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HJ 510-2009: Cleaner production standard. Waste lead-acid battery recycling industry
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Cleaner production standard. Waste lead-acid battery recycling industry
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Basic data | Standard ID | HJ 510-2009 (HJ510-2009) | | Description (Translated English) | Cleaner production standard. Waste lead-acid battery recycling industry | | Sector / Industry | Environmental Protection Industry Standard | | Classification of Chinese Standard | Z62 | | Classification of International Standard | 13.100 | | Word Count Estimation | 11,196 | | Date of Issue | 2009-11-16 | | Date of Implementation | 2010-01-01 | | Quoted Standard | GB/T 469; GB/T 2589; GB/T 15555.2; GB/T 21181; GB/T 24001; HJ/T 56-2000; HJ/T 57-2000 | | Regulation (derived from) | Department of Environmental Protection Notice No. 61 of 2009 | | Issuing agency(ies) | Ministry of Ecology and Environment | | Summary | This standard specifies the lead acid battery scrap recycling industry clean production requirements. This standard will lead acid battery scrap recycling industry clean production indicators are divided into six categories, namely, the production technology and equipment indicators, resource and energy utilization index, product index, pollutant indicator (prior to the end of treatment), waste recycling and environmental management requirements. This standard applies to lead acid battery scrap recycling industry cleaner production audit and cleaner production potential and opportunities sentenced Adams, cleaner production and cleaner production performance evaluation performance disclosure system for environmental impact assessment and environmental management permit regime. | HJ 510-2009: Cleaner production standard. Waste lead-acid battery recycling industry---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Cleaner production standard.Waste lead-acid battery recycling industry
HJ
National Environmental Protection Standard of the People's Republic
Clean production standard lead-acid battery lead recycling industry
Cleaner production standard
-Waste lead-acid battery recycling industry
Released on.2009-11-16
2010-01-01 Implementation
Ministry of Environmental Protection released
Ministry of Environmental Protection
announcement
No. 61 of.2009
To protect the environment and improve enterprises in order to implement the Environmental Protection Law of the People's Republic of China and the Law of the People's Republic of China on Cleaner Production Promotion.
The level of clean production in the industry is now approved as the “clean lead production lead-acid battery lead recycling industry” as the national environmental protection standard, and issued
cloth.
The standard name and number are as follows.
The standard was implemented on January 1,.2010 and published by the China Environmental Science Press. The standard content can be found on the website of the Ministry of Environmental Protection.
Special announcement.
November 16,.2009
Content
Foreword..iv
1 Scope..1
2 Normative references..1
3 Terms and Definitions.1
4 Normative technical requirements..2
5 Data acquisition and calculation method 4
6 Standard implementation.6
Foreword
To implement the Environmental Protection Law of the People's Republic of China, the Law of the People's Republic of China on the Prevention and Control of Environmental Pollution by Solid Wastes, and the Chinese People
The Clean Production Promotion Law of the Republic, which protects the environment and provides technical support and guidance for the clean production of lead-acid battery lead recycling industry.
Set this standard.
This standard stipulates that on the basis of meeting national and local pollutant discharge standards, according to current industry technology, equipment level and management water
Flat, general requirements for clean production of lead-acid battery lead recycling industry. This standard is divided into three levels, one level represents the international advanced level of cleaner production,
The second level represents the advanced level of domestic clean production, and the third level represents the basic level of domestic clean production. With the continuous development and progress of technology, this standard
The Brigadier General is constantly revised.
This standard is the first release.
This standard was formulated by the Science and Technology Standards Department of the Ministry of Environmental Protection.
This standard was drafted. Shenyang Environmental Science Research Institute, Institute of High Energy Physics, Chinese Academy of Sciences, China Nonferrous Metals Industry Association
Metal Branch, Zhejiang Huitong Power Co., Ltd., National Environmental Protection Hazardous Waste Disposal Engineering Technology Center.
This standard was approved by the Ministry of Environmental Protection on November 16,.2009.
This standard has been implemented since January 1,.2010.
