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GB/T 8704.3-2009 English PDF

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GB/T 8704.3-2009: Ferrovanadium -- Determination of sulfur content -- The infrared absorption method and the combustion-neutralization titration method
Status: Valid

GB/T 8704.3: Evolution and historical versions

Standard IDContents [version]USDSTEP2[PDF] delivered inStandard Title (Description)StatusPDF
GB/T 8704.3-2009English209 Add to Cart 3 days [Need to translate] Ferrovanadium -- Determination of sulfur content -- The infrared absorption method and the combustion-neutralization titration method Valid GB/T 8704.3-2009
GB/T 8704.3-1997English359 Add to Cart 3 days [Need to translate] Methods for chemical analysis of ferrovanadium. The infrared absorption method and the combustion neutralization titration method for the determination of sulfur content Obsolete GB/T 8704.3-1997
GB/T 8704.3-1988EnglishRFQ ASK 3 days [Need to translate] Methods for chemical analysis of ferrovanadium--The infrared absorption method for the determination of sulfur content Obsolete GB/T 8704.3-1988

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Basic data

Standard ID GB/T 8704.3-2009 (GB/T8704.3-2009)
Description (Translated English) Ferrovanadium -- Determination of sulfur content -- The infrared absorption method and the combustion-neutralization titration method
Sector / Industry National Standard (Recommended)
Classification of Chinese Standard H11
Classification of International Standard 77.100
Word Count Estimation 9,997
Date of Issue 2009-07-15
Date of Implementation 2010-04-01
Older Standard (superseded by this standard) GB/T 8704.3-1997
Quoted Standard GB/T 4010
Regulation (derived from) National Standard Approval Announcement 2009 No.9 (Total No.149)
Issuing agency(ies) General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary This standard specifies the use of infrared absorption method and combustion and titration of vanadium iron sulfur content. This section applies to the determination of vanadium iron sulfur content. Measuring range (mass fraction): from 0. 005% to 0. 120%.

GB/T 8704.3-2009: Ferrovanadium -- Determination of sulfur content -- The infrared absorption method and the combustion-neutralization titration method


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Ferrovanadium.Determination of sulfur content.The infrared absorption method and the combustion-neutralization titration method ICS 77.100 H11 National Standards of People's Republic of China Replacing GB/T 8704.3-1997 Determination of vanadium iron sulfur content Infrared absorption method and the combustion - neutralization titration method Posted 2009-07-15 2010-04-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released

Foreword

This Part replaces GB/T 8704.3-1997 "determination of sulfur content for chemical analysis of ferrovanadium The infrared absorption method and combustion - neutralization titration method." This portion of the GB/T 8704.3-1997 comparison, the main changes are. --- The method of one of the sample weight 0.500g, 0.200g two tranches adjusted to a file 0.200g; --- The method of one of the iron from the flux amount was adjusted to 0.50g 0.20g; --- The method of one of the first, second gear allows for the consolidation difference sulfur content of 0.005% to 0.015%, 0.002% allowable difference; --- The second method of determination by the scope of < 0.120% to 0.005% and 0.120%. This part is proposed by the China Iron and Steel Association. This part of pig iron and ferroalloy by the National Standardization Technical Committee. This section is drafted. Sichuan Investment Emei Ferroalloy (Group) Co., Ltd. The main drafters of this section. should Tang Hua, Fang Yan, Xuexiu Ping. This part of the standard replaces the previous editions are. --- GB/T 8704.3-1988, GB/T 8704.4-1988, GB/T 8704.3-1997. Determination of vanadium iron sulfur content Infrared absorption method and the combustion - neutralization titration method Warning --- Use this section shall be a person experiences regular laboratory work. This section does not point out all possible security asked question. Users have the responsibility to take appropriate safety and health practices and to ensure compliance with the conditions relevant national regulations.

1 Scope

This section GB/T 8704 regulations using infrared absorption method and combustion - neutralization titration method for the determination of vanadium iron sulfur content. This section applies to the determination of vanadium iron sulfur content. Measurement range (mass fraction). 0.005% and 0.120%.

2 Normative references

The following documents contain provisions cited by GB/T 8704 to the present, constitute provisions of this section. For dated reference documents Member, all subsequent amendments (not including errata content) or revisions do not apply to this section, however, encouraged to reach under this section Parties to research agreement to use the latest versions of these documents. For undated reference documents, the latest versions apply to this section. GB/T 4010 alloy chemical analysis and preparation of samples 3 Method One. The infrared absorption method 3.1 Principle The sample is heated in a high frequency induction furnace combustion oxygen flow generated by the oxygen contained sulfur dioxide infrared analyzer to the measuring chamber dioxide A sulfur absorbing specific wavelengths of infrared energy, which is proportional to the absorbed energy and the concentration of sulfur, based on the detection unit accepts the change in energy can be measured sulfur content. 3.2 Reagents and materials 3.2.1 acetone. sulfur content of the residue after evaporation is less than 0.0005%. 3.2.2 magnesium perchlorate, anhydrous, granular. 3.2.3 asbestos caustic soda, granular. 3.2.4 glass wool. 3.2.5 tungsten particles. sulfur content of less than 0.0002%, particle size 0.8mm ~ 1.4mm. 3.2.6 tin particles. sulfur content of less than 0.0002%, particle size 0.4mm ~ 0.8mm. If necessary, apply acetone (3.2.1) clean the surface and in the room Temperature and dried. 3.2.7 pure iron. purity of greater than 99.8%, a sulfur content of less than 0.0002%, particle size 0.8mm ~ 1.6mm. 3.2.8 Oxygen. The purity of more than 99.95%, if other levels of oxygen to obtain a low and consistent blank, can also be used. 3.2.9 Power Source gas. nitrogen or compressed air, which contaminants (oil and water) content of less than 0.5%. 3.2.10 porcelain crucible. diameter × height, 23mm × 23mm or 25mm × 25mm, and above 1200 ℃ high temperature furnace 4h or by burning oxygen burning to blank the lowest value. 3.2.11 crucible tongs. 3.3 instruments and equipment 3.3.1 Sulphur infrared absorption analyzer (sensitivity of 0.1 × 10-6), which means as shown in Figure 1.

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