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HYT147.3-2013: Code of practice for marine monitoring technology. Part 3: Organism
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Code of practice for marine monitoring technology. Part 3: Organism
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HY/T 147.3-2013
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Basic data | Standard ID | HY/T 147.3-2013 (HY/T147.3-2013) | | Description (Translated English) | Code of practice for marine monitoring technology. Part 3: Organism | | Sector / Industry | Marine Industry Standard (Recommended) | | Classification of Chinese Standard | A45 | | Classification of International Standard | 07.060 | | Word Count Estimation | 69,694 | | Quoted Standard | GB/T 6379.2-2004; GB 17378.1; GB 17378.2; GB 17378.3; GB 17378.6; | | Regulation (derived from) | Industry standard filing Notice 2013 No. 8 (No. 164 overall) | | Issuing agency(ies) | State Oceanic Administration | | Summary | This standard specifies: fish, shrimp, shellfish and other marine organisms monitoring project analysis. This standard applies to: far from the sea, coastal and estuarine marine life monitored. | HYT147.3-2013: Code of practice for marine monitoring technology. Part 3: Organism---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Code of practice for marine monitoring technology.Part 3.Organism
ICS 07.060
A45
People's Republic of China Marine Industry Standard
Marine monitoring technical regulations
Part 3.Organisms
Part 3.Organism
Released on.2013-04-25
2013-05-01 Implementation
Issued by the State Oceanic Administration
Table of contents
Preface Ⅲ
1 Scope 1
2 Normative references 1
3 Terms and definitions 1
4 General provisions 1
5 Determination of total mercury---thermal decomposition cold atomic absorption spectrometry 2
6 Simultaneous determination of copper, lead, zinc, cadmium, chromium, manganese, nickel, arsenic, aluminum, and iron---inductively coupled plasma mass spectrometry 5
7 Polycyclic aromatic hydrocarbons 8
8 Phthalates 20
9 Determination of Organophosphorus Pesticides---Gas Chromatography 28
10 Determination of organotin---gas chromatography 32
11 Determination of polybrominated diphenyl ethers---gas chromatography/mass spectrometry 36
Appendix A (Normative Appendix) Record Sheet 41
Appendix B (informative appendix) Method detection limit 54
Appendix C (informative appendix) Determination of EROD---kinetic fluorescence method 56
Appendix D (informative appendix) Determination of total acetylcholinesterase in marine organisms 61
Figure 1 GC-MS-SIM spectra of 18 PAHs standard solutions Figure 11
Figure 2 Gas chromatogram of 16 PAHs standard solutions 16
Figure 3 Liquid chromatogram of PAHs standard solution Figure 19
Figure 4 Gas chromatography/mass spectrometry diagram of 6 standard solutions of phthalate esters 24
Figure 5 Gas chromatogram of 6 standard solutions of phthalate ester 27
Figure 6 Gas chromatogram of 14 standard solutions of organophosphorus pesticides 31
Figure 7 Gas chromatogram of standard solution of organotin compound 35
Figure 8 Gas Chromatography/Mass Spectrogram of Polybrominated Diphenyl Ether Standard Solution 40
Table 1 Analysis conditions of automatic mercury analyzer 3
Table 2 Working conditions of microwave digestion instrument 6
Table 3 The repeatability, reproducibility and recovery rate of each element determined by ICP-MS 7
Table 4 GC-MS determination of PAHs retention time and quantitative ion 11
Table 5 Repeatability, reproducibility and recovery rate of PAHs measured by GC-MS 12
Table 6 Repeatability, reproducibility and recovery rate of PAHs measured by GC-FID 16
Table 7 HPLC gradient elution program 20
Table 8 The relative standard deviation of repeatability of PAHs determined by HPLC 20
Table 9 Quantitative ion parameters of phthalate esters determined by GC-MS 24
Table 10 GC-MS determination of repeatability, reproducibility and recovery rate of phthalate 24
Table 11 The repeatability, reproducibility and recovery rate of phthalate ester determined by GC-ECD 28
Table 12 The repeatability, reproducibility and recovery rate of organophosphorus pesticides determined by GC-FPD 31
Table 13 The repeatability, reproducibility and recovery rate of organotin compounds determined by GC-FPD 35
Table 14 GC-MS determination of retention time of polybrominated diphenyl ethers and characteristic ions 39
Table 15 The repeatability, reproducibility and recovery rate of polybrominated diphenyl ethers determined by GC-MS 39
Table A.1 Hg analysis record of biological samples 41
Table A.2 Analysis records in biological samples 42
Table A.3 Recording table 43 of internal standard working curve of polycyclic aromatic hydrocarbons in biological samples
Table A.4 Analysis record of polycyclic aromatic hydrocarbons in biological samples Table 44
Table A.5 Polycyclic Aromatic Hydrocarbons Working Curve Record Table 45 in Biological Samples
Table A.6 Analysis record of polycyclic aromatic hydrocarbons in biological samples 46
Table A.7 Analysis Record of Phthalates in Biological Samples Table 47
Table A.8 Standard curve record of phthalates in biological samples 48
Table A.9 Analysis Record of Phthalates in Biological Samples Table 49
Table A.10 Standard curve record of organophosphorus pesticides in biological samples 50
Table A.11 Analysis record of organophosphorus pesticides in biological samples 51
Table A.12 Analysis records of organotin compounds in biological samples Table 52
Table A.13 Analysis record of polybrominated diphenyl ethers in biological samples Table 53
Table B.1 Detection limit of determination method 54
Table C.1 EROD field sampling record table 59
Table C.2 EROD analysis record table 60
Table D.1 AchE field sampling record table 63
Table D.2 AchE Analysis Record Table 64
Foreword
HY/T 147 "Marine Monitoring Technical Regulations" is divided into seven parts.
