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GB/T 31229-2014: Test method for volatility rate by thermogravimetry
Status: Valid
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB/T 31229-2014 | English | 329 |
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Test method for volatility rate by thermogravimetry
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GB/T 31229-2014
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Basic data | Standard ID | GB/T 31229-2014 (GB/T31229-2014) | | Description (Translated English) | Test method for volatility rate by thermogravimetry | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | N04 | | Classification of International Standard | 19.020 | | Word Count Estimation | 14,118 | | Date of Implementation | 4/15/2015 | | Quoted Standard | GB/T 6425; GB/T 8170; GB/T 27762; ASTM E177; ASTM E473; ASTM E691; ASTM E1142 | | Regulation (derived from) | People's Republic of China Announcement of Newly Approved National Standards 2014 No. 22 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This Standard specifies the method for determining thermal gravimetric method of sample evaporation rate. This Standard applies to the use of thermal gravimetric analyzer test 25��C ~ 500��C temperature range, the evaporation rate of a single volatile compo | GB/T 31229-2014: Test method for volatility rate by thermogravimetry---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Test method for volatility rate by thermogravimetry
ICS 19.020
N04
National Standards of People's Republic of China
Standard Test Method for Determination of thermal evaporation rate of gravimetry
Issued on. 2014-09-30
2015-04-15 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Table of Contents
Preface Ⅰ
1 Scope 1
2 Normative references 1
3 Terms and definitions
4 Summary of Test Method 2
5. Significance and Use 3
Interference 3 6
7 Instrument 4
8 5 Sample Preparation
Calibration 9 5
10 Program 5
11 6 Calculation
12 6 Report
Appendix A (informative) Precision and Bias 7
Annex B (informative) The standard numbering ASTME2008-2008 reg reg control number 8
Foreword
This standard was drafted in accordance with GB/T 1.1-2009 given rules.
"Standard Test Method for Determination of the evaporation rate of the thermal gravimetry" This standard is consistent with ASTME2008-2008 technical content.
This standard compared with ASTME2008-2008, the main technical content amended as follows.
--- 3.1 are listed in the definition of thermal gravimetry and thermogravimetry analysis;
Content --- Chapter 9 re-calibration method in accordance with national regulations;
--- Since "mi" and "mf" units of milligrams, and "rv" in units of micrograms per minute for the unit in order to be consistent with the formula (1)
The addition and multiplication 1000;
--- Due to the use of A, at a constant temperature, the evaporation rate of the sample will change with temperature or time, even if there are constant speed volatile
It may volatilize entirely within 30min, so the formula rv = (mi-mf)/30 does not apply, in 11.2 removed the formula;
Chapter 13 --- The precision and bias section from the body moved to Appendix A (informative);
--- Annex B (informative) lists the number of the standard clauses and clauses ASTME2008-2008 a control number
Lanbiao.
This standard was proposed by the Chinese Academy of Sciences.
This standard by the National Standardization Technical Committee of nano technology (SAC/TC279) centralized.
This standard is drafted by. National Center for Nanoscience, NETZSCH Scientific Instruments Trading (Shanghai) Co., Ltd.
The main drafters of this standard. Pu Ling Yu, Chang Huai autumn, Wu Jiao, who Zhiqiang.
Standard Test Method for Determination of thermal evaporation rate of gravimetry
1 Scope
This standard specifies the method for determining the thermal gravimetry sample volatilization rates.
This standard applies to the use of thermal gravimetric analyzer test 25 ℃ ~ 500 ℃ temperature range, the evaporation rate of a single volatile components. This standard is applicable
Samples for testing the evaporation rate greater than 5μg/min of. Responsibility of the user of this standard to determine whether the need to repeat the test and repeat the test
The number of times to achieve the requirements.
This standard does not include associated with its use of all the security issues. Before using this standard method, users are responsible for establishing appropriate
Safety and health standards, specifications and confirm applicability.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
GB/T 6425 Thermal Analysis term
GB/T 8170 GB numerical rounding rules and limit values \u200b\u200band expressed determination
GB/T 27762 TGA quality test methods for calibration indication
ASTME 177 terms used in the precision and bias of the ASTM test method (StandardPracticeforUseofthe
TermsPrecisionandBiasinASTMTestMethods)
ASTME473 Thermal Analysis Standard Terminology (TerminologyRelatingtoThermalAnalysis)
Room ASTME691 laboratory studies Test Method for precision guidance with Practice (StandardPracticeforCon-
ductinganInterlaboratoryStudytoDeterminethePrecisionofaTestMethod)
ASTM E 1142 Standard Terminology (Standard Terminology Relatingto and thermo-physical properties related
ThermophysicalProperties)
3 Terms and Definitions
GB/T 6425, and the following terms and definitions apply ASTME473 and ASTME1142 defined in this document.
3.1
Thermogravimetry thermogravimetry; TG
TGA thermogravimetricanalysis; TGA
Under the program temperature and a certain atmosphere, measuring the technical quality and temperature or the time of the sample.
3.2
Volatile volatility
Volatile solid or liquid material is a gas at room temperature trends.
3.3
Evaporation rate volatilityrate
Solid or liquid material at a given temperature becomes the rate of gas. The test results are volatile content per unit of time to represent.
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