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Calibration Specification for Water Colorimeters
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JJF 1689-2018
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Basic data Standard ID | JJF 1689-2018 (JJF1689-2018) | Description (Translated English) | Calibration Specification for Water Colorimeters | Sector / Industry | Metrology & Measurement Industry Standard | Classification of Chinese Standard | A60 | Word Count Estimation | 18,136 | Date of Issue | 2018-02-27 | Date of Implementation | 2018-05-27 | Regulation (derived from) | AQSIQ Announcement No. 26 of 2018 | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine |
JJF 1689-2018: Calibration Specification for Water Colorimeters---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Calibration Specification for Water Colorimeters
National Metrology Technical Specification of the People's Republic
Water colorimeter calibration specification
Published on.2018-02-27
2018-05-27 implementation
The General Administration of Quality Supervision, Inspection and Quarantine issued
Water colorimeter calibration specification
Focal Point. National Optical Metrology Technical Committee
Main drafting unit. Hebei Institute of Metrology
Henan Institute of Metrology
Participated in the drafting unit. Shanghai Haorui Instrument Co., Ltd.
Hebei Metrology Supervision and Inspection Institute
This specification entrusts the National Optical Metrology Technical Committee to explain
The main drafters of this specification.
Cai Zonglin (Hebei Institute of Metrology)
Sun Xiaoping (Henan Institute of Metrology)
Sun Wei (Hebei Institute of Metrology)
Participate in the drafters.
Zhu Hanfei (Shanghai Haorui Instrument Co., Ltd.)
Wang Yonghao (Hebei Institute of Metrology)
Bi Lixin (Hebei Province Metrology Supervision and Inspection Institute)
Li Wei (Henan Institute of Metrology)
table of Contents
Introduction (II)
1 Scope (1)
2 References (1)
3 terms and units of measurement (1)
3.1 Terminology (1)
3.2 Unit of measurement (1)
4 Overview (1)
5 Measurement characteristics (2)
5.1 Zero-point drift of digital display instrument (2)
5.2 indication error (2)
5.3 Repeatability of digital display (2)
6 Calibration conditions (2)
6.1 Environmental conditions (2)
6.2 Measurement standards and other equipment (2)
7 Calibration items and calibration methods (3)
7.1 Inspection and preparation before calibration (3)
7.2 Zero drift of digital display instrument (3)
7.3 indication error (3)
7.4 Repeatability of digital display instruments (3)
8 calibration result expression (4)
9 re-study interval (4)
Appendix A Calibration Original Record Recommended Format (5)
Appendix B Recommended Format for Calibration Certificate (6)
Appendix C Example of Uncertainty Evaluation of Measurement Results (7)
Appendix D Series Standard Solution Preparation (10)
Appendix E Spectrophotometric Method for Measuring Color Plate Colors of Visual Instruments (11)
Introduction
This specification is based on JJF 1001-2011 "General Terms and Definitions of Measurement", JJF 1059.1-2012
Deterministic Evaluation and Representation, JJF 1094-2002 "Measuring Instrument Characteristics Evaluation" and JJF 1071-2010 "Country
Compilation of the rules for the preparation of metrological calibration specifications.
According to the actual situation of the water color meter, this specification is formulated according to ISO 7887.2011
Method D in Water Quality-Examination and Determination of Color. Natural
Visual method of water color measurement.
This specification is the first release.
Water colorimeter calibration specification
1 Scope
This specification applies to the calibration of water colorimeters using platinum-cobalt units.
2 reference files
GB/T 6682-2008 Analytical laboratory water specifications and test methods
GB/T 11903 Determination of water color chromaticity
ISO 7887.2011 Water quality color detection (Waterquality-Examinationanddetermina-
Tionofcolor)
For dated references, only dated versions apply to this specification; undated quotations
The latest version (including all amendments) applies to this specification.
3 terms and units of measure
3.1 Terminology
3.1.1 Platinum cobalt unit Pt-Counit, PCU
a solution containing platinum (in the form of chloroplatinum (IV) acid salt) and cobalt (II) chloride hexahydrate at a specified concentration
Color unit. Contains 1 mg of platinum per [liter of chloroplatinum (IV) acid salt] and 2 mg of cobalt chloride hexahydrate
The platinum cobalt solution of (II) has a color of 1 degree.
3.2 Unit of measurement
The common unit of water color chromaticity is degree. Other units include milligrams of platinum per liter, platinum-cobalt, platinum-cobalt units, and black.
The unit symbols are mgPtL-1, Pt-Co, PCU, and Hazen, and the conversion relationship is as follows.
1 degree=1mgPtL-1=1Pt-Co=1PCU=1Hazen
4 Overview
Water colorimeter is a measuring instrument for measuring the color of water according to the platinum-cobalt colorimetric method specified in GB/T 11903.
Color test for clean water, lightly polluted and slightly yellowed water, cleaner ground water, ground water and drinking water
Measurement. According to its working principle and method, water quality colorimeter (hereinafter referred to as instrument) can be divided into visual instruments and digital display instruments.
The light source of the visual instrument is transmitted or reflected, and passes through the liquid column from the bottom of the colorimetric tube.
The color of the field of view, the value represented by the color palette that best matches the water sample being tested, is the chromaticity value of the water sample. Visual instrument such as
As shown in Figure 1, it is generally composed of a light source, a light source correction system, a color palette, a sample slot, an observation eyepiece, etc., usually
Equipped with a colorimetric tube.
Digital display instrument according to Lambert-Beer law, when a bundle of parallel monochromatic light passes through a water sample containing a light absorbing substance, the light
Part of the absorption is absorbed, and when the thickness of the absorption layer is constant, the absorbance is proportional to the concentration of the light absorbing substance, and the photodetector is passed through
The optical signal is converted into an electrical signal, and the chromaticity of the water sample is displayed after the microprocessor. The digital display instrument is shown in Figure 2, usually by
Light source, spectroscopic system, sample cell, photodetector, display device, etc.
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