---Part 1.Sea water;
---Part 2.Sediment;
---Part 3.Organisms;
---Part 4.Ocean atmosphere;
---Part 5.Marine ecology;
---Part 6.Marine Hydrology, Meteorology and Sea Ice;
---Part 7.Satellite remote sensing technology methods.
This part is part 3 of HY/T 147.
This section was drafted in accordance with the rules given in GB/T 1.1-2009.
This part was proposed by the National Marine Environmental Monitoring Center.
This part is under the jurisdiction of the National Marine Standardization Technical Committee (SAC/TC283).
This section is responsible for the drafting unit. National Marine Environmental Monitoring Center.
Participating in the drafting of this section. South China Sea Environmental Monitoring Center of State Oceanic Administration, East China Sea Environmental Monitoring Center of State Oceanic Administration, State Oceanic Administration
Beihai Environmental Monitoring Center.
The main drafters of this section. Han Gengchen, Zhang Zhifeng, Yao Ziwei, Wang Juying, Ma Yongan, Jiang Wenbo, Wang Lijun, Liu Guangyuan, Ma Xindong,
Liu Liang, Zhao Dongmei, Lin Zhongsheng, Wang Yanjie, Zhao Shilan, Xu Hengzhen, Cheng Xiangsheng, Liu Fuping, Qin Banghui, Zhang Yong, Qiu Jinkun, Zhang Shugang, Huang Chuguang,
Wu Shiwei, Lu Chuqian, Zhou Peiyu, Lu Dapeng, Cui Wenlin, Yang Xiaofei, Wang Xinping, Yu Zijiang, Zhao Yuhui.
Marine monitoring technical regulations
Part 3.Organisms
1 Scope
This part of HY/T 147 specifies the analysis methods for monitoring items of marine organisms such as fish, shrimp, and shellfish.
This part is applicable to the monitoring of marine life in the open sea, offshore sea and estuary.
2 Normative references
The following documents are indispensable for the application of this document. For dated reference documents, only the dated version applies to this article
Pieces. For undated references, the latest version (including all amendments) applies to this document.
GB/T 6379.2-2004 Measurement methods and accuracy of results (accuracy and precision) Part 2.Determine standard measurement methods
Basic method of method repeatability and reproducibility
GB 17378.1 Marine Monitoring Specification Part 1.General
GB 17378.2 Marine Monitoring Specification Part 2.Data Processing and Analysis Quality Control
GB 17378.3 Marine Monitoring Specification Part 3.Sample Collection, Storage and Transportation
GB 17378.6 Marine Monitoring Specification Part 6.Biological Analysis
3 Terms and definitions
The following terms and definitions defined in GB 17378.1 and GB 17378.2 apply to this document.
3.1
Marine biological sample
Marine organisms in the open sea, offshore waters and estuaries, including fish, shrimp, shellfish and other marine organisms.
3.2
Freeze-drying
A drying method in which the material to be dried is quickly frozen, and then the ice in it is sublimated into water vapor under high vacuum conditions. Due to ice
The sublimation takes away the heat to keep the freeze-drying process in a low-temperature frozen state, which is conducive to retaining the activity of some biological samples (such as proteins).
4 General rules
4.1 Sample collection
The collection, preparation, storage, transportation and pretreatment of samples shall be carried out in accordance with the relevant regulations of GB 17378.3 and GB 17378.6.
4.2 Reagents and materials
The experimental supplies of this part should be handled according to the following requirements.
a) Test tubes with scales, concentrate bottles, pipettes, volumetric flasks, etc. for experiments should be calibrated before use;
b) Glass containers and utensils should be rinsed with water, washed with detergent, then washed with ultrapure water, dried or dried naturally;
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