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YS/T 226.13-2009: Methods for chemical analysis of selenium. Part 13: Determination of siliver, aluminum, arensic, boron, mercury, bismuth, copper, cadmium, iron, gallium, indium, magnesium, nickel, lead, silicon, antimony, tin, tellurium, titanium and zinc content. Induct YS/T 226.13: Evolution and historical versions
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| YS/T 226.13-2009 | English | 349 |
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Methods for chemical analysis of selenium. Part 13: Determination of siliver, aluminum, arensic, boron, mercury, bismuth, copper, cadmium, iron, gallium, indium, magnesium, nickel, lead, silicon, antimony, tin, tellurium, titanium and zinc content. Induct
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YS/T 226.13-2009
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| YS/T 226.13-1994 | English | 199 |
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(Determination of the amount of lead selenide (polarography))
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YS/T 226.13-1994
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Basic data | Standard ID | YS/T 226.13-2009 (YS/T226.13-2009) | | Description (Translated English) | Methods for chemical analysis of selenium. Part 13: Determination of siliver, aluminum, arensic, boron, mercury, bismuth, copper, cadmium, iron, gallium, indium, magnesium, nickel, lead, silicon, antimony, tin, tellurium, titanium and zinc content. Induct | | Sector / Industry | Nonferrous Metallurgy Industry Standard (Recommended) | | Classification of Chinese Standard | H17 | | Classification of International Standard | 77.120.99 | | Word Count Estimation | 10,175 | | Date of Issue | 2009-12-04 | | Date of Implementation | 2010-06-01 | | Older Standard (superseded by this standard) | YS/T 226.3-1994; YS/T 226.6-1994; YS/T 226.8-1994; YS/T 226.13-1994 | | Regulation (derived from) | MIIT [2009] No. 66 | | Issuing agency(ies) | Ministry of Industry and Information Technology | | Summary | This standard specifies the selenium silver, aluminum, arsenic, boron, mercury, bismuth, copper, cadmium, iron, gallium, indium, magnesium, nickel, lead, silicon, antimony, tin, tellurium, titanium, zinc volume method. This standard applies to selenium silver, aluminum, arsenic, boron, mercury, bismuth, copper, cadmium, iron, gallium, indium, magnesium, nickel, lead, silicon, antimony, tin, tellurium, titanium, zinc content. | YS/T 226.13-2009: Methods for chemical analysis of selenium. Part 13: Determination of siliver, aluminum, arensic, boron, mercury, bismuth, copper, cadmium, iron, gallium, indium, magnesium, nickel, lead, silicon, antimony, tin, tellurium, titanium and zinc content. Induct
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Methods for chemical analysis of selenium.Part 13. Determination of siliver, aluminum, arensic, boron, mercury, bismuth, copper, cadmium, iron, gallium, indium, magnesium, nickel, lead, silicon, antimony, tin, tellurium, titanium and zinc content.Induct
ICS 77.120.99
H17
People's Republic of China Nonferrous Metals Industry Standard
Replacing YS/T 226.3-1994
YS/T 226.6-1994
YS/T 226.8-1994
YS/T 226.13-1994
Chemical analysis of selenium
Part 13. silver, aluminum, arsenic, boron, mercury, bismuth, copper, cadmium,
Iron, gallium, indium, magnesium, nickel, lead, silicon, antimony, tin, tellurium, titanium,
Determination of zinc content
Inductively Coupled Plasma Mass Spectrometry
Issued on. 2010-06-01 2009-12-04 implementation
Ministry of Industry and Information Technology of the People's Republic of China released
Foreword
YS/T 226 "selenium chemical analysis method" is divided into 13 parts.
--- Part 1. Determination of bismuth content - Hydride Generation - Atomic Fluorescence Spectrometry
--- Part 2. Determination of antimony content Hydride Generation - Atomic Fluorescence Spectrometry
--- Part 3. Determination of aluminum content Chromazurol S- cetylpyridinium bromide spectrophotometric method
--- Part 4. Determination of mercury content of dithizone - CTC colorimetric titration
--- Part 5. Determination of the amount of silicon silicon molybdenum blue spectrophotometry
--- Part 6. Determination of sulfur content symmetrical diphenyl semicarbazide spectrophotometry
--- Part 7. Determination of magnesium content - Flame atomic absorption spectrometry
--- Part 8. Determination of copper content - Flame atomic absorption spectrometry
--- Part 9. Determination of iron content by flame atomic absorption spectrometry
--- Part 10. Determination of nickel content by flame atomic absorption spectrometry
--- Part 11. Determination of lead content by flame atomic absorption spectrometry
--- Part 12. Determination of the amount of selenium sodium thiosulfate volumetric method
--- Part 13. silver, aluminum, arsenic, boron, mercury, bismuth, copper, cadmium, iron, gallium, indium, magnesium, nickel, lead, silicon, antimony, tin, tellurium, titanium, zinc content of electricity
Inductively coupled plasma mass spectrometry
This section YS/T Part 13 226.
