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HJ 1035-2019 English PDF

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HJ 1035-2019: Technical specification for application and issuance of pollutant permit Inorganic chemical industry
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Basic data

Standard ID HJ 1035-2019 (HJ1035-2019)
Description (Translated English) Technical specification for application and issuance of pollutant permit Inorganic chemical industry
Sector / Industry Environmental Protection Industry Standard
Word Count Estimation 80,836
Date of Issue 2019-08-13
Date of Implementation 2019-08-13
Issuing agency(ies) Ministry of Ecology and Environment

HJ 1035-2019: Technical specification for application and issuance of pollutant permit Inorganic chemical industry


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Technical specification for application and issuance of pollutant permit Inorganic chemical industry National Environmental Protection Standard of the People's Republic Sewage permit application and issuance technical specifications Inorganic chemical industry Technical specification for application and issuance of pollutant permit Inorganic chemical industry Published on.2019-08-13 2019-08-13 Implementation Ministry of Ecology and Environment released - i -

Content

Foreword...ii 1 Scope...1 2 Normative references...1 3 Terms and Definitions...2 4 Basic requirements for reporting the discharge unit...3 5 Corresponding discharge ports and permitted emission limits for producing sewage nodes...31 6 Possible technical requirements for pollution prevention and control...36 7 Self-monitoring management requirements...37 8 Environmental Management Account and Emission Permit Execution Report Compilation Requirements...40 9 Actual emissions accounting method...44 10 Compliance Determination Method...47 Appendix A (informative appendix) recommended feasible technology for waste gas and wastewater treatment...50 Appendix B (informative appendix) Environmental Management Accounting Record Reference Table...53 Appendix C (informative appendix) manual monitoring report example table...60 Appendix D (informative appendix) Contents of the implementation report of the pollutant discharge permit for inorganic chemical industry sewage units...61 - ii -

Foreword

To implement the "Environmental Protection Law of the People's Republic of China" Water Pollution Prevention and Control Law, Law of the People's Republic of China on Soil Pollution Prevention and Control, and other laws and regulations, and the General Office of the State Council on Printing and Controlling Pollutants Notice of Implementation Plan for Emission Permit System (Guo Dang Fa [2016] No. 81) and "Measures for the Administration of Sewage Permits (Trial)" (Ministry of Environmental Protection) Order No. 48), improve the technical support system for pollutant discharge permits, and guide and regulate the application and issuance of pollutant discharge permits for inorganic chemical industry pollutant discharge units Work to develop this standard. This standard specifies the basic conditions for the application and issuance of pollutant discharge permits for inorganic chemical industry pollutant discharge units, and the permitted emission limits. Environmental management for identification, actual emissions accounting and compliance determination methods, self-monitoring, environmental management ledger and discharge permit execution report Requirements, put forward the feasible technical requirements for pollution prevention and control of inorganic chemical industry sewage unit. Appendix A to Appendix D of this standard are informative annexes. This standard is the first release. This standard is formulated by the Department of Environmental Impact Assessment and Emission Management of the Ministry of Ecology and Environment, and the Department of Regulations and Standards. This standard is mainly drafted by. Environmental Engineering Evaluation Center of the Ministry of Ecology and Environment, China Inorganic Salt Industry Association, Chinese Academy of Sciences Process Engineering Institute, Beijing Shenzhou Ruilin Environmental Technology Research Institute Co., Ltd., Qingdao University of Science and Technology, Shandong Province Construction Project Environmental Review Service Center. This standard was approved by the Ministry of Ecology and Environment on August 13,.2019. This standard has been implemented since August 13,.2019. This standard is explained by the Ministry of Ecology and Environment. - 1 - Sewage permit application and issuance technical specification inorganic chemical industry

