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Tissue engineering medical device products--Methods for determination of type Ⅰ collagen
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Basic data Standard ID | YY/T 1453-2016 (YY/T1453-2016) | Description (Translated English) | Tissue engineering medical device products--Methods for determination of type �� collagen | Sector / Industry | Medical Device & Pharmaceutical Industry Standard (Recommended) | Classification of Chinese Standard | C35 | Classification of International Standard | 11.040.40 | Word Count Estimation | 18,125 | Date of Issue | 2016-07-29 | Date of Implementation | 2017-06-01 | Issuing agency(ies) | State Food and Drug Administration |
YY/T 1453-2016: Tissue engineering medical device products--Methods for determination of type Ⅰ collagen ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Tissue engineering medical device products - Methods for determination of type I collagen
ICS 11.040.40
C35
People's Republic of China Pharmaceutical Industry Standard
Tissue engineering medical equipment products
Characterization of type Ⅰ collagen
2016-07-29 released
2017-06-01 implementation
State Food and Drug Administration issued
Directory
Preface III
1 Scope 1
2 normative reference document 1
3 Terms and definitions 1
Test method for type Ⅰ collagen
Appendix A (normative) Determination of purity of type Ⅰ collagen 4
Appendix B (normative) Determination of hydroxyproline content 6
Appendix C (normative) Melting point determination 9
Appendix D (normative) Trace element analysis 10
Appendix E (normative appendix) Determination of total sugar content 11
GB/T 1453-2016
Foreword
This standard is drafted in accordance with the rules given in GB/T 1.1-2009.
Please note that some of the contents of this document may involve patents. The issuer of this document does not assume responsibility for the identification of these patents.
And the normative reference in this standard international documents are consistent with the relationship between China's documents are as follows.
GB/T 16886.1-2011 Biological evaluation of medical devices - Part 1. Evaluation and testing in risk management
(ISO 10993-1..2009, IDT).
This standard is proposed by the State Food and Drug Administration.
This standard by the National Surgical Implant and Orthopedic Equipment Standardization Technical Committee Organizational Engineering Medical Device Products Subcommittee
(SAC/TC110/SC3).
The drafting unit of this standard. China Food and Drug Administration Research Institute.
The main drafters of this standard. Ke Linnan, Fang Yu, Fu Bufang, Wang Jian, Huang Yuanli, Duan Xiaojie, Chen Dandan, Feng Xiaoming, Wang Chunren.
GB/T 1453-2016
Tissue engineering medical equipment products
Characterization of type Ⅰ collagen
1 Scope
This standard specifies the test methods for the preparation of type I collagen for tissue engineering medical device products. This type of prescription is prescribed by this standard
Collagen includes I derived from tissue, such as skin, tendons, bones, etc., extracted, isolated and purified, or other sources
Type collagen.
2 normative reference documents
The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article
Pieces. For undated references, the latest edition (including all modifications) applies to this document.
Food safety - Determination of total arsenic and inorganic arsenic in national standard foodstuffs GB 5009.11-2014
Food safety - Determination of total mercury and organic mercury in national foodstuffs GB 5009.17-2014
GB/T 16886.1 Biological evaluation of medical devices - Part 1. Evaluation and testing in risk management (ISO 10993-1,
IDT)
GB/T 22223-2008 Determination of total fat, saturated fats (acids), unsaturated fats (acids) in food - Hydrolysis - Gas phase color
Spectrum method
Pharmacopoeia of the People's Republic of China (2015)
3 terms and definitions
The following terms and definitions apply to this document.
3.1
Type Ⅰ collagen type Ⅰcolagen
The most abundant collagen protein, which is expressed in the mammalian tissue by the COL1A1 gene encoding the alpha chain and the COL1A2 gene,
In fibrous collagen.
Note 1. The peptide chain of type I collagen consists of repeating glycine-XY (proline often occupies X-position, hydroxyproline occupies Y position) amino acid sequence.
Type Ⅰ collagen is rich in glycine (Gly), L-alanine (L-Ala), L-proline (L-Pro) and 4-hydroxyproline (4-Hypro)
And does not contain L-tryptophan (L-Try).
Note 2. Collagen has three alpha chains formed by three helices. In the case of heating (eg, above 60 ° C) the collagen α chain triple helix structure is irreversible
Denatured into a single alpha chain and some beta and gamma bands (ie gelatin).
Note 3. often associated with type Ⅰ collagen type Ⅲ collagen and Ⅴ collagen, in addition to non-collagen-like proteins such as elastin and other structural molecules (amino
Polysaccharides, lipoproteins and glycoprotein complexes).
3.2
Exogenous factor adventitiousagents
Contaminants present in type I collagen, including bacteria, fungi, mycoplasma and exogenous viruses. These substances may be inadvertently
The ground is introduced into the production process and the final product.
GB/T 1453-2016
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