Evaluation and expression of measurement uncertainty
GA/T 122 Toxicological analysis terminology
3 Terms and definitions
The terms and definitions defined in GA/T 122 apply to this document.
4 Principles
Extract 5F-AMB and 5F-APINACA from suspected drugs (see Appendix A for compound information). liquid chromatography-mass spectrometry
The detection method is based on retention time, mass spectrum characteristic ion pairs and ion pair abundance ratio as the basis for qualitative judgment; the liquid chromatography method is used for detection, and the chromatographic method is used for detection.
The peak area was used as the basis for quantitative analysis, and quantitative analysis was carried out using the external standard single point method or the external standard standard curve method.
5 Reagents and materials
5.1 Reagents
The experimental water should comply with the first-class water specified in GB/T 6682.The reagents used in the analysis are all chromatographically pure and include the following
solution.
a) Acetonitrile.
b) methanol.
c) 0.1% formic acid solution (take preparing 1000mL as an example). Measure 1mL of formic acid, dilute with water and adjust to 1000mL.
...