This standard is explained by the Ministry of Environmental Protection.
Iv
Clean production standard lead-acid battery lead recycling industry
1 Scope of application
This standard specifies the general requirements for clean production of lead-acid battery lead recycling industry. This standard will lead the waste lead acid battery lead recycling industry
The production indicators are divided into six categories, namely, production process and equipment indicators, resource and energy utilization indicators, product indicators, and pollutant production indicators (end treatment).
Before), waste recycling indicators and environmental management requirements.
This standard applies to the clean production audit of waste lead-acid battery lead recycling enterprises and the judgment of clean production potential and opportunity, clean production
The performance appraisal and clean production performance announcement system is also applicable to environmental management systems such as environmental impact assessment and discharge permits.
2 Normative references
The contents of this standard refer to the terms in the following documents. For undated references, the valid version applies to this standard.
GB/T 469 lead ingot
GB/T 2589 General rules for comprehensive energy consumption calculation
GB/T 15555.2 Determination of copper, zinc, lead and cadmium in solid waste - Atomic absorption spectrophotometric method
GB/T 21181 recycled lead and lead alloy ingot
GB/T 24001 Environmental Management System Requirements and User Guide
HJ/T 56-2000 Determination of sulphur dioxide in fixed source s
HJ/T 57-2000 Determination of sulfur dioxide in fixed source exhaust gases
Interim Measures for Clean Production Audit (National Development and Reform Commission, State Environmental Protection Administration Order No. 16)
3 Terms and definitions
3.1 Clean production
Refers to continuous improvement of design, use of clean energy and raw materials, adoption of advanced process technology and equipment, improvement of management, and comprehensive utilization
And other measures to reduce pollution from the source, improve resource utilization, reduce or avoid the production of pollutants in production, service and product use.
And emissions to mitigate or eliminate harm to human health and the environment.
3.2 Waste lead-acid battery
Refers to the loss of the original use value in production, life and other activities or the loss of use value but abandoned or abandoned
Lead-acid batteries.
3.3 Lead recovery
The process of extracting lead from a waste lead-acid battery through various methods, techniques and processes.
3.4 Fire method smelting
A technical process for extracting metals from a molten state by a high temperature method.
3.5 Hydrometallurgy
A technical process for extracting metals from a solution by chemical action using a solvent.
3.6 Lead dust
Solid materials such as waste lead-acid batteries are suspended in a gaseous medium formed by mechanical processes (natural processes) such as crushing, classification, and grinding.
Fine solid particles.
3.7 partition
A lead-acid battery assembly made of an ion-permeable material that prevents contact between plates of opposite polarity in the battery.
4 Normative technical requirements
4.1 Indicator classification
This standard gives three levels of technical indicators for the clean production level of the lead recycling industry production process.
Level 1. International advanced level of cleaner production;
Level 2. advanced level of domestic clean production;
Level 3. The basic level of domestic cleaner production.
4.2 Indicator requirements
The requirements for clean production indicators for the pyrometallurgical lead recycling industry are shown in Table 1.
The requirements for clean production of wet metallurgy lead recycling industry are shown in Table 2.
Table 1 Clean production index requirements for lead recycling industry (fire law smelting class)
Indicator level one level two level three
First, the production process and equipment requirements
Automatic crushing and sorting system mechanized crushing and sorting
1. Pre-desulfurization of preparation technology and equipment (excluding oxygen-rich bottom blowing-blast furnace melting process)
2. Smelting process and equipment rotary short kiln smelting, oxygen-rich bottom blowing - blast furnace melting, automatic ingot casting machine, etc.
Reverberatory furnace
Outside), blast furnace smelting, automatic casting
Ingot machine, etc.
