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JJF 1547-2015 English PDF

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JJF 1547-2015: Calibration Specification for On-line pH Meters
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Basic data

Standard ID JJF 1547-2015 (JJF1547-2015)
Description (Translated English) Calibration Specification for On-line pH Meters
Sector / Industry Metrology & Measurement Industry Standard
Classification of Chinese Standard A61
Classification of International Standard 17.020
Word Count Estimation 20,226
Date of Issue 2015-08-24
Date of Implementation 2015-11-24
Quoted Standard ASTM D5128-2009
Regulation (derived from) AQSIQ Announcement 2015 No.106
Issuing agency(ies) General Administration of Quality Supervision, Inspection and Quarantine
Summary This standard is applicable to the calibration of an on-line pH meter with an electrode method for measuring the pH of water with a conductivity greater than 100 ��S �� cm-1.

JJF 1547-2015: Calibration Specification for On-line pH Meters

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Calibration Specification for On-line pH Meters People's Republic of China National Metrology Technical Specifications Online pH meter calibration specification Issued on. 2015-08-24 2015-11-24 implementation The State Administration of Quality Supervision, Inspection and Quarantine released Online pH meter calibration specification On-linepHMeters Focal point. the National Technical Committee on Physical stoichiometric online chemical analysis instruments Technical Committee The main drafting units. China Institute of Metrology China Testing Technology Research Institute Shandong Province Institute of Metrology Participated in the drafting unit. Guangxi Institute of measurement testing State Power Institute of Science and Technology Jiangsu Power Technology Co., Ltd., days This specification stoichiometric commissioned the National Technical Committee of physical chemical analysis instruments online at the Technical Committee Members will be responsible for interpreting The main drafters of this specification. Repair Hongyu (China Institute of Metrology) Yuan Li (China Testing Technology Research Institute) Gobo (Shandong Province Institute of Metrology) Drafters participate. Feng Shaobo (Guangxi Institute of measurement detection) Zheng (State Power Institute of Science and Technology) HU Guo Zhang (Jiangsu Power Technology Co., Ltd., days)

table of Contents

Introduction (Ⅱ) 1 Scope (1) 2. References (1) 3 Terms (1) 3.1 liquid junction potential (1) 3.2 streaming potential (1) 4 Overview (1) 5 Metrological characteristics (2) Calibration Condition 6 (2) 6.1 environmental conditions (2) 6.2 standard solution and a constant temperature of the electrode system (3) 6.3 standards and other measuring equipment (3) 7 calibration items and calibration methods (3) 7.1 Check the electrode (3) PH 7.2 electricity meter indication error (3) 7.3 meter electric voltage indication error (4) 7.4 input current (4) Enter pH 7.5 Indication error due to the resistance (4) pH 7.6 Indication error caused by temperature compensator (4) 7.7 Temperature indication error (5) PH 7.8 Instrument indication error and Repeatability (5) 7.9 Indication Instruments pH stability (5) 8 calibration results expression (5) 9 Recalibration interval (6) Appendix A Evaluation of Uncertainty instrument error of indication (7) Appendix B Calibration original record format (Reference) (10) Appendix C calibration certificate (within the page) format (reference) (14)

Introduction

This specification according JJF 1071-2010 "National Calibration Specifications writing rules" requirement be written. Standard Test Method ASTM D5128-2009-line measurement of pH in low conductivity water (StandardTest MethodforOn-LinepH MeasurementofWaterofLowConductivity) to water conductivity 100μS · cm-1 for the sector, will be divided into two-line pH meter monitor normal water pH and low conductivity water pH. Is Conductivity measuring different solution, online pH meter calibration method may be different. This specification does not apply to low-power monitoring Conductivity pH of the water-line pH meter. This specification is the first release. Online pH meter calibration specification

1 Scope

This instruction applies to measure the conductivity greater than 100μS · cm-1 water quality of pH electrode method using online pH meter calibration. 2. References This specification refers to the following documents. Standard Test Method for ASTMD5128-2009 line measurement of pH in low conductivity water (StandardTest MethodforOn-LinepH MeasurementofWaterofLowConductivity) For dated references, only the dated edition applies to this specification; undated reference documents Member, the latest edition (including any amendments) applies to this specification.

3 Terms

3.1 liquid junction potential liquidjunctionpotential When two different electrolyte solution in contact with the liquid junction region, the high concentration of ions from one side to the rich Of the lower side of the spread. Solution diffusion coefficient of various positive and negative ions different diffusion rates are different, resulting in industry Electric potential difference generated on both sides. 3.2 streaming potential streamingpotential When the electrolyte solution in a flow of charged insulating surface, the electric double layer surface free of charged particles along the The solution flow direction. These movements cause charged particles downstream of the accumulation of charge, so that between the upstream and downstream production Raw potential difference.

4 Overview

Online pH meter (hereinafter referred to as instruments) are widely used in field operations, and process conditions at the production site of continuous monitoring Water pH value, usually by a pH meter electrical system (secondary instrument systems) and pH electrode system (sensor system) two Part. Figure 1 is its structure diagram. Instrument electrode system in two basic designs. one is immersed for Measuring pH measuring reaction tank, reaction tank, etc. stationary water quality; another way for the flow-through, for the water flowing through a pipe Quality pH measurement. Line pH meter, electrode system measuring the flow of water quality should be grounded, and the use of stainless steel flow Pool to reduce the impact of the flow potential.

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