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YS/T 871-2023 English PDF

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YS/T 871-2023: (Chemical analysis method of pure aluminum Determination of trace impurity element content Glow discharge mass spectrometry)
Status: Valid

YS/T 871: Evolution and historical versions

Standard IDContents [version]USDSTEP2[PDF] delivered inStandard Title (Description)StatusPDF
YS/T 871-2023English179 Add to Cart 3 days [Need to translate] (Chemical analysis method of pure aluminum Determination of trace impurity element content Glow discharge mass spectrometry) Valid YS/T 871-2023
YS/T 871-2013English319 Add to Cart 3 days [Need to translate] Chemical analysis of high purity aluminium. Determination of trace impurities. Glow discharge mass spectrometry Obsolete YS/T 871-2013

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Basic data

Standard ID YS/T 871-2023 (YS/T871-2023)
Description (Translated English) (Chemical analysis method of pure aluminum Determination of trace impurity element content Glow discharge mass spectrometry)
Sector / Industry Nonferrous Metallurgy Industry Standard (Recommended)
Classification of Chinese Standard H13
Classification of International Standard 77.120.40
Word Count Estimation 8,871
Date of Issue 2023-12-20
Date of Implementation 2024-07-01
Issuing agency(ies) Ministry of Industry and Information Technology
Summary This standard specifies the method for the determination of trace impurity elements in pure aluminum. This standard is applicable to the determination of trace impurity element content in pure aluminum. The measuring range of sulfur and chlorine is 0.05mg/kg~10.0mg/kg, and the measuring range of other elements is 0.005mg/kg~10.0mg/kg.

YS/T 871-2013: Chemical analysis of high purity aluminium. Determination of trace impurities. Glow discharge mass spectrometry


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Chemical analysis of high purity aluminium. Determination of trace impurities. Glow discharge mass spectrometry ICS 77.120.40 H13 People's Republic of China Nonferrous Metals Industry Standard Chemical analysis methods of high purity aluminum Determination of trace elements Glow Discharge Mass Spectrometry Issued on. 2013-04-25 2013-09-01 implementation Ministry of Industry and Information Technology of the People's Republic of China released

Foreword

This standard was drafted in accordance with GB/T 1.1-2009 given rules. This standard by the national non-ferrous metals Standardization Technical Committee (SAC/TC243) centralized. This standard was drafted. Beijing Nonferrous Metal Research Institute, public and Xinjiang Co., Ltd., Jinchuan New Material Technology Co., Ltd., Shandong Yankuang Light Alloy Co., Ltd. The main drafters of this standard. Li Ai Chang, Liu Hong, Li Jidong, Sun Zeming, Liu Ying, Tao, Xiaoli Mei, Zhou Wei, SONG Dai Zhenzhen, Qinfang Lin, Qiu Ping. Chemical analysis methods of high purity aluminum Determination of trace elements Glow Discharge Mass Spectrometry

1 Scope

This standard specifies the use of high-quality resolution Test Method for Determination of trace elements in high-purity aluminum glow discharge mass spectrometry. This standard applies to the determination of trace elements in high aluminum content. Determination of the elements in the range of 5.0 × 10-7% ~ 1.0 × 10-3% (Ω%).

2 Method summary

The specimen as a cathode is mounted to the plasma discharge chamber, an inert gas (argon) at high pressure generated from the ionized Son hit the sample surface to make it happen sputtering, sputtered from the surface of the sample out of the atom is ionized by double focusing magnetic sector mass spectrometer Focused ion beam is, in turn, is collected by a mass spectrometer detector. Each element in the mass number of scanning points and impose a preset integration time phase Should peak integration, the resulting area is the peak intensity. According to formula (1) is calculated by the instrument software impurity element content.

3 Reagents and materials

3.1 ethanol (ρ = 0.789g/mL), pure class distinctions. 3.2 hydrochloric acid (ρ = 1.19g/mL), pure class distinctions. 3.3 hydrochloride (11). Nitrogen 3.4 [ω (N2)] ≥99.99%. 3.5 Argon [ω (Ar)] ≥99.99%. 3.6 deionized water. resistivity required to achieve 18.2MΩ · cm. 3.7 standard high purity materials. conditions permit, the use of high purity standard RSG relative sensitivity factor RSFx measured elements.

4 Instrument

4.1 high resolution glow discharge mass spectrometer (GDMS). mass resolution up to 9000. 4.2 machining equipment, enables the sample and reference samples into the desired geometry and a smooth surface.

5 Sample

5.1 with uniform and representative sample. 5.2 Sample should not take the surface of the base material, will be the bulk sample preparation, it requires at least a glow discharge for a smooth plane; sample Size requirements can be placed in a glow discharge specimen holder cavity and its smooth surface can cover the sample holder on the discharge hole; specimen thickness requirements After the sample into sample holder does not affect the ion source chamber is closed.

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