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US$199.00 · In stock Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. SN/T 1407-2004: Determination of active content of 2.5% brodifacoum mother solution for import and export. HPLC Status: Valid
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| SN/T 1407-2004 | English | 199 |
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Determination of active content of 2.5% brodifacoum mother solution for import and export. HPLC
| Valid |
SN/T 1407-2004
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PDF similar to SN/T 1407-2004
Basic data | Standard ID | SN/T 1407-2004 (SN/T1407-2004) | | Description (Translated English) | Determination of active content of 2.5% brodifacoum mother solution for import and export. HPLC | | Sector / Industry | Commodity Inspection Standard (Recommended) | | Classification of Chinese Standard | G25 | | Classification of International Standard | 65.100 | | Word Count Estimation | 6,691 | | Date of Issue | 2004-06-01 | | Date of Implementation | 2004-12-01 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People Republic of China | | Summary | This standard specifies the use of HPLC 2. 5% bromine content of rat liquor effective way. This standard applies to 2. 5 percent bromine Rat Lung liquor valid content. |
SN/T 1407-2004: Determination of active content of 2.5% brodifacoum mother solution for import and export. HPLC ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of active content of 2.5% brodifacoum mother solution for import and export.HPLC
People's Republic of China Entry-Exit Inspection and Quarantine Industry Standard
Import and export of 2.5% bronomore mother liquor
Determination method high performance liquid chromatography
Released on June.2004
Implementation of.2004-12-01
People's Republic
The General Administration of Quality Supervision, Inspection and Quarantine issued
Foreword
This standard is proposed and managed by the National Certification and Accreditation Administration.
This standard was drafted by the Tianjin Entry-Exit Inspection and Quarantine Bureau of the People's Republic of China.
The main drafters of this standard. Liu Shaocong, Hu Xingong, Lu Gang, Liu Jun, Zhang Lai.
This standard is the industry standard for inspection and quarantine issued for the first time.
Import and export of 2.5% bronomore mother liquor
Determination method high performance liquid chromatography
1 Scope
This standard specifies the method for the determination of the effective content of 2.5% bronopolone mother liquor by high performance liquid chromatography.
This standard applies to the determination of the effective content of 2.5% bronomore mother liquor.
Active ingredient. 3-[3-(4'-bromobiphenyl-4-yl)-1,2,3,4-tetrahydro-1-naphthyl]-4-hydroxycoumarin (IUPAC), 3- {3-[4'-bromo-
One(CA;56073-10-0)
Structure.
Molecular formula. C31H23BrO3
Relative molecular weight. 523.4 (according to the international atomic weight in.1995)
2 Method summary
The sample was dissolved in acetone, and the mobile phase was fixed to volume. The sample was separated by a liquid chromatography column with 5 μm ODS (C18) as a filler, and the ultraviolet detector was used.
(254 nm) detection, external standard method quantification.
3 reagents and solutions
3.1 Methanol. chromatographically pure.
3.2 Glacial acetic acid. excellent grade pure.
3.3 pH=4.0 acetic acid-sodium acetate buffer solution. Weigh NaAc·3H2O20g, dissolve in appropriate amount of water, add 6mol/LHAc
134 mL, diluted to 500 mL.
3.4 Mobile phase. acetic acid-sodium acetate buffer solution of methanol.pH=4, 90.10 (volume fraction).
3.5 Acetone. excellent grade pure.
3.6 Distilled water.
3.7 Bromo-rhamone standard. known content ≥ 99.0%.
4 instruments
4.1 High Performance Liquid Chromatograph. UV detector with variable wavelength.
4.2 Column. 250mm × 4.6mm (inside diameter) stainless steel column, filled with C18 filler, particle size 5μm.
4.3 Injection valve. 20 μL.
4.4 Ultrasonic cleaner.
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