Second, product indicators
1. Recycled crude lead main grade /% lead ≥ 99 lead ≥ 98.5 lead ≥ 98
2. Polypropylene has a purity of 98% to 99% and a lead content of less than 0.1%.
Third, resource and energy utilization indicators
1. Total lead recovery /% >98 >97 >95
2. Total sulfur utilization rate /% ≥98 ≥96 ≥95
3. Comprehensive utilization of resources /% ≥95 ≥90 ≥85
4. Unit comprehensive energy consumption (standard coal/crude lead)/(kg/t) < 100 < 120 < 130
5. Unit power consumption/(kW·h/t) < 100 < 100 < 100
Fourth, pollutant production indicators (before end treatment)
1. Lead content of slag /% < 1.8 < 1.9 < 2.0
2. Separator (accounting for the quality of the product after dismantling of the waste battery
Percentage) /% 1.0 to 3.0 1.0 to 3.0 1.0 to 3.0
3. Sulfur dioxide mass fraction a (acid production process) /% 8.0 ~ 10.0 3.5 ~ 4.5 1.0 ~ 3.5
4. Sulfur dioxide mass concentration (pretreatment desulfurizer
Art)/(mg/m3) ≤ 460 ≤ 760 ≤ 960
V. Waste recycling and utilization indicators
1. Plastic recovery rate /% ≥99 ≥98 ≥95
2. Waste electrolyte comprehensive utilization rate /% >98 >95 >90
3. Waste water recycling rate /% >95 >93 >90
Sixth, environmental management requirements
1. Environmental laws and regulations are in compliance with relevant national and local laws and regulations. Pollutant emissions meet national and local pollutant discharge standards and total control requirements. Sewage permit and collection, storage, transportation and disposal of hazardous waste meet regulatory requirements
2. Production process environmental management
Each production process must have operational procedures, and work instructions for key positions must be provided; equipment that is prone to pollution and
There should be warning signs on the parts of waste generation; the production process can be graded; the environmental management system should be established, including
Including. environmental management procedures during start-up and shutdown and maintenance; new, modified, and expanded project management and acceptance procedures;
Storage and transportation system pollution control system; environmental monitoring management system; pollution accident emergency treatment plan, and performance
Practice; environmental management records and ledgers
Continued
Indicator level one level two level three
3. The environmental audit was carried out in accordance with the requirements of the Interim Measures for Clean Production Audit, and all of them were implemented with no or low-cost schemes. Local environmental protection department evaluated the cleaner production plan
4. Environmental management system
Established operation according to GB/T 24001
Environmental management system, related environmental management
Handbook, program files and working papers
Ready
Sound environmental management system, original records and statistical data are complete and effective
5. Solid waste treatment and disposal
Properly dispose of general industrial solid waste. Dangerous waste such as lead dust is detoxified according to relevant requirements
Dispose of. Hazardous waste management plans should be developed (including measures to reduce the amount and hazard of hazardous waste generation and
Hazardous Waste Storage, Utilization, Disposal Measures) To the local environmental protection supervisor of the local people's government at or above the county level
The department has filed the record. Report the production of hazardous waste to the local environmental protection department of the local people's government at or above the county level
Relevant information on types, production, flow, storage, disposal, etc. Should be directed to the generation, collection, and
Storage, transportation, utilization, disposal, development of accident prevention measures and emergency plans, and to the county
The local environmental protection department of the local people's government shall file the record
6. Relevant environmental management The collection and transportation of waste lead-acid batteries is strictly in accordance with the hazardous waste management procedures; the management of raw material suppliers; the environmental management procedures of the partners and service providers are complete.
a Regenerate the crude lead main grade corresponding to the corresponding level.
