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SN/T 1045.2-2010: Determination of banned azo colourants in dyed textiles and leather products for import and export. Part 2: Gas chromatography/mass spectrography method
Status: Valid SN/T 1045.2: Evolution and historical versions
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| SN/T 1045.2-2010 | English | 319 |
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Determination of banned azo colourants in dyed textiles and leather products for import and export. Part 2: Gas chromatography/mass spectrography method
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SN/T 1045.2-2010
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| SN/T 1045.2-2002 | English | 559 |
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Method for the determination of banned azo colourants in dyed textiles and leather products for import and export. Gas chromatography/mass spectrography method
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SN/T 1045.2-2002
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PDF similar to SN/T 1045.2-2010
Basic data | Standard ID | SN/T 1045.2-2010 (SN/T1045.2-2010) | | Description (Translated English) | Determination of banned azo colourants in dyed textiles and leather products for import and export. Part 2: Gas chromatography/mass spectrography method | | Sector / Industry | Commodity Inspection Standard (Recommended) | | Classification of Chinese Standard | W04;Y45 | | Classification of International Standard | 59.080.30; 59.140.35 | | Word Count Estimation | 12,125 | | Date of Issue | 2010-01-10 | | Date of Implementation | 2010-07-16 | | Older Standard (superseded by this standard) | SN/T 1045.2-2002 | | Quoted Standard | GB/T 6682; SN/T 1045.1 | | Regulation (derived from) | National Quality Inspection (2010) No. 13 | | Issuing agency(ies) | General Administration of Customs | | Summary | This standard specifies the dyeing of textile and leather products 23 kinds of aromatic amines is disabled (see Appendix A) content by gas chromatography/mass spectrometry. This standard applies to imports and dyeing textiles (including cotton, linen, silk, wool, chemical fiber, etc.) and dyed leather products 23 kinds of disabling the detection of aromatic amines. | SN/T 1045.2-2010: Determination of banned azo colourants in dyed textiles and leather products for import and export. Part 2: Gas chromatography/mass spectrography method
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Determination of banned azo colourants in dyed textiles and leather products for import and export Part 2. Gas chromatography/mass spectrography method
Exit inspection and quarantine industry standard book People's Republic of China
Instead of the SN/T 1045.2-2002
Importers dyed textiles and leather products
Determination of azo dye disabled
Part 2. Gas Chromatography/Mass Spectrometry
Issued on. 2010-01-10
2010-07-16 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
SN/T 1045 "Importers dyed textiles and leather products - Determination of banned azo" is divided into three parts.
--- Part 1. liquid chromatography;
--- Part 2. Gas chromatography/mass spectrometry;
--- Part 3. Gas Chromatography.
This section SN/T 1045 Part 2.
This part is the SN/T 1045.2-2002 "Importers dyed textiles and leather products banned azo gas test method
Amendment chromatography/mass spectrometry, "the.
This section compared with the SN/T 1045.2-2002, the main differences are as follows.
--- Increasing the types of detectable aromatic amines, can detect 23 kinds of aromatic amines. The increase is three kinds.
(1) 2,4-dimethylaniline (2,4-Xylidine);
(2) 2,6-dimethylaniline (2,6-Xylidine);
--- Extraction solvent ether to methyl tert-butyl ether;
--- Reagent eleven to eleven tungsten tungsten potassium silicate sodium silicate;
--- Final volume is defined as 2mL solvent methyl t-butyl ether;
--- Delete the original table 2 aromatic amines selected ion analysis conditions and Appendix C aromatic amines spectrum.
This section Purifying Unlike other standards or methods when using other standards or test results obtained by the method has a strong matrix interference, no
When the method is accurate qualitative and quantitative, it recommended adopting the standard method.
This section in Appendix A, Appendix C is a normative appendix, Appendix B, Appendix D and Appendix E is an informative annex.
This section proposed and managed by the National Certification and Accreditation Administration Committee.
This section was drafted by. People's Republic of China Shandong CIQ.
The main drafters of this section. Cattle Zengyuan, Ye Xi Wen, with Liu, Ke Zhen, Sunzhong Song, Wang.
This section first published in 2002, in 2010 the first amendment.
Importers dyed textiles and leather products
Determination of azo dye disabled
Part 2. Gas Chromatography/Mass Spectrometry
1 Scope
SN/T 1045 provisions of this part of the dyed textiles and leather products 23 kinds of banned aromatic amines (see Appendix A) content of gas chromatography
Spectrum/MS detection method.
This section applies to import and export textile dyeing (including cotton, hemp, silk, wool and chemical fiber) and dyed leather 23 kinds of banned aromatic amines
Detection.
2 Normative references
The following documents contain provisions which, through reference SN/T 1045 and become part of the provisions of this section. For dated references,
All subsequent amendments (not including errata content) or revisions do not apply to this section, however, encourage the agreement on this section
Whether the parties can study the latest versions of these documents. For undated reference documents, the latest versions apply to this section.
Laboratory use specifications and test methods GB/T 6682 Analysis
SN/T 1045.1 Importers dyed textiles and leather products - Determination of banned azo Part 1. liquid chromatography
Principle 3
In citrate buffer (pH = 6.0) in the sample is reduced azo dyes sodium dithionite to the corresponding aromatic amine intermediate.
With methyl tert-butyl ether - methylene chloride solution in a mixed solvent extraction of aromatic amines. Extract aromatic amine with hydrochloric acid and sodium tungstate eleven
After the solution was acidified to a salt concentration, the residue was washed with an organic solvent. After alkalizing to free the aromatic amine was extracted with methyl tert-butyl ether and dilute with
In Gas Chromatography/Mass Spectrometry.
4 Reagents
Unless otherwise specified, the reagents were of analytical grade, water use in line with two water GB/T 6682 regulations.
4.1 hexane. chromatographically pure.
4.2 methyl tert-butyl ether. chromatography (CAS Number. 1634-04-4).
4.3 dichloromethane. chromatography.
4.4 Nitrogen. more than 99.99% purity.
4.5 hydrochloric acid solution. 1mol/L.
4.6 hydrochloric acid solution. 4mol/L.
4.7 Sodium hydroxide solution. 5mol/L.
4.8 citrate buffer solution. 0.06mol/L, pH = 6.0. Citric acid and sodium hydroxide weighed 12.526g 6.320g, dissolved
1000mL water.
4.9 dithionite solution.200mg/mL, the time is now equipped with.
4.10 Extraction solvent. methyl tert-butyl ether (4.2) and 3 parts of dichloromethane (4.3) 1 shake mix.
4.11 eleven tungsten silicate (Na8SiW11O39 · like H2O). homemade. The 91g of sodium tungstate (Na2WO4 · 2H2O) and 7.37g silicic acid
Sodium (Na2SiO3 · 9H2O) were dissolved in 150mL of hot water, placed on a magnetic stirrer, while heating and stirring, was added dropwise
98mL hydrochloric acid solution (4.6), set on stove, cover pan heating surface micro-boiling 1h. Then filtered, saturated sodium chloride was added to the filtrate
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