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YS/T 1165-2016 English PDF

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YS/T 1165-2016: Determination method for copper, manganese, chromium, cobalt, nickel, vanadivin, zinc, lead, iron, magnesium, indium and arsenic content in high pure germanium tetrachloride. Inductively coupled plasma mass spectrometry method
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YS/T 1165-2016English279 Add to Cart 3 days [Need to translate] Determination method for copper, manganese, chromium, cobalt, nickel, vanadivin, zinc, lead, iron, magnesium, indium and arsenic content in high pure germanium tetrachloride. Inductively coupled plasma mass spectrometry method   YS/T 1165-2016

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Basic data

Standard ID YS/T 1165-2016 (YS/T1165-2016)
Description (Translated English) Determination method for copper, manganese, chromium, cobalt, nickel, vanadivin, zinc, lead, iron, magnesium, indium and arsenic content in high pure germanium tetrachloride. Inductively coupled plasma mass spectrometry method
Sector / Industry Nonferrous Metallurgy Industry Standard (Recommended)
Classification of Chinese Standard H17
Classification of International Standard 77.040
Word Count Estimation 8,845
Date of Issue 2016-07-11
Date of Implementation 2017-01-01
Regulation (derived from) Notice of the Ministry of Industry and Information Technology (2016 No. 37)
Issuing agency(ies) Ministry of Industry and Information Technology
Summary This standard specifies the determination method of copper, manganese, chromium, cobalt, nickel, vanadium, zinc, lead, iron, magnesium, indium and arsenic in high purity antimony tetrachloride.

YS/T 1165-2016: Determination method for copper, manganese, chromium, cobalt, nickel, vanadivin, zinc, lead, iron, magnesium, indium and arsenic content in high pure germanium tetrachloride. Inductively coupled plasma mass spectrometry method



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Determination method for copper, manganese, chromium, cobalt, nickel, vanadivin, zinc, lead, iron, magnesium, indium and arsenic content in high pure germanium tetrachloride. Inductively coupled plasma mass spectrometry method ICS 77.040 H17 People's Republic of China Nonferrous Metals Industry Standard High purity antimony tetrachloride in copper, manganese, chromium, cobalt, nickel, vanadium, Determination of zinc, lead, iron, magnesium, indium and arsenic Inductively coupled plasma mass spectrometry Released on.2016-07-11 2017-01-01 implementation Ministry of Industry and Information Technology of the People's Republic of China

Foreword

This standard was drafted in accordance with the rules given in GB/T 1.1-2009. This standard is proposed and managed by the National Nonferrous Metals Standardization Technical Committee (SAC/TC243). This standard was drafted. National Standard (Beijing) Inspection and Certification Co., Ltd., Yunnan Linyi Xinyuan Industry Co., Ltd., Nanjing Zhonghao Technology limited liability company. The main drafters of this standard. Liu Hong, Li Aizhen, Dong Chaobo, Li Jidong, Sun Zeming, Liu Ying, Pu Shikun, Liu Xinjun. High purity antimony tetrachloride in copper, manganese, chromium, cobalt, nickel, vanadium, Determination of zinc, lead, iron, magnesium, indium and arsenic Inductively coupled plasma mass spectrometry Warning. Personnel using this document should have hands-on experience with formal laboratory work. This standard does not address all possible security issues. It is the responsibility of the user to take appropriate safety and health measures and to ensure compliance with the conditions set by the relevant national regulations.

1 Scope

This standard specifies the determination method of copper, manganese, chromium, cobalt, nickel, vanadium, zinc, lead, iron, magnesium, indium and arsenic in high purity antimony tetrachloride. This standard applies to the determination of copper, manganese, chromium, cobalt, nickel, vanadium, zinc, lead, iron, magnesium, indium and arsenic in high purity antimony tetrachloride. The measurement range (mass fraction) is 1×10-9%~2×10-5%, and iron is determined by dynamic reaction cell mode.

2 Method summary

Under the heating condition, the main body of antimony tetrachloride was volatilized, and the organic matter in the residue was removed by nitric acid, and the inductively coupled plasma mass spectrometry was used. The method directly measures the contents of copper, manganese, chromium, cobalt, nickel, vanadium, zinc, lead, iron, magnesium, indium and arsenic.

3 reagents

Unless otherwise stated, only reagents identified as electronic grades were used in the analysis; the water used was deionized water and the resistivity should be 18.0 MΩ·cm. 3.1 Nitric acid (ρ = 1.42 g/mL). 3.2 Hydrochloric acid (ρ=1.19g/mL). 3.3 Nitric acid (1 1). Configured by nitric acid (3.1). 3.4 Multi-element mixed standard solution A. It is prepared by domestic and foreign certified standard materials that can be traced back to the source. Copper, manganese, chromium, cobalt, The mass concentrations of nickel, vanadium, zinc, lead, iron, magnesium, indium and arsenic are each 1000 μg/mL. 3.5 Mixing standard solution B. Take 10mL of mixed standard solution A (3.4) in a 100mL volumetric flask, add 5mL of nitric acid (3.1), use Dilute the water to the mark and mix. 1 mL of this solution contained 100 μg each of copper, manganese, chromium, cobalt, nickel, vanadium, zinc, lead, iron, magnesium, indium and arsenic. 3.6 Mixing standard solution C. Take 10mL of mixed standard solution B (3.5) in a 100mL volumetric flask, add 5mL of nitric acid (3.1), use Dilute the water to the mark and mix. 1 mL of this solution contained 10 μg each of copper, manganese, chromium, cobalt, nickel, vanadium, zinc, lead, iron, magnesium, indium and arsenic. 3.7 Mixing standard solution D. Take 10mL of mixed standard solution C (3.6) in a 100mL volumetric flask, add 5mL of nitric acid (3.1), use Dilute the water to the mark and mix. 1 mL of this solution contained 1 μg of each of copper, manganese, chromium, cobalt, nickel, vanadium, zinc, lead, iron, magnesium, indium and arsenic. 3.8 铯 internal standard storage solution, 1000μg/mL. provided by the National Standards Research Center. 3.9 铯 internal standard solution A. Take 10mL 铯 internal standard storage solution (3.8) in a 100mL volumetric flask, add 5mL nitric acid (3.1), dilute to the mark with water and mix. 1 mL of this solution contained 100 μg of hydrazine. 3.10 铯 internal standard solution B. Take 10mL 铯 internal standard solution A (3.9) in a 100mL volumetric flask, add 5mL nitric acid (3.1), dilute to the mark with water and mix. 1 mL of this solution contained 10 μg of hydrazine. 3.11 铯 internal standard solution C. Take 10mL 铯 internal standard solution B (3.10) in a 100mL volumetric flask, add 5mL of nitric acid (3.1), dilute to the mark with water and mix. 1 mL of this solution contained μ1 μg.

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