Table 2 Clean production index requirements for lead recycling industry (hydrometallurgy)
Indicator level one level two level three
First, the production process and equipment requirements
Automatic crushing and sorting system mechanized crushing and sorting
1. Preparation technology and equipment
Pre-desulfurization
2. Production process and equipment electrolytic deposition process equipment, electric reduction process equipment, automatic ingot casting machine
Second, product indicators
Electrolytic lead meets GB/T 469 lead standard
Third, resource and energy utilization indicators
1. Total lead recovery /% >99 >98 >95
2. Total sulfur utilization rate /% ≥99 ≥97 ≥95
3. Comprehensive utilization of resources /% ≥95 ≥90 ≥85
4. Current efficiency /% ≥ 96 ≥ 95 ≥ 92.5
5. DC unit consumption/(kW · h/t) ≤ 550 ≤ 700 ≤ 800
6. Unit comprehensive energy consumption (standard coal/electricity lead)/(kg/t) ≤ 280 ≤ 320 ≤ 360
Fourth, pollutant production indicators (before end treatment)
1. Lead content of slag /% < 1.6 < 1.8 < 2.0
2. Separator (accounting for the quality of the product after dismantling the waste battery
Percentage) /% 1.0 to 3.0 1.0 to 3.0 1.0 to 3.0
V. Waste recycling and utilization indicators
1. Plastic recovery rate /% ≥99 ≥98 ≥95
2. Comprehensive utilization rate of waste electrolyte /% ≥98 95～98 90～95
3. Waste water recycling rate /% >95 >93 >90
Sixth, environmental management requirements
1. Environmental laws and regulations are in compliance with relevant national and local laws and regulations. Pollutant emissions meet national and local pollutant discharge standards and total control requirements. Sewage permit and collection, storage, transportation and disposal of hazardous waste meet regulatory requirements
Continued
Indicator level one level two level three
2. Production process environmental management
Every production process must have operating procedures, work instructions for key positions, equipment and waste that are likely to cause pollution.
There must be warning signs on the parts of the production; the production process can be graded
It is necessary to establish an environmental management system, including. environmental management procedures for start-stop work and shutdown maintenance; new, modified,
Expansion project management and acceptance procedures; pollution control system for storage and transportation systems; environmental monitoring management system; pollution accidents
Emergency response plan and drills; environmental management records and ledgers
3. The environmental audit conducted a clean production audit in accordance with the requirements of the Interim Measures for Clean Production Audit, and all of them implemented a no-low and low-cost plan. Local environmental protection department evaluated the cleaner production plan
4. Environmental management system
Established operation according to GB/T 24001
Environmental management system, related environmental management
Handbook, program files and working papers
Ready
Sound environmental management system, original records and statistical data are complete and effective
5. Solid waste treatment and disposal
Properly dispose of general industrial solid waste. For hazardous waste such as lead dust, it is harmless according to relevant requirements.
Set. Hazardous waste management plans should be developed (including measures to reduce the amount and hazard of hazardous waste generation and hazards)
Waste storage, utilization, and disposal measures shall be prepared by the local environmental protection department of the local people's government at or above the county level.
case. Report the types and production of hazardous wastes to the local environmental protection authorities of the local people's governments at or above the county level
Raw materials, flow, storage, disposal and other relevant information. Should be directed to the generation, collection, storage, transportation of hazardous waste,
Use and dispose of, develop accident prevention measures and emergency plans, and report to local people's governments at or above the county level
Environmental protection department for record
6. Relevant party environmental management The collection and transportation of waste lead-acid batteries is strictly in accordance with the hazardous waste management procedures; the environmental management procedures of the partners and service providers are complete.
5 data acquisition and calculation methods
5.1 Sampling and monitoring
The sampling and monitoring of various pollutant production indicators (before end treatment) of this standard shall be carried out in accordance with the monitoring methods specified by the State, and the pollutants shall be concentrated.
The degree of measurement is based on the method criteria listed in Table 3.
Table 3 Standards for determination of pollutants
Contaminant project method standard name method standard number
Lead solid wastes - Determination of copper, zinc, lead and cadmium - Atomic absorption spectrophotometric method GB/T 15555.2
Determination of sulphur dioxide in exhaust gas from fixed pollution sources - Method of iodine method HJ/T 56-2000 Determination of sulphur dioxide in exhaust gas from sulphur dioxide fixed source of pollution Statistic potential electrolysis method HJ/T 57-2000
5.2 Calculation method of related indicators
5.2.1 Total lead recovery
In the lead smelting process, the amount of metal lead entering the lead smelting product accounts for the total amount of lead in the raw material. Calculated as follows.