1 Scope of application

This standard specifies the basic conditions for the application and issuance of pollutant discharge permits for inorganic chemical industry pollutant discharge units, and the permitted emission limits. Environmental management such as determination, actual emissions accounting, compliance determination methods, and self-monitoring, environmental management ledgers, and discharge permit execution reports According to the requirements, the feasible technical requirements for pollution prevention and control of inorganic chemical industry were put forward. This standard is applicable to guide the inorganic chemical industry pollutant discharge unit to fill in the "Sewage Permit Application Form" and the national sewage permit management information The platform application system fills in relevant application information, and is also applicable to guide the issuing authority to review and determine the inorganic chemical industry sewage permit permit. Claim. This standard is applicable to the management of pollutant discharge permits for atmospheric pollutants and water pollutants discharged by inorganic chemical industry pollutant discharge units, including In the economic economic industry classification (GB/T 4754), inorganic acid production 2611, inorganic alkali production 2612, inorganic salt production 2613 and other foundations Manufacture of chemical raw materials in the manufacture of inorganic chemical industrial products in 2619. Emission from other chemical production units that use the above substances as by-products The discharge permit management of atmospheric pollutants and water pollutants is not applicable to this standard, and the application of the pollutant discharge permit and the technical regulations for the issuance of the corresponding industries are implemented. Fan; production of biological hydrogen, general gas (except electrolytic hydrogen), rare gases, liquid air and compressed air, etc. The discharge permit management of atmospheric pollutants and water pollutants discharged by sewage units shall refer to the General Rules for Application and Issuance of Pollution Discharge Permits (HJ ) 942) Execution. In the inorganic chemical industry sewage disposal unit, the production facilities and discharge ports of the "Fire Power Plant Air Pollutant Emission Standards" (GB 13223) shall be implemented. Applicable to the Technical Specification for Application and Issuance of Pollution Discharge Permits in Thermal Power Industry (Annex 1 of Water Body [2016] No. 189); The production facilities and discharge ports of the Gas Pollutant Emission Standard (GB 13271) are applicable to the “Application for Pollution Discharge and the Issuance of Technical Boilers” (HJ 953). Inorganic chemical industrial pollutant discharge units that do not stipulate this standard but emit industrial waste water, waste gas or toxic and harmful pollutants specified by the state. Other sewage facilities and discharges shall be implemented in accordance with the General Rules for the Application and Approval of Pollution Discharge Permits (HJ 942).

2 Normative references

The contents of this standard refer to the following documents or their terms. For undated references, the valid version applies to this standard. quasi. GB 8978 Integrated Wastewater Discharge Standard GB 9078 industrial furnace kiln air pollutant discharge standards GB 13223 Standard for emission of atmospheric pollutants from thermal power plants GB 13271 Boiler Air Pollutant Emission Standard GB 14554 Odor Pollutant Emission Standard GB 15581 caustic soda, polyvinyl chloride industrial pollutant discharge standards GB 16297 Integrated emission standards for atmospheric pollutants GB 26131 Nitric acid industrial pollutant discharge standard GB 26132 Sulfuric acid industrial pollutant discharge standard GB 31573 Pollutant Standard for Pollutants in Inorganic Chemical Industry - 2 - GB/T 4754 National Economic Industry Classification GB/T 16157 Determination of particulate matter in fixed pollution source exhaust gas and sampling method of gaseous pollutants GB/T 32123 Cyanide-containing wastewater treatment and disposal specifications HJ 75 Fixed Pollution Source Flue Gas (SO2, NOx, Particulate Matter) Emissions Continuous Monitoring Technical Specification HJ 76 Technical requirements and test methods for continuous monitoring system for flue gas (SO2, NOx, particulate matter) from stationary sources HJ 493 Technical regulations for the preservation and management of water sampling samples HJ 494 Water Quality Sampling Technical Guidance HJ 495 water quality sampling plan design technical regulations HJ 608 sewage unit coding rules HJ 819 General Guidelines for Self-Monitoring Technical Units of Sewage Units HJ 942 General Regulations for the Application and Issuance of Pollution Discharge Permits HJ 953 Sewage Permit Application and Issuance Technical Specification Boiler HJ/T 55 Technical Guidelines for the Monitoring of Unorganized Emissions of Air Pollutants HJ/T 91 Surface Water and Wastewater Monitoring Technical Specifications HJ/T 194 Technical Specifications for Manual Air Quality Monitoring HJ/T 212 pollution source online automatic monitoring (monitoring) system data transmission standard HJ/T 353 Water Pollution Source Online Monitoring System Installation Technical Specification (Trial) HJ/T 354 Water Pollution Source Online Monitoring System Acceptance Technical Specification (Trial) Technical Specifications for Operation and Assessment of HJ/T 355 Water Pollution Source Online Monitoring System (Trial) HJ/T 356 Water Pollution Source Online Monitoring System Data Validity Discrimination Technical Specification (Trial) HJ/T 397 Fixed Source Exhaust Gas Monitoring Technical Specification "13th Five-Year Plan" Ecological Environmental Protection Plan (Guo Fa [2016] No. 65) Technical Requirements for Standardized Remediation of Sewage Discharges (Trial) (National Environmental Protection Agency Environmental Supervision [1996] No. 470) Circular on Carrying out the Management of Elevated Source Pollution Discharge Permits in Thermal Power, Papermaking Industry and Beijing-Tianjin-Hebei Pilot City (Circular Water Body [2016] No. 189) Announcement on the Implementation of Special Emission Limits for Air Pollutants (Announcement No. 14 of.2013) Reply to the Issues Concerning the Implementation of Special Emission Limits for Air Pollutants (Environmental Letter [2016] No. 1087) Announcement on the Implementation of Special Emission Limits for Air Pollutants in the Beijing-Tianjin-Hebei Air Pollution Transmission Channel City (Announcement No. 9 of.2018) National Directory of Hazardous Wastes (Order No. 39 of the Ministry of Environmental Protection) Notice on Strengthening Prevention and Control of Nitrogen and Phosphorus Pollution from Fixed Pollution Sources (Circular Water Body [2018] No. 16)

