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YS/T 438.5-2013 English PDF

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YS/T 438.5-2013: Methods for physical performance determination of Sandy alumina. Part 5: X-ray diffraction spectrum method for detemination of α-alumina content
Status: Valid

YS/T 438.5: Evolution and historical versions

Standard IDContents [version]USDSTEP2[PDF] delivered inStandard Title (Description)StatusPDF
YS/T 438.5-2013English159 Add to Cart 3 days [Need to translate] Methods for physical performance determination of Sandy alumina. Part 5: X-ray diffraction spectrum method for detemination of α-alumina content Valid YS/T 438.5-2013
YS/T 438.5-2001English199 Add to Cart 2 days [Need to translate] Methods for physical performance determination of sandy alumina. Determination of α-alumina content. X-ray diffraction spectrum method Obsolete YS/T 438.5-2001

PDF similar to YS/T 438.5-2013


Standard similar to YS/T 438.5-2013

YS/T 581.15   GB/T 1425   GB/T 351   YS/T 438.2   YS/T 438.3   YS/T 438.1   

Basic data

Standard ID YS/T 438.5-2013 (YS/T438.5-2013)
Description (Translated English) Methods for physical performance determination of Sandy alumina. Part 5: X-ray diffraction spectrum method for detemination of ��-alumina content
Sector / Industry Nonferrous Metallurgy Industry Standard (Recommended)
Classification of Chinese Standard H21
Classification of International Standard 71.100.10
Word Count Estimation 6,630
Older Standard (superseded by this standard) YS/T 438.5-2001
Regulation (derived from) Ministry of Industry and Information Technology Bulletin 2013 No. 23; industry standard filing Notice 2013 No. 7 (No. 163 overall)
Issuing agency(ies) Ministry of Industry and Information Technology
Summary This standard specifies the X-ray diffraction method sandy alumina in ��-Al2O3 content approach. This standard applies to sandy alumina ��-Al2O3 content. Measuring range: �� 20. 0%.

YS/T 438.5-2013: Methods for physical performance determination of Sandy alumina. Part 5: X-ray diffraction spectrum method for detemination of α-alumina content


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Methods for physical performance determination of Sandy alumina Part 5. X-ray diffraction spectrum method for detemination of α-alumina content ICS 71.100.10 H21 People's Republic of China Nonferrous Metals Industry Standard Replacing YS/T 438.5-2001 Sandy alumina determination of physical performance Part 5. X- ray diffraction method α- alumina content Part 5. X-raydiffractionspectrummethodfordeterminationof α-aluminacontent Issued on. 2013-04-25 2013-09-01 implementation Ministry of Industry and Information Technology of the People's Republic of China released

Foreword

YS/T 438 "sandy alumina determination of physical performance" is divided into five sections. --- Part 1. Determination of particle size distribution by sieving; --- Part 2. Determination of the abrasion index; --- Part 3. Determination of angle of repose; --- Part 4. Determination of specific surface area; --- Part 5. Determination of α- alumina content of X- ray diffraction. This is Part 5. The partial replacement of YS/T 438.5-2001 "Determination of α- alumina content of sandy alumina determination of physical performance X-ray diffraction method." This part is the "determination of α- alumina content of sandy alumina determination of physical performance X-ray diffraction method" YS/T 438.5-2001 of Revised, compared with YS/T 438.5-2001, the main changes are as follows. --- Increased reagent Chapter 3; --- Increased precision; --- Increase the content quality assurance and control. This section drafted in accordance with GB/T 1.1-2009 given rules. The non-ferrous metal part by the National Standardization Technical Committee (SAC/TC243) centralized. This part mainly drafted by. Aluminum Corporation of China Guangxi Branch, Luoyang Xiangjiang Wanji Aluminum Co., Ltd. The main drafters of this section. Yang Yun screen, the more Liang Bin, Luo Xiangning, Liu Yong, Zhang Feng flowers, Jiang Wei. This part of the standard replaces the previous editions are. --- YS/T 438.5-2001. Sandy alumina determination of physical performance Part 5. X- ray diffraction method α- alumina content

1 Scope

This section provides a method for determining X- ray diffraction sandy alumina content of the α-Al2O3. This section applies to the determination of sandy alumina content in α-Al2O3. Measuring range. ≤20.0%.

2 Method summary

In the same diffraction conditions were samples and standard samples (012) crystal face of the integrated intensity values measured in accordance with standard samples containing the α-Al2O3 The amount of the sample to calculate the content of α-Al2O3.

3 Reagents

3.1 high purity alumina (99.99%). 3.2 aluminum hydroxide. 3.3 ethanol. 3.4 corundum crucible (100mL).

4 Instrument

4.1 agate mortar. 4.2 X- ray diffraction. General Instrument stability better than 0.5%, work on indicators see Appendix A. 4.3 Oven. Maximum operating temperature 300 ℃ ± 5 ℃. 4.4 high-temperature furnace. maximum operating temperature of 1600 ℃ ± 5 ℃.

5 Sample Preparation

5.1 The high purity alumina (3.1) in 100mL corundum crucible (3.4) was packed to 2/3, at 1450 ℃ ± 20 ℃ baking after 6h The resulting alumina regarded as containing α-Al2O3 (100.0%). 5.2 aluminum hydroxide (3.2) placed in 100mL corundum crucible (3.4) was packed to 2/3, after 700 ℃ ± 20 ℃ baking 4h prepared Alumina deemed free of α-Al2O3. 5.3 A sample (5.1), (5.2) drying 2h at 105 ℃ ± 5 ℃, dubbed by the mass ratio α-Al2O3 content of 0,5.0%, 10.0%, respectively, 15.0%, 20.0% of the standard sample, and mix thoroughly ground to a particle size of less than 10μm.

6 measuring step

6.1 adjusting X diffractometer (4.2) to reach a steady state measurement requirements.

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