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SN/T 0604-2014: Determination of duren residue in vegetable for export. GC-MS method
Status: Valid SN/T 0604: Evolution and historical versions
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| SN/T 0604-2014 | English | 419 |
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Determination of duren residue in vegetable for export. GC-MS method
| Valid |
SN/T 0604-2014
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| SN 0604-1997 | English | RFQ |
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3 days [Need to translate]
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(Vegetables for export durene Residue testing methods)
| Obsolete |
SN 0604-1997
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| SN 0604-1996 | English | 519 |
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Method for the determination of durene residues in vegetables for export
| Obsolete |
SN 0604-1996
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PDF similar to SN/T 0604-2014
Basic data | Standard ID | SN/T 0604-2014 (SN/T0604-2014) | | Description (Translated English) | Determination of duren residue in vegetable for export. GC-MS method | | Sector / Industry | Commodity Inspection Standard (Recommended) | | Classification of Chinese Standard | B31 | | Word Count Estimation | 16,183 | | Date of Issue | 4/9/2014 | | Date of Implementation | 11/1/2014 | | Older Standard (superseded by this standard) | SN 0604-1996 | | Quoted Standard | GB/T 6682 | | Regulation (derived from) | State inspection certification (2014) 210 | | Issuing agency(ies) | General Administration of Customs | | Summary | This standard specifies the vegetables for export durene residues by gas chromatography - mass spectrometry method. This standard applies to cabbage, tomatoes, green beans, broccoli durene residues measured and confirmed. | SN/T 0604-2014: Determination of duren residue in vegetable for export. GC-MS method---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
(Vegetables for export durene residues detected by gas chromatography - mass spectrometry)
People's Republic of China Entry-Exit Inspection and Quarantine Standards
Replacing SN 0604-1996
Detection vegetables for export durene residues
Gas chromatography - mass spectrometry
GC-MSmethod
Issued on. 2014-04-09
2014-11-01 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
This standard was drafted in accordance with GB/T 1.1-2009 given rules.
This standard replaces SN 0604-1996 "durene residues in vegetables for export."
This standard compared with SN 0604-1996, in addition to editorial changes outside the main technical changes are as follows.
--- Changing the name of the standard;
--- Apply matrix detection range expanded to cabbage, tomatoes, green beans, broccoli;
--- Modify the sample pretreatment methods, pretreatment methods to extract homogeneous solid - phase extraction (SPE);
--- Modify the sample detection method, the detection method to gas chromatography - mass spectrometry;
--- Increased durene confirmation.
Please note that some of the content of this document may involve patents. Release mechanism of the present document does not assume responsibility for the identification of these patents.
This standard is proposed and managed by the National Certification and Accreditation Administration Committee.
This standard was drafted. People's Republic of China Zhejiang Exit Inspection and Quarantine.
The main drafters of this standard. Song Weihua, Hubei Zhen, Bin Business Studies, Dongwen Hong, Shaotie Feng, Yang Pao roots.
This standard replaces the standards previously issued as follows.
--- SN 0604-1996.
Detection vegetables for export durene residues
Gas chromatography - mass spectrometry
1 Scope
This standard specifies the vegetables for export durene residues by gas chromatography - mass spectrometry method.
This standard applies to cabbage, tomatoes, green beans, broccoli durene residues measured and confirmed.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
Laboratory use specifications and test methods GB/T 6682 Analysis
3 Method summary
Sample remaining durene by hexane extraction, solid phase extraction (SPE) purification, gas chromatography - mass spectrometer and validation, external standard method or
Internal standard.
4 Reagents and materials
Except where noted, all reagents were of analytical grade water as a water GB/T 6682 regulations.
4.1 hexane. chromatographically pure.
4.2 sodium chloride.
4.3 Standard. durene (durene), CAS No. 95-93-2, purity ≥98.0%.
4.4 internal standard. durene isotope internal standard (1,2,4,5-tetramethylbenzene-3,6-d2, CAS No. 1859-01-4).
4.5 standard stock solution. accurately weighed amount of durene standard substance, n-hexane formulated into 100μg/mL standard stock solution, to avoid
Light stored at 0 ℃ ~ 4 ℃.
4.6 durene isotope internal standard stock solution. accurately weighed amount of durene isotope internal standard reference material, which is equipped with n-hexane
Made 1μg/mL standard stock solution, stored in the dark at 0 ℃ ~ 4 ℃.
4.7 standard solution. according to testing requirements before use with n-hexane diluted stock standard solution into a standard working solution of appropriate concentration is required
When added to a certain concentration of the internal standard solution (4.6). Using now.
4.8 Florisil solid-phase extraction column (6mL, 500mg). n-hexane before use with 5mL activation.
5. Apparatus
5.1 GC - MS.
5.2 Multifunctional Organization mashed machines.
5.3 rotary evaporator.
5.4 High-speed homogenizer. not less than 10000r/min.
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