3 Terms and definitions

The following terms and definitions apply to this standard. 3.1 Inorganic chemical industry pollutant discharge unit It refers to the production of inorganic acids, inorganic bases, inorganic salts, other basic chemical raw materials, etc. from natural resources, industrial products and industrial by-products. Industrial sewage unit of machine chemical products. - 3 - 3.2 Permitted emission limits Refers to the maximum emission concentration (rate) and maximum emission of pollutants allowed by the discharge unit specified in the discharge permit. 3.3 special period special periods Refers to the environmental quality deadlines and other relevant environmental management regulations formulated by the local people's government according to law, and for the sewage disposal units. Periods with special requirements for pollutant discharge, including heavy pollution weather response period and winter defense period.

4 Basic requirements for reporting the discharge unit

4.1 General principles Inorganic chemical industry sewage disposal units shall, in accordance with the requirements of this standard, report to the National Pollution Discharge Permit Management Information Platform Application System Corresponding information sheet in the certifiable application form. The local ecological environment authorities not included in the drop-down menu of the filling system have regulations to fill in the report. If the pollutant discharge unit thinks it needs to be reported, it may add the content by itself. The local ecological environment competent department at or above the municipal level in the district may increase the need for the pollutant discharge permit according to the local regulations on environmental protection. The contents stated in the report will be filled in the management system of the pollutant discharge permit management information platform. Content" column. Did not obtain the approval opinions of the environmental impact assessment of the construction project according to law, or did not obtain the local people's government according to the relevant state regulations The pollutant discharge unit of the relevant certification materials issued by the rectification and regulation shall not meet the permissible emission concentration. The pollutant discharge unit sought, as well as other pollutant discharge units that need to correct the behavior according to the regulations, should report the information on the application for the discharge permit for the first time. The “Revision Regulations” column in the National Pollution Discharge License Management Information Platform Declaration System proposes a rectification plan. The basic situation of the inorganic chemical industry pollutant discharge unit shall be reported according to the actual situation, and the authenticity, legality and integrity of the submitted application materials shall be submitted. Negative legal responsibility. 4.2 Basic information of sewage disposal units The basic information of the pollutant discharge unit includes the name of the unit, whether it needs to be corrected, the license management category, the postal code, the industry category, and whether it is put into production. And the date of production, the latitude and longitude of the production and operation site, and whether the location is an environmentally sensitive area (such as the atmospheric key control area, the total phosphorus total nitrogen control area), Whether it is located in the industrial park and its industrial park name, environmental impact assessment approval number (record number), identification or filing number, major pollution Gross distribution plan document number, total particulate matter index, total sulfur dioxide index, total nitrogen oxides index, total chemical oxygen demand Volume indicators, total ammonia nitrogen indicators, other indicators of total pollutants (if any). 