Pb
Pb
Pb
100%
PR
= ×
Where. RPb--total lead recovery, %;
PPb--the amount of metal lead entering the lead smelting product, t/a;
SPb - lead content in raw materials, t/a.
5.2.2 Total sulfur utilization
Refers to the utilization rate of sulfur in raw materials in the process of recycling lead smelting through various recycling methods, excluding waste gas
End treatment and discharge of sulfur into the environment. Its calculation formula is as follows.
100%
PR
= ×
Where. RS - total sulfur utilization rate, %;
PS--the total amount of sulfur recovered during the crude lead smelting process, t/a;
SS - the amount of sulfur in the raw material, t/a.
5.2.3 Comprehensive utilization of resources
Refers to the mass ratio of the total amount of actual recycled materials of the waste lead storage battery to the total amount of waste lead storage batteries. Calculated as follows.
1 2 3 100%n
GGGG
= ×"
Comprehensive utilization of resources
Where. G1--the first product quality;
G2--the second product quality;
G3--the third product quality;
Gn--the nth product quality;
G total - the total mass of waste batteries.
5.2.4 Unit comprehensive energy consumption
The ratio of the total energy consumption obtained by the enterprise after comprehensive calculation to the lead production of the enterprise during the statistical period of the same plan during the planning period. Calculation
The formula is as follows.
Ui 1 000
EE
= ×
Where. Eui--unit comprehensive energy consumption (standard coal/lead), kg/t;
Ei--the amount of energy consumed (standard coal) consumed during the statistical period of the enterprise plan, t;
Qi--In the same plan period, the company's lead production, t.
Note. Comprehensive calculation. The actual amount of various energy sources actually consumed is converted into the sum of primary energy according to the specified calculation method and unit. Comprehensive energy consumption master
It should include primary energy (such as coal, oil, natural gas, etc.), secondary energy (such as steam, electricity, etc.) and energy consumption directly used for production (such as cold
Water, compressed air, etc., but does not include energy consumption for power consumption (such as power generation, boilers, etc.). Specific comprehensive energy consumption according to GB/T 2589
Calculation.
5.2.5 Unit power consumption
Refers to the production of unit lead (t) in the process of reducing lead, the amount of electricity consumed (kW·h). Total electricity consumed during the production of reduced lead
The ratio of (kW·h) to the total lead production (t) in the same period. Calculated as follows.
Total power consumption
Total lead production
Where. W -- unit power consumption, kW · h/t; electricity
W total power consumption - total power consumption, kW · h;
The total amount of lead produced by W--the total amount of lead reduced or the total amount of lead produced, t.
5.2.6 Lead content of slag
Refers to the total amount of elemental lead in the lead slag and the mass percentage of the total amount of lead slag. Calculated as follows.
100%
= × lead in slag
Total slag
Slag lead ratio
Where. G - lead content in slag, t; lead in slag
The total amount of G slag - the total amount of slag, t.
5.2.7 Current efficiency
The percentage of the ratio of the amount of metal actually deposited on the cathode to the theoretical amount of precipitation during electrolytic production. Calculated as follows.
100%G
qItN
η = ×
Where. η--current efficiency, %;
G--the actual precipitation amount of the cathode of the N electrolytic cells in the energization time t, g;
Q--electrochemical equivalent, g/(A · h), lead electrification equivalent is 3.867 g/(A · h);
I--the current intensity through the electrolytic cell, A;
T--electrolytic energization time, h;
N--Number of electrolytic cells.
5.2.8 DC unit consumption
The electric energy consumed by the cathode per unit weight of metal lead (t) during electrolysis. Calculated as follows.
310VW
Qη= ×
Where. W--DC unit consumption, kW·h/t;
V--slot voltage, V;
Q--electrochemical equivalent, g/(A · h), lead electrification equivalent is 3.867 g/(A · h);
η - current efficiency, %.
6 Standard implementation
This standard is supervised and implemented by the environmental protection administrative department of the people's government at or above the county level.
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