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YC/T 561-2018: Characteristic components of tobacco. Determination of enantiomer ratio of nicotine. High performance liquid chromatography method and ultra performance convergence chromatography-tandem mass spectrometry method
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Characteristic components of tobacco. Determination of enantiomer ratio of nicotine. High performance liquid chromatography method and ultra performance convergence chromatography-tandem mass spectrometry method
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YC/T 561-2018
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Basic data | Standard ID | YC/T 561-2018 (YC/T561-2018) | | Description (Translated English) | Characteristic components of tobacco. Determination of enantiomer ratio of nicotine. High performance liquid chromatography method and ultra performance convergence chromatography-tandem mass spectrometry method | | Sector / Industry | Tobacco Industry Standard (Recommended) | | Classification of Chinese Standard | X87 | | Word Count Estimation | 12,129 | | Date of Issue | 2018-01-18 | | Date of Implementation | 2018-02-01 | | Quoted Standard | GB/T 6682 | | Regulation (derived from) | State-Tobacco-Technology (2018) No. 20; Industry Standard Registration Announcement No. 3 of 2018 (Total No. 219) | | Issuing agency(ies) | State Tobacco Monopoly Administration | YC/T 561-2018: Characteristic components of tobacco. Determination of enantiomer ratio of nicotine. High performance liquid chromatography method and ultra performance convergence chromatography-tandem mass spectrometry method
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Characteristic components of tobacco.Determination of enantiomer ratio of nicotine.High performance liquid chromatography method and ultra performance convergence chromatography-tandem mass spectrometry method
ICS 65.160
X87
Record number. 61389-2018
People's Republic of China tobacco industry standard
Nicotine optical isomer
Proportional determination of high performance liquid chromatography and
Ultra-high performance convergent chromatography-tandem mass spectrometry
Published on.2018-01-18
2018-02-01 implementation
National Tobacco Monopoly Bureau released
Foreword
This standard is drafted in accordance with the rules given in GB/T 1.1-2009 and GB/T.20001.4-2015.
Please note that some of the contents of this document may involve patents. The issuing organization of this document is not responsible for identifying these patents.
This standard was proposed by the State Tobacco Monopoly Bureau.
This standard is under the jurisdiction of the National Tobacco Standardization Technical Committee Cigarette Subcommittee (SAC/TC144/SC1).
This standard was drafted. National Tobacco Quality Supervision and Inspection Center, Shanghai Tobacco Group Co., Ltd., Shanghai New Tobacco Products Research
Research Institute, Yunnan China Tobacco Industry Co., Ltd., Hunan China Tobacco Industry Co., Ltd., Guangxi China Tobacco Industry Co., Ltd., Zhejiang Zhongyan
Industrial Co., Ltd., Shandong Tobacco Quality Supervision and Inspection Station, Sichuan Tobacco Quality Supervision and Inspection Station, Zhengzhou Tobacco Research Institute, Guangdong Middle
Tobacco Industry Co., Ltd., Henan China Tobacco Industry Co., Ltd.
The main drafters of this standard. Hu Qingyuan, Zhang Hongfei, Fei Ting, Hou Hongwei, Chen Huan, Cai Junlan, Wu Da, Pang Yongqiang, Li Xiangyu, Yu Jingjing,
Luo Yanbo, Han Shulei, Fu Yaning, Liu Shaofeng, Yang Jing, Yang Liu, Wang Zhiguo, Tian Yongfeng, Duan Qixing, Li Xiaolan, Ji Lishun, Chen Yongkuan, Tao Xiaoqiu,
Zhu Donglai, Lu Xinbo, Zhu You, Xiong Wei, Yan Dawei, Dai Lu, Wang Bing, Shen Xiaojie, Han Bing, Zhou Yi, Yu Fei, Li Lijun, Tian Haiying, Qin Yanhua,
Yang Ji, Si Xiaoxi, Zhu Ruizhi, Cui Huapeng, Zhao Yang, Qin Yaqiong, Jia Yunqi, Cao Depo, Bie Zhenying, Pang Wei, Wu Jingjing.
Nicotine optical isomer
Proportional determination of high performance liquid chromatography and
Ultra-high performance convergent chromatography-tandem mass spectrometry
1 Scope
This standard specifies the method for the determination and analysis of the proportion of nicotine optical isomers of tobacco characteristic components.
This standard applies to tobacco and tobacco products, electronic cigarette smoke, smokeless tobacco products and other samples of tobacco characteristic components nicotine rotation
For the determination of the proportion of the structure, the gum base type tobacco product can be used for reference. Among them, high performance liquid chromatography is suitable for nicotine optical isomer ratio in samples.
For the routine detection of the example, ultra-high performance convergent-phase chromatography-tandem mass spectrometry is suitable for the confirmatory detection of the proportion of nicotine optical isomers in the sample.
2 Normative references
The following documents are indispensable for the application of this document. For dated references, only the dated version applies to this article.
Pieces. For undated references, the latest edition (including all amendments) applies to this document.
GB/T 6682 Analytical laboratory water specifications and test methods
3 Principle
The nicotine in the sample is extracted with a mixed solution of n-hexane and methanol under an alkaline solution, and the extract is subjected to matrix-dispersed solid phase extraction.
After normalization, the positive-phase liquid chromatography UV detector was used to detect the (S)-(-)-nicotine and tobacco in tobacco and tobacco products by external standard method.
(R)-()-nicotine content, then calculate the proportion of nicotine optical isomers.
4 reagents
Analytical grade or higher reagents should be used unless otherwise specified.
4.1 Water, GB/T 6682, level one.
4.2 Methanol.
4.3 n-hexane.
4.4 Sodium hydroxide.
4.5 5% aqueous sodium hydroxide, weigh 5.0g of sodium hydroxide (4.4), completely dissolved with water (4.1), transferred to 100mL plastic capacity
In the bottle, dilute to the mark with water (4.1).
4.6 n-hexane and methanol solution (volume ratio of 98.2), pipet 20mL of methanol (4.2) into a 1000mL volumetric flask, with n-hexane
(4.3) Make up to the scale.
4.7 Graphitized carbon black (GCB).
4.8 N-propyl ethylenediamine bonded silica gel (PSA).
4.9 Anhydrous magnesium sulfate (MgSO4).
4.10 (S)-(-)-nicotine standard, the purity is not less than 99%.
4.11 (R)-()-nicotine standard, the purity is not less than 99%.
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