US$149.00 · In stock Delivery: <= 2 days. True-PDF full-copy in English will be manually translated and delivered via email. GB/T 9735-2008: Chemical reagent -- General method for the determination of heavy metals Status: Valid GB/T 9735: Evolution and historical versions
Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
GB/T 9735-2008 | English | 149 |
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Chemical reagent -- General method for the determination of heavy metals
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GB/T 9735-2008
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GB/T 9735-1988 | English | 199 |
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Chemical reagent--General method for the determination of heavy metals
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GB/T 9735-1988
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PDF similar to GB/T 9735-2008
Basic data Standard ID | GB/T 9735-2008 (GB/T9735-2008) | Description (Translated English) | Chemical reagent -- General method for the determination of heavy metals | Sector / Industry | National Standard (Recommended) | Classification of Chinese Standard | G60 | Classification of International Standard | 71.040.30 | Word Count Estimation | 5,528 | Date of Issue | 2008-05-15 | Date of Implementation | 2008-11-01 | Older Standard (superseded by this standard) | GB/T 9735-1988 | Quoted Standard | GB/T 602; GB/T 603; GB/T 6682 | Adopted Standard | ISO 6353-1-1982, NEQ | Regulation (derived from) | National Standard Approval Announcement 2008 No.8 (Total No.121) | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | Summary | This standard specifies the acetic acid in the medium into heavy metal sulfides and general method by visual colorimetric assay. This standard applies to the determination of heavy metals in Pb chemical reagents. Saturated aqueous solution of hydrogen sulfide colorimetric detection range is 0. 3��g/mL ~ 2��g/mL (Pb), sulfide-glycerol colorimetric detection range is 0. 4��g/mL ~ 3��g/mL (as Pb). |
GB/T 9735-2008: Chemical reagent -- General method for the determination of heavy metals---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Chemical reagent. General method for the determination of heavy metals
ICS 71.040.30
G60
National Standards of People's Republic of China
Replacing GB/T 9735-1988
General method for determination of heavy metals Chemicals
(ISO 6353-1. 1982, Reagentsforchemicalanalysis-
Part 1. Generaltestmethods, NEQ)
Posted 2008-05-15
2008-11-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
This standard and ISO 6353-1. 1982 "Chemical analysis of reagent --- Part 1. General test method" non-equivalent.
This standard replaces GB/T 9735-1988 "General method for the determination of heavy metals in chemical reagents," compared with the GB/T 9735-1988 Main
Changes are as follows.
--- Increased sodium sulfide - Determination of Heavy Metal glycerol method (Excerpts Chapter 1, Chapter 5).
The standard proposed by China Petroleum and Chemical Industry Association.
This standard by the National Standardization Technical Committee Chemistry Chemicals Branch (SAC/TC63/SC3) centralized.
This standard was drafted. Guangzhou Chemical Reagent Factory.
The main drafters of this standard. Yu Xiaoqi, Fuqiong Lian, Liu Chao Yuan.
This standard was first published in 1988.
General method for determination of heavy metals Chemicals
1 Scope
This standard specifies the acetic acid in the medium heavy metals into sulfides with the general method of visual colorimetric assay.
This standard applies to the determination of heavy metals in the lead in terms of the chemical reagent. Colorimetric detection range for hydrogen sulphide saturated aqueous
0.3μg/mL ~ 2μg/mL (as Pb); sodium sulfide - Glycerin colorimetric detection range of 0.4μg/mL ~ 3μg/mL
(Pb).
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
GB/T 602 Determination of impurities in chemical reagents prepared standard solution (GB/T 602-2002, ISO 6353-1. 1982, NEQ) with
GB/T 603 chemical reagent test method Preparations of articles (GB/T 603-2002, ISO 6353-1 with. 1982,
NEQ)
GB/T 6682 analytical laboratory use specifications and test methods (GB/T 6682-2008, ISO 3696. 1987, MOD)
3 PRINCIPLE OF THE METHOD
Heavy metal ions and negative ions generated through a divalent sulfur sulfide precipitation in acid medium. Low content of heavy metal elements to form a stable
Given dark suspensions, for visual colorimetric determination of heavy metals.
4 Reagents
Unless otherwise specified in this standard, the standard solution used in formulations and products, according to GB/T 602, the provisions of the preparation of GB/T 603, the experiment
Water should be consistent with GB/T 6682 water in three specifications, are used in mass fraction in% of the solution.
5 Determination
5.1 Colorimetric hydrogen sulphide saturated aqueous
Sampling according to product standards and the preparation of test solution (pH value of the test solution was adjusted to 4 if necessary), acetic acid solution was added 0.2mL
(30%), diluted to 25mL, 10mL of water was added a saturated hydrogen sulfide freshly prepared, shake, place 10min. The standard solution was dark and
Comparison of colorimetric solution.
Preparation of the standard color solution containing a predetermined ratio of the amount taken is lead (Pb) and the amount of the standard solution of the substrate (if the sample solution containing no substrate or substrate
No effect on the determination of the presence, it does not add), with the same volume of test solution at the same time the same treatment.
5.2 Sodium sulfide - Glycerin colorimetry
5.2.1 sulfide - Preparation of glycerol solution
Weigh 5g mixture of sodium sulfide, dissolved in 10mL water and 30mL glycerol, protected from light seal, valid for one month.
5.2.2 Determination
Sampling according to product standards and the preparation of test solution (pH value of the test solution was adjusted to 4 if necessary), acetic acid solution was added 0.2mL
(30%), diluted to 25mL, 0.1mL sodium sulfide was added - glycerol solution, shake, place 10min. Dark standard colorimetric solution was
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