|
US$169.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email.
GB/T 3884.8-2012: Methods for chemical analysis of copper concentrates -- Part 8: Determination of zinc content -- Na2EDTA titration method
Status: Valid GB/T 3884.8: Evolution and historical versions
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB/T 3884.8-2012 | English | 169 |
Add to Cart
|
3 days [Need to translate]
|
Methods for chemical analysis of copper concentrates -- Part 8: Determination of zinc content -- Na2EDTA titration method
| Valid |
GB/T 3884.8-2012
|
| GB/T 3884.8-2000 | English | 199 |
Add to Cart
|
2 days [Need to translate]
|
Methods for chemical analysis of copper concentrates Determination of zinc content
| Obsolete |
GB/T 3884.8-2000
|
| GB/T 3884.8-1983 | English | RFQ |
ASK
|
3 days [Need to translate]
|
Methods for chemical analysis of copper concentrates--The EDTA-volumetric method for the determination of lead content
| Obsolete |
GB/T 3884.8-1983
|
PDF similar to GB/T 3884.8-2012
Basic data | Standard ID | GB/T 3884.8-2012 (GB/T3884.8-2012) | | Description (Translated English) | Methods for chemical analysis of copper concentrates -- Part 8: Determination of zinc content -- Na2EDTA titration method | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | H13 | | Classification of International Standard | 77.120.60 | | Word Count Estimation | 7,760 | | Older Standard (superseded by this standard) | GB/T 3884.8-2000 | | Regulation (derived from) | National Standards Bulletin No. 41 of 2012 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the determination of zinc in concentrate method. This section applies to the determination of zinc in concentrate. Measuring range: greater than 1. OO% ~ 13. OO%. | GB/T 3884.8-2012: Methods for chemical analysis of copper concentrates -- Part 8: Determination of zinc content -- Na2EDTA titration method
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
ICS77.120.60
H13
National Standards of People's Republic of China
Replacing GB/T 3884.8-2000
Methods for chemical analysis of copper concentrates
Part 8. Determination of zinc contents
Na2EDTA titration
Part 8. Determinationofzinccontent-
Issued on. 2013-10-01 2012-12-31 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
GB/T 3884 "chemical analysis of copper concentrate" is divided into 14 parts.
--- Part 1. Determination of copper content iodometry;
--- Part 2. Determination of the amount of gold and silver by flame atomic absorption spectroscopy and fire assay;
--- Part 3. Determination of sulfur content - Gravimetric and combustion - titration;
--- Part 4. Determination of magnesium oxide content - Flame atomic absorption spectrometry;
--- Part 5. Determination of the amount of fluorine ion selective electrode method;
--- Part 6. Determination by flame atomic lead, zinc, cadmium and nickel absorption spectrometry;
--- Part 7. Determination of lead content Na2EDTA titration;
--- Part 8. Determination of zinc contents Na2EDTA titration;
--- Part 9. Determination of the amount of arsenic and bismuth hydride generation - atomic fluorescence spectrometry, potassium bromate titration and diethyl ammonia
Silver group acid spectrophotometry;
--- Part 10. Determination of antimony content hydride generation - atomic fluorescence spectrometry;
--- Part 11. Determination of mercury content - Cold atomic absorption spectrometry;
--- Part 12. Determination of the amount of fluorine and chlorine ion chromatography;
--- Part 13. Determination of the amount of copper electrolysis;
--- Part 14. Determination of the amount of gold and silver fire assay gravimetric method and atomic absorption spectrometry.
This section section 8.
Rules in this section in accordance with GB/T 1.1-2009 given draft.
This Part replaces GB/T 3884.8-2000 "Methods for chemical analysis of copper concentrates Determination of zinc content" and GB/T 3884.8-2000 phase
Ratio, mainly the following changes.
--- Text format has been modified;
--- Supplementary terms of precision and test reports.
The non-ferrous metal part by the National Standardization Technical Committee (SAC/TC243) centralized.
This section is responsible for drafting unit. Daye Nonferrous Metals Group Holdings Limited.
This section is drafted. Tongling Nonferrous Metals Group Holdings Limited.
Participated in the drafting of this section. Daye Nonferrous Metals Group Holdings Limited, Zhongtiaoshan Nonferrous Metals Group Co., Ltd., Yunnan Copper
Co., Ltd., Yanggu Yoshimitsu Copper Co., Ltd., Kunming Metallurgy Research Institute.
The main drafters of this section. Xiao-Yan Chen, Li Qinmei, and from Shao, Cheng Haoyu, Wang Junyi, Zeng Jing, often wing Xiang, Wu Zhiqing, Zhang, the
Liuying Bo, Miss Li Qian Ling, Shen Li, Li Jin, Zhaoxiao Pei.
This part of the standard replaces the previous editions are.
--- GB/T 3884.13-1983, GB/T 3884.8-2000.
Methods for chemical analysis of copper concentrates
Part 8. Determination of zinc contents
Na2EDTA titration
1 Scope
This section GB/T 3884 provides for determination of copper concentrate zinc content.
This section applies to the determination of copper concentrate zinc content measurement range. > 1.00% ~ 13.00%.
2 Method summary
Sample decomposition with an acid, in the presence of an oxidant ammonia buffer solution under the separation of iron, manganese and other interfering elements, plus the elimination of covert agents of copper, aluminum, etc.
The interference at pH5.0 ~ 6.0, with xylenol orange as indicator, titrated with Na2EDTA standard titration solution, the measured results for zinc, cadmium together
The amount is deducted from the amount of cadmium zinc content.
3 Reagents
Unless otherwise indicated in the analysis using only recognized as analytical grade reagents and distilled or deionized water or equivalent purity.
3.1 ammonium chloride.
3.2 potassium fluoride.
3.3 ascorbic acid.
3.4 hydrochloric acid (ρ = 1.19g/mL).
3.5 hydrochloride (11).
3.6 sulfate (ρ = 1.84g/mL).
3.7 sulfate (11).
3.8 nitric acid (ρ = 1.42g/mL).
3.9 perchloric acid (ρ = 1.67g/mL).
3.10 sulfur nitrate mixed acid. stirring and cooling, 150mL sulfuric acid (3.6) slowly added to 350mL nitric acid (3.8), and cooled
spare.
3.11 aqueous ammonia (ρ = 0.90g/mL).
3.12 ammonia (11).
3.13 ammonia (119).
3.14 ammonium persulfate solution (100g/L). Using now.
3.15 thiourea saturated solution.
3.16 acetic acid - sodium acetate buffer solution (pH5.5). 150g of anhydrous sodium acetate dissolved in water, was added 50mL of glacial acetic acid, diluted with water to
1000mL, and mix.
3.17 washing solution. 5g of ammonium chloride (3.1) was dissolved in 200mL ammonia (3.13) in.
3.18 Zinc standard solution. Weigh 1.0000g pure zinc (wZn≥99.99%), placed in 300mL beaker, was added 30mL of hydrochloric acid (3.5),
Placed on a hot plate heat gently to dissolve, cooled and transferred to 1000mL volumetric flask, dilute with water to volume, and mix. This solution containing 1mL
|