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YS/T 956.1-2014 English PDF

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YS/T 956.1-2014: Chemical analysis method of gold and germanium alloys. Part 1: Determination of germanium content. Inductively coupled plasma atomic emission specitrometry
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YS/T 956.1-2014English159 Add to Cart 3 days [Need to translate] Chemical analysis method of gold and germanium alloys. Part 1: Determination of germanium content. Inductively coupled plasma atomic emission specitrometry Valid YS/T 956.1-2014

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Basic data

Standard ID YS/T 956.1-2014 (YS/T956.1-2014)
Description (Translated English) Chemical analysis method of gold and germanium alloys. Part 1: Determination of germanium content. Inductively coupled plasma atomic emission specitrometry
Sector / Industry Nonferrous Metallurgy Industry Standard (Recommended)
Classification of Chinese Standard H68
Classification of International Standard 70.120.99
Word Count Estimation 6,623
Date of Issue 10/14/2014
Date of Implementation 4/1/2015
Quoted Standard YS/T 371
Regulation (derived from) People's Republic of China Ministry of Industry and Information Technology Notice 2014 No. 63; Industry Standard Filing Notice 2014 No. 12 (Overall No. 180)
Issuing agency(ies) Ministry of Industry and Information Technology
Summary This Standard specifies the determination of the amount of germanium gold-germanium alloy. This section applies to the determination of gold-germanium alloy of germanium content. Determination of the range of 0.50% to 5.00%.

YS/T 956.1-2014: Chemical analysis method of gold and germanium alloys. Part 1: Determination of germanium content. Inductively coupled plasma atomic emission specitrometry


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Chemical analysis method of gold and germanium alloys Part 1. Determination of germanium content Inductively coupled plasma atomic emission specitrometry ICS 77.120.99 H68 People's Republic of China Nonferrous Metals Industry Standard Gold-germanium alloys - Determination of germanium content. Part 1 Inductively Coupled Plasma Atomic Emission Spectrometry Part 1. Determinationofgermaniumcontent- Issued on. 2014-10-14 2015-04-01 implementation Ministry of Industry and Information Technology of the People's Republic of China released

Foreword

YS/T 956 "gold-germanium alloy chemical analysis method" is divided into two parts. --- Part 1. germanium content - Inductively coupled plasma atomic emission spectrometry; --- Part 2. Determination of germanium content of potassium iodate potentiometric titration. This section YS/T Part 1 956. This section drafted in accordance with GB/T 1.1-2009 given rules. The non-ferrous metal part by the National Standardization Technical Committee (SAC/TC243) centralized. This section is responsible for drafting unit. Your research Platinum Ltd., your research resources (Yi door) Limited. This section participated in the drafting unit. China Nonferrous Metals Industry Standards and Metrology Quality Research Institute, Northwest Nonferrous Metal Research Institute, Beijing Institute of Mining and Metallurgy Study General Hospital, Beijing Nonferrous Metal Research Institute, Guangzhou Nonferrous Metal Research Institute. The main drafters of this section. Li Guangli, Gan Jian Zhuang, to Lei, Zhu Wuxun, Liu, He Jiao, Fang Haiyan, Giulia, Xie Hong Chao, Yu Fengshan, Li Na, Lu Ni, Feng advanced Wanghao Ying, Chen Xiaolan, Xiong Xiaoyan, Li Bo. Gold-germanium alloys - Determination of germanium content. Part 1 Inductively Coupled Plasma Atomic Emission Spectrometry

1 Scope

This section YS/T 956 specifies the method for the determination of germanium content of gold-germanium alloy. This section applies to the determination of gold-germanium alloy of germanium content. Determination of the range of 0.50% to 5.00%.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document. 371 precious metal alloys - General rules and regulations YS/T

3 Method summary

Samples with hydrochloric acid, hydrogen peroxide in the teflon digestion tank exploded in a closed room. Au (Ⅲ) with hydrazine elemental Au, in Hydrochloric acid medium, inductively coupled plasma spectrometry, mass fraction of germanium calculated.

4 Reagents and materials

Unless otherwise indicated, this part of the reagents and materials shall comply with the provisions of YS/T 371's. 4.1 Hydrogen peroxide (30% volume fraction). 4.2 hydrochloric acid (ρ = 1.19g/mL). 4.3 hydrochloride (14). 4.4 hydrochloride (19). 4.5 hydrazine monohydrate (19). 4.6 Sodium hydroxide solution (50g/L). 4.7 purity argon gas (φAr≥99.99%). 4.8 Germanium standard stock solution. Weigh 0.2000g metal germanium (mass fraction of not less than 99.99%), placed in 250mL beaker, add 10mL of hydrogen peroxide (4.1), 2mL sodium hydroxide solution (4.6), cover the surface of the dish, was dissolved in a hot plate < 100 ℃, additional hydrogen peroxide, Until completely dissolved. Remove, rinse the beaker and watch glass wall, into the 200mL volumetric flask, dilute to the mark with hydrochloric acid solution (4.3) Degree, and mix. 1mL solution containing 1mg germanium. 4.9 Teflon digestion tank volume 30mL.

5 Instruments

Inductively coupled plasma atomic emission spectrometer. Under optimum working conditions for those who can reach the following indicators can be used.

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