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US$199.00 ยท In stock Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. GB/T 6730.14-2017: Iron ores -- Determination of calcium content -- Flame atomic absorption spectrometric method Status: Valid GB/T 6730.14: Evolution and historical versions
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB/T 6730.14-2017 | English | 199 |
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Iron ores -- Determination of calcium content -- Flame atomic absorption spectrometric method
| Valid |
GB/T 6730.14-2017
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| GB/T 6730.14-1986 | English | 279 |
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Methods for chemical analysis of iron ores. The flame atomic absorption spectrophotometric method for the determination of calcium and magnesium content
| Obsolete |
GB/T 6730.14-1986
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PDF similar to GB/T 6730.14-2017
Basic data | Standard ID | GB/T 6730.14-2017 (GB/T6730.14-2017) | | Description (Translated English) | Iron ores -- Determination of calcium content -- Flame atomic absorption spectrometric method | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | D31 | | Classification of International Standard | 73.060.10 | | Word Count Estimation | 10,167 | | Date of Issue | 2017-10-14 | | Date of Implementation | 2018-09-01 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China |
GB/T 6730.14-2017: Iron ores -- Determination of calcium content -- Flame atomic absorption spectrometric method ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Iron ores - Determination of calcium content - Flame atomic absorption spectrometric method
ICS 73.060.10
D31
National Standards of People's Republic of China
Partially replace GB/T 6730.14-1986
Iron ores - Determination of calcium content
Flame atomic absorption spectrometry
2017-10-14 Published
2018-09-01 implementation
General Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
China National Standardization Administration released
Foreword
GB/T 6730 "iron ore" is divided into dozens of parts.
This section GB/T 6730 Part 14.
This section drafted in accordance with GB/T 1.1-2009 given rules.
This Part Replaces GB/T 6730.14-1986 "Iron ore chemical analysis atomic absorption spectrophotometric determination of calcium and magnesium" in calcium
Determination of part of this section compared with GB/T 6730.14-1986, in addition to editorial changes, the main technical changes are as follows.
--- Remove the original standard determination of magnesium content;
--- Increasing the normative references;
--- Modify the principle and instrument part of the statement;
--- Increased the requirements of safe operation of the instrument;
--- Modify the absorbance measurement and curve of the operation sequence;
--- Modify the data processing part of the statement;
--- Increased test report.
This part is proposed by China Iron and Steel Association.
This part of the National Iron Ore and Direct Reduced Iron Standardization Technical Committee (SAC/TC317) centralized.
This part of the drafting unit. Anshan Iron and Mining Group, Jiangsu Province (Sha Steel) Iron and Steel Research Institute, Shougang Institute of Technology, Jiangsu Sha Steel Group Co., Ltd.
Division, Exit Inspection and Quarantine of Ningbo, Changsha Institute of Mining and Metallurgy Co., Ltd., Metallurgical Industry Information Standards Institute.
The main drafters of this section. Shen Hengchang, Chen Zhihua, Gao Jingjun, Lu Naping, Zhang Liangfen, Sun Deming, Nianqijiang, Zhu Chunyao, Li Xiaobo,
Wang Dan, Ma Caiyun, Zhang Lei, Chen Zi Bin.
This part replaces the standards previously issued as.
--- GB/T 6730.14-1986.
Iron ores - Determination of calcium content
Flame atomic absorption spectrometry
Warning --- personnel using this section should have formal laboratory experience. This section does not indicate all possible security issues. user
It is your responsibility to take appropriate safety and health measures and to ensure compliance with the conditions of the relevant state laws and regulations.
1 Scope
GB/T 6730 provisions of this part of the flame atomic absorption spectrometry Determination of calcium content.
This section applies to iron ore, iron ore, sinter and pellets Determination of calcium content. Measuring range (mass fraction) .0.030% ~
1.50%.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version applies to this article
Pieces. For undated references, the latest edition (including all amendments) applies to this document.
GB/T 6682 analytical laboratory water specifications and test methods
Preparation of pre-dried samples for analysis of iron ores GB/T 6730.1
GB/T 8170 repair value of about rules and limit values and judgment
GB/T 10322.1 Iron ore sampling and sample preparation methods
GB/T 12806 laboratory glassware single standard line capacity bottle
GB/T 12807 Laboratory glassware graduated pipette
GB/T 12808 laboratory glassware single standard pipette
3 principle
The sample was decomposed with hydrochloric acid-nitric acid and evaporated to dryness. The residue was treated with hydrofluoric acid, melted with sodium carbonate, and combined with the main liquid. In a certain acidity, with chlorine
Strontium as a release agent, at an atomic absorption spectrophotometer wavelength of 422.7nm, the use of air - acetylene flame, were measured.
4 reagent
Unless otherwise indicated in the analysis, the use of only approved analytical reagents and in line with GB/T 6682 provisions of distilled water or its purity phase
When water.
4.1 sodium carbonate, anhydrous.
4.2 Hydrochloric acid, p = 1.19 g/mL.
4.3 hydrochloric acid, 1 3.
4.4 Hydrochloric acid, 5 95.
4.5 nitric acid, p = 1.42 g/mL.
4.6 sulfuric acid, 1 1.
4.7 hydrofluoric acid, p = 1.15 g/mL.
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