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GB/T 43197-2023: Determination of prohibited acid red 73 and solvent red 1 in cosmetics - Liquid chromatography-tandem mass spectrometry
Status: Valid
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB/T 43197-2023 | English | 189 |
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Determination of prohibited acid red 73 and solvent red 1 in cosmetics - Liquid chromatography-tandem mass spectrometry
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GB/T 43197-2023
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Basic data | Standard ID | GB/T 43197-2023 (GB/T43197-2023) | | Description (Translated English) | Determination of prohibited acid red 73 and solvent red 1 in cosmetics - Liquid chromatography-tandem mass spectrometry | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | Y42 | | Classification of International Standard | 71.100.70 | | Word Count Estimation | 10,148 | | Date of Issue | 2023-09-07 | | Date of Implementation | 2024-04-01 | | Issuing agency(ies) | State Administration for Market Regulation, China National Standardization Administration | GB/T 43197-2023: Determination of prohibited acid red 73 and solvent red 1 in cosmetics - Liquid chromatography-tandem mass spectrometry
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
ICS 71.100.70
CCSY42
National Standards of People's Republic of China
Banned components in cosmetics, acid red 73 and solvent red 1
Determination of liquid chromatography-tandem mass spectrometry
Published on 2023-09-07
2024-04-01 Implementation
State Administration for Market Regulation
Released by the National Standardization Administration Committee
Foreword
This document complies with the provisions of GB/T 1.1-2020 "Standardization Work Guidelines Part 1.Structure and Drafting Rules of Standardization Documents"
Drafting.
Please note that some content in this document may be subject to patents. The publisher of this document assumes no responsibility for identifying patents.
This document is proposed by the Light Industry Federation.
This document is under the jurisdiction of the National Standardization Technical Committee for Flavors, Flavors and Cosmetics (SAC/TC257).
This document was drafted by. Shanghai Fragrance Research Institute Co., Ltd., Shanghai Institute of Quality Supervision and Inspection Technology, Infinitus (China) Co., Ltd.
Company, Beijing Product Quality Supervision and Inspection Institute, Hebei Food Inspection Institute, Shanghai Jahwa United Co., Ltd., Proya Chemical
Cosmetics Co., Ltd., Shanghai Institute of Food and Drug Inspection, Yiwu Institute of Standardization, Huzhou Jiaheng Industrial Co., Ltd., Mechulai
(Hangzhou) Cosmetics Co., Ltd., Zhejiang Yanxue Cosmetics Co., Ltd.
The main drafters of this document. Yang Bin, Zheng Yuanjun, Sun Hongmei, Nie Lei, Chen Jun, Lu Xiaorui, Zhang Yan, Ma Qiang, Wang Jing, Chen Zhitao, Sun Shurong,
Zheng Rong, Zhou Jiang, Cao Ping, Han Jiedian, He Guangming, Huang Qimin, Cao Jiadi.
Introduction
The tested substances in this document are prohibited raw materials stipulated in my country's "Technical Safety Specifications for Cosmetics (2015 Edition)".
Banned raw materials refer to substances that are not allowed to be used as cosmetic raw materials. "Safety Technical Specifications for Cosmetics (2015 Edition)" stipulates. "If technology
When it is technically unavoidable that banned substances are brought into cosmetics as impurities, the national limited limits shall be in compliance with its regulations; if no limits are specified, they shall be
Conduct a safety risk assessment to ensure that it will not cause harm to human health under normal, reasonable and foreseeable conditions of use. "
At present, our country has not stipulated the limit value of this substance. The formulation of this document only provides detection methods for the determination of this substance in cosmetics.
Banned components in cosmetics, acid red 73 and solvent red 1
Determination of liquid chromatography-tandem mass spectrometry
Warning---Personnel using this document should have practical experience in regular laboratory work. This document does not address all possible security issues
question. Users are responsible for taking appropriate safety and health measures and ensuring compliance with relevant national regulations.
1 Scope
This document describes the principles of the liquid chromatography-tandem mass spectrometry method for Acid Red 73 (CI27290) and Solvent Red 1 (CI12150) in cosmetics.
management, reagents and materials, instruments and equipment, test procedures, test data processing, recovery rate, precision, etc.
This document is applicable to the determination of Acid Red 73 (CI27290) and Solvent Red 1 (CI12150) in cosmetics such as nail polish, lipstick, and foundation.
In this document, the method detection limits of Acid Red 73 (CI27290) and Solvent Red 1 (CI12150) are both 0.034mg/kg, and the quantification limits are both
0.10mg/kg.
2 Normative reference documents
The contents of the following documents constitute essential provisions of this document through normative references in the text. Among them, the dated quotations
For undated referenced documents, only the version corresponding to that date applies to this document; for undated referenced documents, the latest version (including all amendments) applies to
this document.
GB/T 6682 Specifications and test methods for water used in analytical laboratories
3 Terms and definitions
There are no terms or definitions to be defined in this document.
4 Principles
After the sample is extracted by ultrasonic dispersion with tetrahydrofuran and ammonia solution (or water and sodium chloride), methanol is added and ultrasonic extraction is performed, followed by centrifugation and filtration.
Afterwards, liquid chromatography-tandem mass spectrometry was used to determine the retention time and relative ion pair abundance, and the external standard method was used for quantitation.
5 Reagents and materials
Unless otherwise stated, all reagents used were of analytical grade.
5.1 Water. GB/T 6682, Level 1.
5.2 Methanol. chromatographically pure.
5.3 Acetonitrile. chromatographically pure.
5.4 Ammonium acetate. chromatographically pure.
5.5 Tetrahydrofuran. chromatographically pure.
5.6 Methanol-tetrahydrofuran solution. 1 1 (volume ratio).
5.7 Sodium chloride. analytical grade.
5.8 Ammonia. superior grade pure 25%~28%.
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