4.3 Main products and production capacity 4.3.1 General principles When reporting the main products and production capacity, you should choose "inorganic acid", "inorganic alkali", "inorganic salt" or "other basic chemical raw materials", and then specific Fill in the actual production product name. The pollutant discharge unit shall fill in the relevant main production unit and main work in the declaration system of the pollutant discharge permit management information platform according to the requirements of this standard. Order, production facilities, production facility number, facility parameters, product name, production capacity and unit of measurement, design annual production time and other options Information such as items. - 4 - 4.3.2 Main production unit The main production units are required, which are divided into raw material pretreatment/preparation, reaction unit, crude product separation, product refining, dry packaging, and common use. Unit, etc. 4.3.3 Main production processes The main production processes are required, including but not limited to the following. Raw material pretreatment/preparation. crushing, grinding, drying, batching, etc.; Reaction unit. calcination (calcination), electrolysis, neutralization, synthesis, oxidation, reduction, carbonization, multi-effect evaporation, crystallization, etc.; Crude separation. filtration, crystallization, distillation, etc.; Product refining. extraction, recrystallization, washing, rectification, etc.; Dry packaging. drying, packaging, granulation, etc.; Common units. storage, gas/fuel preparation, others. The production process is reported in Tables 1.1 to 1.5. Other inorganic chemical industry sewage units can be reported with reference to similar industry processes. Table 1.1 Production Process Table of Major Inorganic Acid Industry Industry production process Raw material pretreatment/production Reaction unit Rough grade Product refinement Drying bag Inorganic acid sulfuric acid Sulphur-based acid sulphur, filtered sulfur, conversion and absorption /// Pyrite pyrolysis, roasting, conversion and absorption /// Gypsum acid compounding, drying and calcining, conversion and absorption /// Nitric acid Dilute nitric acid production Ammonia evaporation, ammonia mixing Ammonia oxidation, heat recovery, suction / Bleaching / Straight nitrate method Nitric acid production) Ammonia evaporation, ammonia mixing Ammonia oxidation, high pressure synthesis, absorb / Bleaching / Inter-nitrogen method Nitric acid production) Mixing Acid, concentrated nitric acid magnesium) Concentrated, cooled, condensed / Bleached, cold Phosphoric acid a thermal phosphorus burning, hydration / Concentrate Color, arsenic removal Note. a Phosphoric acid production in this specification includes only the thermal phosphoric acid production process. Table 1.2 Production Process Table of Major Inorganic Base Industry Industry production process raw material pretreatment/preparation reaction unit crude separation Product precision Drying bag Inorganic base Caustic soda acid) Electrolytic salting and refining Electrolysis, caustic soda evaporation, chlorine Hydrogen absorption Chlorine gas soda ash Natural alkali method purification evaporation, calcination filtration centrifugal packaging Refined by alkali Ammonia, carbonization, calcination, crystallization Filtered centrifugal packaging Ammonia alkali method Refined, limestone calcination Ammonia, carbonization, calcination, Mother liquor Filtered centrifugal packaging - 5 - Table 1.3 Production Process Table of Major Inorganic Salt Industry Industry production process Raw material pre-treatment Management/preparation Reaction unit crude separation product refined dry packaging Inorganic Calcium carbide electrothermal method Calcination, baking Dry, broken Broken, sieved Reduction (calcium furnace)/broken / Chromium salt (weight Chromic acid sodium) Liquid phase method Grinding, hitting Oxidation, filtration, carbon Chemical Evaporation, filtration, concentration and crystallization, separation and packaging Solid phase roasting Grinding Roasting, leaching, solid-liquid Separation, neutralization, over Filtration, acidification Filtration, one acid steaming, two Acid vapor Crystallization, separation packaging Liquid phase method, Solid phase roasting / reaction, drying, roasting// packaging Dry chromium slag Detoxification Drying reduction /// Wet chromium residue Detoxification Wet grinding, hitting Acidification, reduction filtration, separation // Disulfide Carbon Natural gas law Liquid sulfur Preparation, natural Gas pretreatment a Synthesis/distillation / Cyanide Sodium b Acrylonitrile Production method / Alkali absorption evaporation, crystallization, dry molding packaging Light oil cracking Liquid ammonia gasification Cracking, dust removal, alkali suction Evaporation, crystallization, dry molding Angle Liquid ammonia Transformation Adsorption Synthesis, alkali absorption evaporation, crystallization, dry molding packaging Carbonic acid Carbonization grinding Roasting, leaching, passing Filtration, carbonization Dry screening package Silicic acid Dry ingredient roasting cooling/packaging White charcoal Precipitation/hydration reaction aging, filtration, washing / Dry, powder Broken, packed Gas phase method Gasification, water Gather Cyclone separation, deacidification, cold Dry, bag - 6 - Continued Industry production process Raw material pretreatment / preparation Reaction unit crude separation product refined dry packaging Inorganic salt Lithium carbonate Brine calcination spray drying Calcination, leaching, solid Liquid separation, lithium deposition Separation / Dry, bag Solid phase sulfuric acid grinding Crystal form conversion, sulfuric acid Roasting, leaching, solid Liquid separation, lithium deposition Separation / Dry, bag Light calcium carbonate carbonization Calcination, digestion, carbon Separation / Dry, bag Feed grade phosphoric acid Calcium salt Wet grinding Acid extraction, acid , neutralization filter/ Dry, bag Dithion Sodium formate method/synthesis Crystallization Dry, bag Note. a includes conventional natural gas, unconventional natural gas, and associated gas in the oil field. b refers to the production of solid sodium cyanide, which can be reported by reference to its corresponding production process. Table 1.4 Main other chemical raw materials industry production process table Industry production process Raw material pre-treatment Management/preparation Reaction unit crude separation Product precision Drying bag Other basics Learning materials Yellow phosphorus Electric furnace method Broken, baked Reduction (yellow phosphorus electric furnace), water Quenching (or air cooling) Condensation Washing essence Phosphorus acid/phosphorus mud treatment// / Table 1.5 Other inorganic chemical industry production process table Industry production process raw material pretreatment/preparation reaction unit crude separation product refining Drying bag Other inorganic chemistry / Broken, ground, baked Dry, ingredients, etc. Calcination (calcination), electrolysis, Neutralization, synthesis, oxidation, and Original, carbonized, multi-effect evaporation, Crystallization, etc. Filtering, knotting Crystal, distillation, etc. Extraction, re-knotting Crystal, washing, Rectification, etc. dry, package, Granulation, etc. 4.3.4 Production facilities Production facilities are divided into required and optional items. The specific requirements are as follows. a) Facilities that characterize the production capacity of the production unit are required, such as crushers or mills for raw material pretreatment/preparation units, and reaction units Type reaction furnace, various extraction or filtration equipment for crude separation unit, packaging machine for dry packaging unit, etc.; b) Production facilities for generating or discharging process wastewater and waste gas are required; c) Gas generators, torches, etc. are required; d) Other production facilities are optional. This standard has not been stipulated, but produces industrial waste gas, wastewater and has clear national or local emission (control) standards, corresponding production Facilities are required. The general production facilities of the inorganic chemical industry sewage disposal unit can be seen in Table 2. The production facilities of some major industrial products can be found in Table 3. - 7 - Table 2 General production facility table Industry production unit production process general production facilities all Raw material pre-treatment Management/preparation Crusher, mill, etc. Drying drum dryer, etc. Ingredient batching tank (tank), etc. Reaction unit Roaster, boiling furnace, calciner, oxidation tower, electrolysis tank, rotary kiln, tunnel kiln, horseshoe kiln, Push plate kiln, roller kiln, carbonization tower, light oil cracking furnace, ore-heating electric furnace, phosphorus burning tower, evaporator, Distillation tower, etc. Crude separation evaporator, leaching tank, cooling/condensing equipment, filtration equipment, centrifuge, extraction tower, etc. Product refined distillation column, washing tower, evaporator, crystallizer, filtration equipment, centrifuge, etc. Dry packaging Drying tower (furnace/kiln), drum dryer, fluidized bed, granulator (tower), pulverizer, vibration Sieve, packaging machine, cool alkali furnace, etc. Common unit Storage materials and product storage areas (facilities), etc. Fuel preparation gas generator, etc. Processing (storage) facilities, torches, etc. for other auxiliary production systems Table 3 Table of production facilities of some major industries Industry production process Raw material pretreatment/production Reagent unit crude product separation Inorganic acid sulfuric acid Sulfuric ...

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