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Rapid determination of eight elements content for phosphate rock and concentrate -- X-ray fluorescence spectrometry
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GB/T 35996-2018
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Basic data Standard ID | GB/T 35996-2018 (GB/T35996-2018) | Description (Translated English) | Rapid determination of eight elements content for phosphate rock and concentrate -- X-ray fluorescence spectrometry | Sector / Industry | National Standard (Recommended) | Classification of Chinese Standard | D51 | Classification of International Standard | 73.080 | Word Count Estimation | 10,130 | Date of Issue | 2018-03-15 | Date of Implementation | 2018-10-01 | Issuing agency(ies) | State Administration for Market Regulation, China National Standardization Administration |
GB/T 35996-2018: Rapid determination of eight elements content for phosphate rock and concentrate -- X-ray fluorescence spectrometry ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Rapid determination of eight elements content for phosphate rock and concentrate--X-ray fluorescence spectrometry
ICS 73.080
D51
National Standards of People's Republic of China
Phosphorus ore and phosphorus concentrate in eight elements
Rapid determination of X-ray fluorescence spectrometry
Published by.2018-03-15
2018-10-01 implementation
General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China
China National Standardization Administration released
Foreword
This standard was drafted in accordance with the rules given in GB/T 1.1-2009.
This standard is proposed by China Petroleum and Chemical Industry Federation.
This standard is under the jurisdiction of the Chemical Industry Standardization Technical Committee.
This standard is mainly drafted by. Yunnan Phosphor Chemical Group Co., Ltd., China Blue Lianhai Design & Research Institute, Qifu (Group) Co., Ltd., Lake
Peking University Sankou Chemical Co., Ltd., Lianyungang Entry-Exit Inspection and Quarantine Bureau.
Drafters of this standard. Li Yaoji, Zhang Xiaomei, Feng Xiaojun, Zhang Hui, Yang Hong, Ling Huchang Jin, Jiang Zhensheng, Wang Heng.
Phosphorus ore and phosphorus concentrate in eight elements
Rapid determination of X-ray fluorescence spectrometry
Warnings - Persons using this standard should have practical experience in regular laboratory work. This standard does not suggest all possible safety issues.
question. It is the user's responsibility to take appropriate safety and health measures and to ensure compliance with the conditions set by the relevant national laws and regulations.
1 Scope
This standard specifies the determination of eight elements of phosphorus, magnesium, iron, aluminum, silicon, calcium, potassium and sodium in phosphate ore concentrates by X-ray fluorescence spectrometry.
content.
This standard applies to the determination of phosphorus, magnesium, iron, aluminum, silicon, calcium, potassium and sodium in the phosphate ore concentrates. Determination of each element
The range (expressed as oxide) is shown in Table 1.
Table 1 Determination range of each element
Component determination range/%
P2O5 2.00~37.00
MgO 0.20~16.00
Fe2O3 0.50~5.00
Al2O3 0.50~7.00
SiO2 3.00~40.00
CaO 19.00~52.00
K2O 0.10~3.00
Na2O 0.050~1.00
2 Normative references
The following documents are indispensable for the application of this document. For dated references, only dated versions apply to this article
Pieces. For undated references, the latest version (including all amendments) applies to this document.
GB/T 1868 Phosphate rock and phosphate concentrate sampling and sample preparation method
GB/T 1875 Determination of ignition loss in phosphate rock and phosphate concentrates
GB/T 8170 Representation and Determination of Numerical Rounding Rules and Limit Values
General principles of JY/T 016 wavelength dispersive X-ray fluorescence spectrometry
3 Principle
The sample was melted at 1050°C with a mixed flux of lithium tetraborate and lithium metaborate to prepare a glass fuse, which was measured by X-ray fluorescence spectrometry.
The fluorescence X-ray intensity of each element to be measured. According to the quantitative relationship between the fluorescence X-ray intensity of the test element and the content of the test element,
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