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YC/T 540-2016 English PDF

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YC/T 540-2016: Cigarettes. Determination of ethylene oxide and propylene oxide in mainstream cigarette smoke. Gas chromatography-mass spectrometry method
Status: Valid
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YC/T 540-2016English229 Add to Cart 3 days [Need to translate] Cigarettes. Determination of ethylene oxide and propylene oxide in mainstream cigarette smoke. Gas chromatography-mass spectrometry method Valid YC/T 540-2016

PDF similar to YC/T 540-2016


Standard similar to YC/T 540-2016

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Basic data

Standard ID YC/T 540-2016 (YC/T540-2016)
Description (Translated English) Cigarettes. Determination of ethylene oxide and propylene oxide in mainstream cigarette smoke. Gas chromatography-mass spectrometry method
Sector / Industry Tobacco Industry Standard (Recommended)
Classification of Chinese Standard X87
Classification of International Standard 65.160
Word Count Estimation 10,148
Date of Issue 2016-01-23
Date of Implementation 2016-02-15
Quoted Standard GB/T 19609
Regulation (derived from) Industry standard filing notice 2016 No. 3 (total 195)
Issuing agency(ies) State Tobacco Monopoly Administration
Summary This standard specifies the determination of ethylene oxide and propylene oxide in the mainstream smoke of cigarettes by gas chromatography-mass spectrometry. This standard applies to the determination of ethylene oxide and propylene oxide in mainstream cigarette smoke. The limit of quantification of ethylene oxide and propylene oxide in cigarette smoke was 0.10ug/cig, 23.1ng/cig, and the detection limits were 0.029ug/cig, 6.9ng/cig, respectively.

YC/T 540-2016: Cigarettes. Determination of ethylene oxide and propylene oxide in mainstream cigarette smoke. Gas chromatography-mass spectrometry method


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Cigarettes.Determination of ethylene oxide and propylene oxide in mainstream cigarette smoke.Gas chromatography-mass spectrometry method ICS 65.160 X87 Record number. 53109-2016 Tobacco Industry Standard of the People's Republic of China Cigarette in mainstream fumes in ethylene oxide and propylene oxide Determination of Gas Chromatography - Mass Spectrometry Cigarettes-Determination ofethyleneoxideandpropyleneoxideinmainstream 2016-01-23 released 2016-02-15 Implementation State Tobacco Monopoly Bureau released

Foreword

This standard is drafted in accordance with the rules given in GB/T 1.1-2009. Please note that some of the contents of this document may involve patents. The issuer of this document does not assume responsibility for the identification of these patents. This standard is proposed by the State Tobacco Monopoly Bureau. This standard is under the jurisdiction of the National Tobacco Standardization Technical Committee's Subcommittee on Taxes (SAC/TC144/SC1). The drafting of this standard unit. China Tobacco Corporation Zhengzhou Tobacco Research Institute, Fujian Tobacco Industry Co., Ltd., Guangxi tobacco industry has Limited liability company, Hubei tobacco industry limited liability company, Yunnan tobacco industry limited liability company, Gansu tobacco industry limited liability company. The main drafters of this standard. Liu Shaofeng, Qin Yajiong, Xie Wei, Cui Huapeng, Wang Xiaoyu, Sun Xuehui, Jia Yunzhen, Su Mingliang, Xu Aifei, Li Wenjing, Cui Zhuwen, Gao Yuzhen, Xie Fuwei, Xie Yulong, Chen Zhiyan. Cigarette in mainstream fumes in ethylene oxide and propylene oxide Determination of Gas Chromatography - Mass Spectrometry

1 Scope

This standard specifies the determination of ethylene oxide and propylene oxide in the mainstream smoke of cigarettes by gas chromatography-mass spectrometry. This standard applies to the determination of ethylene oxide and propylene oxide in mainstream cigarette smoke. The limit of quantification of ethylene oxide and propylene oxide in the mainstream smoke of the cigarette was 0.10μg/cig, 23.1ng/cig, the detection limit Respectively 0.029 μg/cig, 6.9 ng/cig.

2 normative reference documents

The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article Pieces. For undated references, the latest edition (including all modifications) applies to this document. GB/T 19609 Routine analysis of cigarettes Determination of total particulate matter and tar with a smoking machine

3 principle

The main flue gas particles of the cigarette were captured with a glass fiber filter, and two series absorption vials placed in a dry ice-isopropanol cold trap were used Toluene as the absorption liquid) to capture the mainstream smoke gas phase. The ethylene oxide and propylene oxide were measured by gas chromatography-mass spectrometry Alkane, internal standard method.

4 Reagents and Materials

In addition to the special requirements, should use the analysis of pure or above reagents. 4.1 Toluene Chromatographic purity (or analysis after pure re-use). 4.2 Ethylene oxide standard solution (10mg/mL) Ethylene oxide, purity ≥99.5%. 4.3 Propylene oxide Purity ≥99.5%. 4.4 D6-propylene oxide Purity ≥99.3%.

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