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YS/T 938.2-2013 English PDF

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YS/T 938.2-2013: Chemical analysis methods of gold alloys and palladium alloys for dental ceramic restoration. Part 2: Determination of palladium content. Dimethylglyoxime gravimetry
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YS/T 938.2-2013English159 Add to Cart 3 days [Need to translate] Chemical analysis methods of gold alloys and palladium alloys for dental ceramic restoration. Part 2: Determination of palladium content. Dimethylglyoxime gravimetry Valid YS/T 938.2-2013

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Standard similar to YS/T 938.2-2013

GB/T 17472   GB/T 17473.2   GB/T 17473.1   YS/T 938.3   YS/T 938.4   YS/T 938.1   

Basic data

Standard ID YS/T 938.2-2013 (YS/T938.2-2013)
Description (Translated English) Chemical analysis methods of gold alloys and palladium alloys for dental ceramic restoration. Part 2: Determination of palladium content. Dimethylglyoxime gravimetry
Sector / Industry Nonferrous Metallurgy Industry Standard (Recommended)
Classification of Chinese Standard H68
Classification of International Standard 77.120.99
Word Count Estimation 6,664
Regulation (derived from) Ministry of Industry and Information Technology Bulletin No. 52, 2013; industry standard for filing Notice No. 1 of 2014 (No. 169 overall)
Issuing agency(ies) Ministry of Industry and Information Technology
Summary This standard specifies the porcelain dental restoration and the determination of the amount of palladium-based alloys with gold base. This standard applies to repair dental porcelain base with gold and palladium-based alloys of palladium content. Measuri

YS/T 938.2-2013: Chemical analysis methods of gold alloys and palladium alloys for dental ceramic restoration. Part 2: Determination of palladium content. Dimethylglyoxime gravimetry


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Chemical analysis methods of gold alloys and palladium alloys for dental ceramic restoration Part 2. Determination of palladium content Dimethylglyoxime gravimetry ICS 77.120.99 H68 People's Republic of China Nonferrous Metals Industry Standard Porcelain dental restoration with gold-based alloys and palladium-based analysis Part 2. Determination of the amount of palladium Dimethylglyoxime gravimetric method restoration- Part 2. Determinationofpaladiumcontent- Issued on. 2013-10-17 2014-03-01 implementation Ministry of Industry and Information Technology of the People's Republic of China released

Foreword

YS/T 938 "dental gold PFM group and palladium-based alloy chemical analysis method" is divided into four parts. --- Part 1. determination of gold by weight of sodium nitrite reduction method; --- Part 2. Determination of the amount of palladium dimethylglyoxime gravimetric method; --- Part 3. Determination of the amount of silver by flame atomic absorption spectrometry and potentiometric titration; --- Part 4. Inductively coupled plasma atomic gold, platinum, palladium, copper, tin, indium, zinc, gallium, beryllium, iron, manganese, lithium amount of emitted light Spectroscopy. This section YS/T 938 Part 2. This section drafted in accordance with GB/T 1.1-2009 given rules. The non-ferrous metal part by the National Standardization Technical Committee (SAC/TC243) centralized. This section is responsible for drafting unit. Beijing Nonferrous Metal Research Institute, China Nonferrous Metals Industry Institute of Standards and Metrology and Quality. Participated in the drafting of this section. Beijing Mining Research Institute, Guangzhou Nonferrous Metal Research Institute, Xuzhou Flexcomm New Material Technology Company Limited Division, the China Nonferrous Guilin Research Institute of Geology and Minerals Co. Ltd., Fujian Zijin Mining and Metallurgy Testing Technology Limited. The main drafters of this section. Liu Bing, Zang Muwen, Li Na, to Lei, Zhang Li, Wang Haoying, Chen Xiaolan, Yufeng Shan Hu Zhen Zhen, Liu hair, Mary, Redevex school, Xu Chaoxiu, Fang. Porcelain dental restoration with gold-based alloys and palladium-based analysis Part 2. Determination of the amount of palladium Dimethylglyoxime gravimetric method

1 Scope

This section YS/T 938 provides for dental porcelain repair method for the determination of gold and palladium-based alloys base amount of palladium. This section applies to dental porcelain restoration with gold-based and palladium-based alloys of palladium contents. Measurement range. 15.00% - 60.00%.

2 Method summary

Mixing the sample with hydrochloric acid, nitric acid dissolved. After precipitation of silver chloride in addition to silver, in dilute hydrochloric acid medium to precipitate palladium dimethylglyoxime. Drying Shen Lake, constant weight, and calculate the mass fraction of palladium.

3 Reagents and materials

Unless otherwise specified, the reagents were analytical reagent solution preparation and analysis are secondary distilled water or equivalent purity test Room with water. 3.1 hydrochloric acid (ρ = 1.19g/mL). 3.2 nitric acid (ρ = 1.42g/mL). 3.3 mixed acid. hydrochloric acid (3.1) and nitrate (3.2) in a volume ratio 40︰7 mixed preparation. 3.4 hydrochloride (199). 3.5 hydrochloride (11). 3.6 dimethylglyoxime in ethanol (10g/L). Weigh 1g diacetyldioxime, dissolved in 100mL ethanol solution and mix. 3.7 G4 glass frit funnel (particle size 3μm ~ 4μm).

4 Sample

Sample (sheet) is processed into crushed particles with acetone to remove oil, washed with water, dried and mixed. Step 5 Analysis 5.1 Sample Table 1 sample was weighed, accurate to 0.0001g. Table 1 Sample volume Palladium mass fraction /% sample weight/g 15 to 30 0.20 > 30 to 60 0.10