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US$159.00 · In stock Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. SN/T 3368-2012: Determination of phosphorus content in carbon steel and low-middle alloy steel. Phosphomolybdate blue spectrophotometric method Status: Valid
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| SN/T 3368-2012 | English | 159 |
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Determination of phosphorus content in carbon steel and low-middle alloy steel. Phosphomolybdate blue spectrophotometric method
| Valid |
SN/T 3368-2012
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Standard similar to SN/T 3368-2012 SN/T 5268
Basic data | Standard ID | SN/T 3368-2012 (SN/T3368-2012) | | Description (Translated English) | Determination of phosphorus content in carbon steel and low-middle alloy steel. Phosphomolybdate blue spectrophotometric method | | Sector / Industry | Commodity Inspection Standard (Recommended) | | Word Count Estimation | 6,659 | | Quoted Standard | GB/T 602; GB/T 6379.2; GB/T 6682; GB/T 20066 | | Regulation (derived from) | National Quality Inspection (2012) 777; industry standard filing Notice 2013 No. 4 (No. 160 overall) | | Issuing agency(ies) | General Administration of Customs | | Summary | This standard specifies the molybdenum blue spectrophotometric determination of carbon steel, low alloy steel phosphorus content approach. This standard applies to carbon steel, low alloy steel Determination of phosphorus content, determination range of 0 |
SN/T 3368-2012: Determination of phosphorus content in carbon steel and low-middle alloy steel. Phosphomolybdate blue spectrophotometric method ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of phosphorus content in carbon steel and low-middle alloy steel.Phosphomolybdate blue spectrophotometric method
People's Republic of China Entry-Exit Inspection and Quarantine Standards
Determination of carbon steel, low alloy steel phosphorus content
Phosphorus molybdenum blue spectrophotometry
Issued on. 2012-12-12
2013-07-01 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
This standard was drafted in accordance with GB/T 1.1-2009 given rules.
This standard is proposed and managed by the National Certification and Accreditation Administration Committee.
This standard was drafted. Tianjin People's Republic of China Exit Inspection and Quarantine.
The main drafters of this standard. new Hood, Wanghao Yun, Chen Yan, Ann Peng Sheng, Wang Zhaorui, from Madrid.
Determination of carbon steel, low alloy steel phosphorus content
Phosphorus molybdenum blue spectrophotometry
1 Scope
This standard specifies the phosphorus molybdenum blue spectrophotometric determination of carbon steel, low alloy steel phosphorus content approach.
This standard applies to carbon steel, low alloy steel in the determination of phosphorus content was measured in the range of 0.005% to 0.15% carbon, low-alloy steel
0.005% to 0.10%.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
Preparation of standard solution of GB/T 602 Determination of impurities in chemical reagents
GB/T 6379.2 measurement methods and results of Accuracy (trueness and precision) - Part 2. Determine the standard measurement method to repeat
And basic methods of reproduction
Laboratory use specifications and test methods GB/T 6682 Analysis
GB/T 20066 Steel and iron - Sampling and determination of the chemical composition of the sample with a sample preparation method
3 Method summary
Carbon perchloric acid sample dissolution, low alloy steel with nitric acid - hydrochloric acid mixed acid, perchloric acid decomposition sample in sulfuric acid and molybdic acid
Ammonium form a yellow complex with stannous chloride to restore phosphorus molybdenum blue absorbance was measured on a spectrophotometer at the wavelength of 660nm at.
4 Reagents and materials
Unless otherwise indicated, the reagents used were of analytical grade reagent water to comply with two water GB/T 6682 regulations.
4.1 perchloric acid (ρ = 1.67g/mL).
4.2 sulfate (ρ = 1.84g/mL).
4.3 nitric acid (ρ = 1.42g/mL).
4.4 hydrochloric acid (ρ = 1.19g/mL).
4.5 perchloric acid (11).
4.6 sulfate (114).
4.7 sulfate (124).
4.8 nitric acid - mixing hydrochloric acid. amount of 100mL nitric acid (4.3), was added to 200mL of hydrochloric acid (4.4), and mix well.
4.9 sodium sulfite solution (10%). Weigh 10g of sodium sulfite, dissolved in 60mL water, dilute with water to 100mL.
4.10 ammonium molybdate solution (5%). Weigh 5g of ammonium molybdate was dissolved in 60mL water, dilute with water to 100mL.
4.11 sodium fluoride solution (2.4%). Weigh 2.4g of sodium fluoride, dissolved in 60mL water, dilute with water to 100mL.
Sodium Fluoride 4.12 - Stannous chloride solution. 100mL sodium fluoride (4.11) was added 0.2g of stannous chloride, formulated with time.
4.13 P standard stock solution (100μg/mL). according to GB/T 602 formulated or direct purchase of certified reference materials.
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