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SN/T 1504.1-2014 English PDF

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SN/T 1504.1-2014: Plastics used for food container and package. Part 1: Determination of phenolic antioxidants and erucamide slip additives in polypropylene homopolymer formulations. Liquid chromatography
Status: Valid

SN/T 1504.1: Evolution and historical versions

Standard IDContents [version]USDSTEP2[PDF] delivered inStandard Title (Description)StatusPDF
SN/T 1504.1-2014English209 Add to Cart 3 days [Need to translate] Plastics used for food container and package. Part 1: Determination of phenolic antioxidants and erucamide slip additives in polypropylene homopolymer formulations. Liquid chromatography Valid SN/T 1504.1-2014
SN/T 1504.1-2005English319 Add to Cart 3 days [Need to translate] Food containers, packaging plastic raw materials - Part 1: polypropylene homopolymer determination of phenolic antioxidants and erucic amide slip agent. Liquid chromatography Obsolete SN/T 1504.1-2005

PDF similar to SN/T 1504.1-2014


Standard similar to SN/T 1504.1-2014

GB/T 325.6   GB/T 325.1   SN/T 4148   SN/T 5154   SN/T 1504.5   SN/T 1504.2   

Basic data

Standard ID SN/T 1504.1-2014 (SN/T1504.1-2014)
Description (Translated English) Plastics used for food container and package. Part 1: Determination of phenolic antioxidants and erucamide slip additives in polypropylene homopolymer formulations. Liquid chromatography
Sector / Industry Commodity Inspection Standard (Recommended)
Classification of Chinese Standard A82
Classification of International Standard 55.100
Word Count Estimation 8,861
Older Standard (superseded by this standard) SN/T 1504.1-2005
Adopted Standard ASTM D6042-2009, MOD
Regulation (derived from) AQSIQ notification issued in 2014 on the first batch of 230 industry-standard entry-exit inspection and quarantine
Issuing agency(ies) General Administration of Customs
Summary This Standard specifies the food containers, packaging polypropylene homopolymer determination of phenolic antioxidants and erucamide slip agent. This section applies to food containers, packaging polypropylene homopolymer phenolic antioxidant and liquid

SN/T 1504.1-2014: Plastics used for food container and package. Part 1: Determination of phenolic antioxidants and erucamide slip additives in polypropylene homopolymer formulations. Liquid chromatography



---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Plastics used for food container and package.Part 1. Determination of phenolic antioxidants and erucamide slip additives in polypropylene homopolymer formulations.Liquid chromatography People's Republic of China Entry-Exit Inspection and Quarantine Standards Instead of the SN/T 1504.1-2005 Food containers, plastic packaging materials Part 1. polypropylene homopolymer of phenolic antioxidants and Erucamide slip agent liquid chromatography method for the determination Part 1. Determinationofphenolicantioxidantsand Issued on. 2014-01-13 2014-08-01 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released

Foreword

SN/T 1504 "food containers, plastic packaging materials" is divided into five parts. --- Part 1. polypropylene homopolymer phenolic antioxidants and erucamide slip agent liquid chromatography method for the determination; --- Part 2. linear low density polyethylene phenolic antioxidants and erucamide slip agent liquid chromatography method for the determination; --- Part 3. ethylene polymers and ethylene - vinyl acetate (EVA) copolymer butyl - hydroxy toluene (BHT) measured gas Chromatography; --- Part 4. High density polyethylene phenolic antioxidants was measured by liquid chromatography; --- Part 5. Polyolefin Determination of impurity elements in the X-ray fluorescence spectrometry. This section SN/T 1504 Part 1. This section drafted in accordance with GB/T 1.1-2009 given rules. The partial replacement of SN/T 1504.1-2005 "food packaging plastic container materials - Part 1. polypropylene homopolymer phenolic antioxidant Erucamide slip agent and method for measuring liquid chromatography ", this section compared with the SN/T 1504.1-2005, the main differences are as follows. Text --- this section in accordance with GB/T 1.1-2009 write; --- 4.5 filter plate pore size from the original 0.45μm to "pore size 0.45μm or less"; --- Increased 4.5 annotations; --- 5.6 10μL injection volume is changed from "10μL, or based on liquid chromatography systems appropriate to reduce the injection volume." The partial modification using ASTMD6042. Content 2009, where the title changed to "food containers, packaging material polypropylene plastic Homopolymer of phenolic antioxidants and erucamide slip agent liquid chromatography method for the determination. " This section proposed and managed by the National Certification and Accreditation Administration Committee. This section is drafted. Tianjin People's Republic of China Exit Inspection and Quarantine. The main drafters of this section. From Liu Shao, Lu Gang, Ding Yu, Yang Jing, Wang Na, Zhang Bin. This part of the standard replaces the previous editions are. --- SN/T 1504.1-2005. Food containers, plastic packaging materials Part 1. polypropylene homopolymer of phenolic antioxidants and Erucamide slip agent liquid chromatography method for the determination

1 Scope

SN/T 1504 provisions of this part of the food containers, packaging polypropylene homopolymer phenolic antioxidants and erucamide slip additives Determination. This section applies to food containers and packaging polypropylene homopolymer phenolic antioxidants and erucamide slip agent and liquid chromatography Determination.

2 Method summary

Ground to a particle size of 20 polypropylene mesh powder, with dichloromethane and then cyclohexane (7525) was refluxed extraction or ultrasonic extraction Take, extract by liquid chromatography to measure the internal standard method.

3 Reagents and solutions

3.1 2 (2 'hydroxy-5'-methylphenyl) benzothiazole (Tinuvin-P), 99%. 3.2 Vitamin E (VitaminE). 3.3 erucamide (Erucamide), 99%. 3.4 tris (2,4-di-t-butylphenyl) phosphite (Irgafos168), 99%. 3.5 tetrakis (3,5-di-tert-butyl-4-hydroxy) benzenepropanoic acid pentaerythritol ester (Irganox1010), 99%. 3.6 β- (3,5- di-t-butyl-4-hydroxyphenyl) propionate, n-octadecanol ester (Irganox1076), 99%. 3.7 1,3,5-tris (3,5-di-tert-butyl-4-hydroxybenzyl) isocyanurate (Irganox3114), 99%. 3.8 dichloromethane. chromatography. 3.9 Cyclohexane. chromatography. 3.10 TP Internal standard solution. dichloromethane - solution was added a mixed Tinuvin-P cyclohexane internal standard (7525), formulated as a concentration A solution of 51.8mg L /. 3.11 Water. Helium degassed through degassing or vacuum filtration. 3.12 acetonitrile. chromatography. 3.13 isopropanol. chromatography. NOTE. dichloromethane and cyclohexane combustible, the extraction process is carried out in a fume hood.

4 Instrument

4.1 liquid chromatography. equipped with UV detector, column heating system and gradient elution device with 10μL sample injection valve. 4.2 Grinding. filled with 20 mesh sieve and water cooling system, to prevent thermal decomposition of the antioxidant. 4.3 reflux extraction device. the condenser (24/40 ground glass mouth), 125mL flat-bottomed flask (with 24/40 ground glass mouth) and with magnetic Agitation heating plates, sample extraction device, see Appendix A in Figure A.1. 4.4 ultrasonic bath instrument. ultrasonic water bath, 125mL flat-bottomed flask with a 24/40 ground glass mouth, 24/40 ground glass stopper.

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