The partial replacement of YS/T 226.3-1994 "selenium Determination of tin content Phenylfluorone - bromo cetyltrimethylammonium absorptiometry"
YS/T 226.6-1994 "selenium arsenic content determination of arsenic molybdenum blue spectrophotometric method", YS/T 226.8-1994 "selenium in determining the amount of boron times
Methylene blue photometric method "and YS/T 226.13-1994" selenium and tellurium in determining the amount of oscillopolarographic law. " And YS/T 226.3-1994,
YS/T 226.6-1994, YS/T 226.8-1994 and YS/T 226.13-1994 compared, this section there are major changes as follows.
--- Using the ICP-MS method for the determination.
--- Expand the scope of determination of elements, including silver, aluminum, arsenic, boron, mercury, bismuth, copper, cadmium, iron, gallium, indium, magnesium, nickel, lead, silicon, antimony, tin, tellurium, titanium,
The amount of zinc and the like.
The non-ferrous metal part by the National Standardization Technical Committee and centralized.
This section is responsible for drafting unit. Jinchuan Group Limited.
This section is drafted. Beijing Nonferrous Metal Research Institute.
Participated in the drafting of this section. Jinchuan Group Ltd, China Aluminum Henan branch.
The main drafters of this section. Liu Ying, Liu Hong, Gao Yan, Wang Ke Zhen, high Zexiang, ORTHOPAEDICS.
Chemical analysis of selenium
Part 13. silver, aluminum, arsenic, boron, mercury, bismuth, copper, cadmium,
Iron, gallium, indium, magnesium, nickel, lead, silicon, antimony, tin, tellurium, titanium,
Determination of zinc content
Inductively Coupled Plasma Mass Spectrometry
1 Scope
YS/T 226 This part provides selenium silver, aluminum, arsenic, boron, mercury, bismuth, copper, cadmium, iron, gallium, indium, magnesium, nickel, lead, silicon, antimony, tin, tellurium,
Titanium, zinc content.
This section applies to silver, aluminum, arsenic, boron, mercury, bismuth, copper, cadmium, iron, gallium, indium, magnesium, nickel, lead, silicon, antimony, tin, tellurium, titanium, zinc contents in selenium.
Measuring range. measuring range of the elements shown in Table 1.
Table 1 element Measuring range
Element measurement range/measuring range of elements% /%
Ag 0.00005 ~ 0.0010 In 0.00005 ~ 0.0010
Al 0.00005 ~ 0.0010 Mg 0.00005 ~ 0.0010
As 0.00005 ~ 0.0010 Ni 0.00005 ~ 0.0010
B 0.00010 ~ 0.0010 Pb 0.00005 ~ 0.0010
Hg 0.00005 ~ 0.0010 Si 0.00010 ~ 0.0010
Bi 0.00005 ~ 0.0010 Sb 0.00005 ~ 0.0010
Cu 0.00005 ~ 0.0010 Sn 0.00005 ~ 0.0010
Cd 0.00005 ~ 0.0010 Te 0.00005 ~ 0.0010
Fe 0.00005 ~ 0.0010 Ti 0.00005 ~ 0.0010
Ga 0.00005 ~ 0.0010 Zn 0.00005 ~ 0.0010
2 Method summary
The sample is dissolved in nitric acid in acid medium, using ICP-MS mass spectrometry direct determination. All standard method to correct measured.
3 Reagents
The standard water is deionized water, conductivity is not more than 6.67 × 10-2μS · cm
-1.
Nitrate 3.1 (ρ1.42g/mL).
3.2 hydrochloride (ρ1.19g/mL).
3.3 hydrofluoric acid, mos level.
3.4 pure water (resistance > 18MΩ · cm).
3.5 silver standard stock solution. Weigh 1.0000g silver [silver mass fraction ≥99.9%], placed in 300mL beaker, add 10mL nitrate
Acid (3.1), low dissolved, heating to remove nitrogen oxides, remove the cooled and transferred to 1000mL volumetric flask 100mL nitric acid
(3.1), dilute to the mark and mix. 1mL solution containing 1mg silver.
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