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GB/T 6730.47-2017: Iron ores -- Determination of niobium content -- Sulfochlorophenol S spectrophotometric method
Status: Valid GB/T 6730.47: Evolution and historical versions
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| GB/T 6730.47-2017 | English | 199 |
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Iron ores -- Determination of niobium content -- Sulfochlorophenol S spectrophotometric method
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GB/T 6730.47-2017
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| GB/T 6730.47-1986 | English | 199 |
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Methods for chemical analysis of iron ores. The sulfochlorophenol S photometric method for the determination of niobium content
| Obsolete |
GB/T 6730.47-1986
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PDF similar to GB/T 6730.47-2017
Basic data | Standard ID | GB/T 6730.47-2017 (GB/T6730.47-2017) | | Description (Translated English) | Iron ores -- Determination of niobium content -- Sulfochlorophenol S spectrophotometric method | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | D31 | | Classification of International Standard | 73.060.10 | | Word Count Estimation | 10,182 | | Date of Issue | 2017-09-07 | | Date of Implementation | 2018-06-01 | | Older Standard (superseded by this standard) | GB/T 6730.47-1986 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | GB/T 6730.47-2017: Iron ores -- Determination of niobium content -- Sulfochlorophenol S spectrophotometric method
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Iron ores - Determination of niobium content - Sulfochlorophenol S spectrophotometric method
ICS 73.060.10
D31
National Standards of People's Republic of China
Replacing GB/T 6730.47-1986
Iron ores - Determination of niobium content
Chlorosulphonol S spectrophotometry
2017-09-07 Posted
2018-06-01 implementation
General Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
China National Standardization Administration released
Foreword
GB/T 6730 "iron ore" is divided into dozens of sections.
This section GB/T 6730 Part 47.
This section drafted in accordance with GB/T 1.1-2009 given rules.
This section instead of GB/T 6730.47-1986 "chemical analysis of iron ores chlorosulfonols S luminosity Determination of niobium," This section and
GB/T 6730.47-1986 compared to, in addition to editorial changes, the main technical changes are as follows.
--- The standard name was changed to "determination of niobium content of iron ore chlorosulfonol S spectrophotometry";
--- Added "warning" "normative references" "instrument" and "test report" chapter and content, the original chapter number has been adjusted accordingly;
--- Clear and standardized sample and sample preparation of the specific requirements;
--- The "sample size" to "sample size", and clear the weighing accuracy;
--- Removed the coefficient (1) of the coefficient "K" and "K" of the statement;
--- Added "to determine the results of the analysis."
This part is proposed by China Iron and Steel Association.
This part of the National Iron Ore and Direct Reduced Iron Standardization Technical Committee (SAC/TC317) centralized.
This part of the drafting unit. Ningbo Inspection and Quarantine Science and Technology Research Institute, Shanghai Entry-Exit Inspection and Quarantine, Metallurgical Industry Information Standards Research
Institute.
The main drafters of this section. Chen Hehai, Zhu Zhixiu, Tang Yun, Li Yulu, Chen Zi Bin, Ying Haisong, Liao Haiping, Zhang Aizhen.
This part of the standard replaces the previous version of the release.
--- GB/T 6730.47-1986.
Iron ores - Determination of niobium content
Chlorosulphonol S spectrophotometry
Warning --- personnel using this section should have formal laboratory work experience. This section does not indicate all possible safety issues
question. It is the user's responsibility to take appropriate safety and health measures and to ensure compliance with the requirements of the relevant state laws and regulations.
1 Scope
GB/T 6730 provisions of this part of the chlorosulfonate S spectrophotometric determination of niobium content.
This section applies to the determination of iron ore, iron ore, sinter and pellet niobium content. Determination of the range (mass fraction) .0.007% ~
0.350%.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version applies to this article
Pieces. For undated references, the latest edition (including all amendments) applies to this document.
GB/T 6682 analytical laboratory water specifications and test methods
Preparation of pre-dried samples for analysis of iron ores GB/T 6730.1
GB/T 8170 rounded repair rules and limit values of the representation and judgment
GB/T 10322.1 Iron ore sampling and sample preparation methods
GB/T 12806 laboratory glassware single standard line capacity bottle
GB/T 12807 Laboratory glassware graduated pipette
GB/T 12808 laboratory glassware single standard pipette
3 principle
The sample was decomposed by hydrofluoric acid, the insoluble residue was dissolved with potassium pyrosulfate and leached with tartaric acid. In 0.5mol/L ~ 2mol/L hydrochloric acid medium,
Niobium and chlorosulfonated S form a stable 1. 1 blue-green complex. The absorbance is measured at a wavelength of 650 nm, whereby the amount of niobium is measured.
Hydrofluoric acid destruction of niobium - chlorosulfonates S complex test solution as a reference, to increase the allowable amount of coexisting elements.
4 Reagents and materials
Unless otherwise indicated in the analysis, the use of only approved analytical reagent and in line with GB/T 6682 more than three distilled water or its
The purity of water.
4.1 potassium pyrosulfate.
4.2 Ammonium chloride.
4.3 Hydrochloric acid, p approximately 1.19 g/mL.
4.4 Nitric acid, p about 1.42 g/mL.
4.5 hydrofluoric acid, p approximately 1.15 g/mL.
4.6 Ammonium hydroxide, p about 0.90 g/mL.
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