US$139.00 · In stock Delivery: <= 2 days. True-PDF full-copy in English will be manually translated and delivered via email. GB/T 9730-2007: Chemical reagent -- General method for the determination of oxalates Status: Valid GB/T 9730: Evolution and historical versions
Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
GB/T 9730-2007 | English | 139 |
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Chemical reagent -- General method for the determination of oxalates
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GB/T 9730-2007
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GB/T 9730-1988 | English | 199 |
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Chemical reagent--General method for the determination of oxalates
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GB/T 9730-1988
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PDF similar to GB/T 9730-2007
Basic data Standard ID | GB/T 9730-2007 (GB/T9730-2007) | Description (Translated English) | Chemical reagent -- General method for the determination of oxalates | Sector / Industry | National Standard (Recommended) | Classification of Chinese Standard | G60 | Classification of International Standard | 71.040.30 | Word Count Estimation | 5,562 | Date of Issue | 2007-09-26 | Date of Implementation | 2008-04-01 | Older Standard (superseded by this standard) | GB/T 9730-1988 | Adopted Standard | ISO 6353-1-1982, NEQ | Regulation (derived from) | China National Standard Approval Announcement2007 No.11 (Total No.111) | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | Summary | This standard specifies the azo compounds to convert oxalate into common approach with colorimetric assay. This standard applies to the determination of trace organic reagents oxalate. Spectrophotometric detection range 1��g/mL ~ 20��g/mL (in C2O4 dollars), visual colorimetric detection range of 0. 4 ��g/mL ~ 20��g/mL (in C2O4 dollars). |
GB/T 9730-2007: Chemical reagent -- General method for the determination of oxalates---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Chemical reagent. General method for the determination of oxalates
ICS 71.040.30
G60
National Standards of People's Republic of China
Replacing GB/T 9730-1988
Chemical Reagents
General method for determination of oxalate
(ISO 6353-1. 1982, Reagentsforchemicalanalysis-
Part 1. Generaltestmethods, NEQ)
Posted 2007-09-26
2008-04-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
This standard and ISO 6353-1. 1982 "Reagents for chemical analysis - Part 1. General test method" non-equivalent.
This standard replaces GB/T 9730-1988 "General method for determination of chemical reagents oxalates," compared with the GB/T 9730-1988 Cancel
1988 edition Appendix A.
The standard proposed by China Petroleum and Chemical Industry Association.
This standard by the National Standardization Technical Committee Chemistry Chemicals Branch (SAC/TC63/SC3) centralized.
This standard was drafted. Sinopharm Chemical Reagent Co., Ltd.
The main drafters of this standard. Chenhao Yun, Chen Hong.
This standard was first published in 1988.
Chemical Reagents
General method for determination of oxalate
1 Scope
This standard specifies the oxalate to convert azo compound with the general method of colorimetric determination.
This standard applies to the determination of trace organic reagent oxalate. Spectrophotometric detection range of 1μg/mL ~ 20μg/mL (in
C2O4 meter), visual colorimetric detection range of 0.4μg/mL ~ 20μg/mL (in C2O4 dollars).
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
GB/T 602 Determination of impurities in chemical reagents prepared standard solution (GB/T 602-2002, ISO 6353-1. 1982, NEQ) with
GB/T 603 chemical reagent test method Preparations of articles (GB/T 603-2002, ISO 6353-1 with. 1982,
NEQ)
GB/T 6682 analytical laboratory use specifications and test methods (GB/T 6682-1992, neq ISO 3696. 1987)
GB/T 9721 Chemicals General molecular absorption spectrophotometry (UV and visible part)
3 PRINCIPLE OF THE METHOD
In the medium of hydrochloric acid, oxalic acid with zinc reduced to glyoxylic acid, glyoxylic acid and hydrochloric acid phenylhydrazine reaction of glyoxylic acid phenylhydrazone. Adding an oxidizing agent,
The excess phenylhydrazine is converted to a diazonium salt, and then reacted with glyoxylic acid phenylhydrazone, generating azo compounds, pink in an acidic medium, it may be visually
Colorimetric or spectrophotometric determination of oxalate.
4 Reagents and materials
Unless otherwise specified in this standard, the standard solution, preparations and products, according to GB/T 602, the provisions of the preparation of GB/T 603, the experimental
Water should be consistent with GB/T 6682 in the three water specifications.
5 Instruments
5.1 General laboratory equipment.
5.2 Spectrophotometer shall comply with GB/T 9721's.
6 Determination
6.1 visual colorimetry
Sampling according to product standards and test solution preparation. Take 5mL sample solution into 25mL colorimetric tube, add 2mL of hydrochloric acid, 1g arsenic-free
Zinc, immediately incubated in a boiling water bath for 1min, standing out 2min, containing 0.25mL immediately poured into a solution of phenylhydrazine hydrochloride (10g/L) ratio of the color
Tube (without rendering zinc particles poured), washed three times with water colorimetric tube (using a pipette operation), each 1mL, will be incorporated into the lotion containing phenylhydrazine hydrochloride solution
Colorimetric tube (the volume of the solution at this time should not exceed 10mL). Incubated in a boiling water bath for 1min, rapidly cooled in running water, diluted hydrochloric acid
To 25mL, plus 0.25mL iron potassium cyanide solution (50g/L), and shake. The solution was pink with the standard comparative colorimetric solution.
Preparation of the standard developing solution is a specified amount than the oxalate (C2O4) standard solution, was diluted to 5mL, at the same time with the same volume of the same test solution
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